• 한국산학기술학회논문지
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• 제11권9호
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• pp.3161-3167
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• 2010

제어를 위한 기구부의 위치 정보는 BLDC 모터의 홀센서를 이용하여 정확한 위치 및 속도제어가 가능하도록 알고리즘을 구현하였으며, 실제 기구부의 방위각과 고도각에 대한 제어 정밀도를 측정한 결과 최대 $2.02^{\circ}$, $1.01^{\circ}$. 오차범위 $1.86^{\circ}$이내로 비교적 정확하였다. 태양광 발전 모니터링 시스템은 LCU를 중심으로 한 통합 모니터링 제어 시스템으로 모든 장비들은 1:N 방식으로 다중 동시접속이 가능하고, 원격지에서 시스템의 제어 및 현재 상태에 대한 실시간 감시가 가능하도록 개발하였다.

• 한국근적외분광분석학회:학술대회논문집
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• 한국근적외분광분석학회 2001년도 NIR-2001
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• pp.1071-1071
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• 2001

Near-infrared spectroscopy (NIRS) is potentially a powerful and revolutionary technology for environmental analysis. It is supported by a large body of scientific and experiential knowledge. The instrumentation is well-developed, with easy-to-use, highly dependable instruments, but at the same time it is still developing, particularly with the production of more portable and rapid instruments, and more powerful software. NIRS is used globally in numerous industries for commodity analysis. Yet NIRS is largely unknown in the field of environmental chemistry and monitoring, and is not even routinely used in soil analysis, where the research literature on NIRS extends over four decades. Part of the explanation for the poor visibility of NIRS is the fact that NIRS is not routinely taught in Chemistry programs in universities, where most environmental chemists and environmental technicians are trained. This presentation examines the unique capabilities of NIRS, such as rapid, real-time analysis; analysis of whole samples; simultaneous analysis of multiple constituents; cost-effectiveness, and portability, as they match needs for analysis in several environmental areas. Examples of NIRS usage and published and unpublished results will be described for such areas as soil and sediment analysis; water quality monitoring; and nutrient loading in application of manures and sewage sludge (biosolids) to land. Present barriers to the use of NIRS in environmental analysis will be discussed. It is argued that emerging environmental problems and increasing attention to some traditional problems will enhance the application of NIRS in the future.

• 한국축산식품학회지
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• 제41권5호
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• pp.816-825
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• 2021

This study aims to validate a fast method of simultaneous analysis of 365 LCamenable and 142 GC-amenable pesticides in hen eggs by liquid chromatography-tandem mass spectrometry (LC-MS/MS) and gas chromatography-tandem mass spectrometry (GC-MS/MS), respectively, operating in multiple reaction monitoring (MRM) acquisition modes. The sample preparation was based on quick, easy, cheap, effective, rugged, and safe (QuEChERS) extraction. Key method performance parameters investigated were specificity, linearity, limit of quantification (LOQ), accuracy, precision and measurement uncertainty. The method was validated at two spiking levels (10 and 50 ㎍/kg), and good recoveries (70%-120%) and relative standard deviations (RSDs) (≤20) were achieved for 92.9% of LC-amenable and 86.6% of GC-amenable pesticide residues. The LOQs were ≤10 ㎍/kg for 94.2% of LC-amenable and 92.3% of GC-amenable pesticides. The validated method was further applied to 100 egg samples from caged hens, and none of the pesticides was quantified.

• 센서학회지
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• 제31권6호
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• pp.441-447
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• 2022

This study describes a novel method for detecting and measuring partial discharge (PD) on an electrical facility such as an insulated power cable or switchgear using fiber optic sensing technology, and a distributed acoustic sensing (DAS) system. This method has distinct advantages over traditional PD sensing techniques based on an electrical method, including immunity to electromagnetic interference (EMI), long range detection, simultaneous detection for multiple points, and exact location. In this study, we present a DAS system for PD detection with performance evaluation and experimental results in a simulated environment. The results show that the system can be applied to PD detection.

• Mass Spectrometry Letters
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• 제10권1호
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• pp.18-26
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• 2019

We developed a bioanalytical method for simultaneous determination of nine NBOMe derivatives (25H-NBOMe, 25B-NBOMe, 25E-NBOMe, 25N-NBOMe, 25C-NBOH, 25I-NBOH, 25B-NBF, 25C-NBF, and 25I-NBF) in human plasma using liquid chromatography tandem mass spectrometry (LC-MS/MS). Human plasma samples were pre-treated using solid-phase extraction. Separation was achieved on a C18 column under gradient elution using a mobile phase containing 0.1% formic acid in acetonitrile and 0.1% formic acid in water at a flow rate of 0.3 mL/min. Mass detection was performed in the positive ion mode using multiple reaction monitoring. The calibration range was 1-100 ng/mL for all quantitative analytes, with a correlation coefficient greater than 0.99. The intra- and inter-day precision and accuracy varied from 0.85 to 6.92% and from 90.19 to 108.69%, respectively. The recovery ranged from 86.36 to 118.52%, and the matrix effects ranged from 27.09 to 99.72%. The stability was acceptable in various conditions. The LC-MS/MS method was validated for linearity, accuracy, precision, matrix effects, recovery and stability in accordance with the FDA guidance. The proposed method is suitable for reliable and robust routine screening and analysis of nine NBOMe derivatives in forensic field.

• 한국환경농학회지
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• 제39권4호
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• pp.368-374
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• 2020

BACKGROUND: The residual analysis of polar pesticides has remained a challenge. It is even more difficult to simultaneously analyze multiple polar pesticides. Diquat, paraquat, and chlormequat are typical examples of highly polar pesticides. The existing methods for the analysis of diquat, paraquat and chlormequat are complex and time consuming. Therefore, a simple, quick and effective method was developed in the represent study for simultaneous analysis of diquat, paraquat and chlormequat in animal products, meat and fat using UPLC-MS/MS. METHODS AND RESULTS: Sample extraction was carried out using acidified acetonitrile and water and re- extracted with acidified acetonitrile and combine the extracts followed by centrifugation. The extract was then cleaned up with a HLB cartridge after reconstitution with acidic acetonitrile and water. The method was validated in quintuplicate at three different concentrations. The limits of detection (LOD) and quantification (LOQ) were 0.0015 and 0.005 mg/L, respectively. Matrix suppression effect was observed for all of the analytes. A seven point matrix matched calibration curve was constructed for each of the compound resulted excellent linearity with determination coefficients (R2) ≥ 0.991. Accuracy and precision of the method was calculated from the recovery and repeatability and ranged from 62.4 to 119.7% with relative standard deviation less than 18.8%. CONCLUSION: The recovery and repeatability of the developed method were in the acceptable range according to the Codex Alimentarius guideline. The developed method can be applied for the routine monitoring of diquat, paraquat, and chlormequat in animal products, meat and fat.

• 한국수산과학회지
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• 제57권4호
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• pp.327-335
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• 2024

A simultaneous analytical method was developed to quantify antifouling agents and triazine herbicides in seawater using liquid chromatography-tandem mass spectrometry (LC-MS/MS). The target compounds included diuron, irgarol 1051, and prometryn, which are prevalent in marine environments owing to their extensive use in antifouling coatings and agriculture. The analytical procedure involves solid-phase extraction (SPE) using HLB cartridges followed by LC-MS/MS analysis for precise quantification. The method exhibits high recovery rates for diuron (101% ± 1.25), irgarol 1051 (94.7% ± 2.08), and prometryn (93.7% ± 3.06). Seawater samples from 30 coastal sites in Korea were analyzed. Irgarol 1051 was not detected, whereas diuron was consistently detected across all sites, with concentrations from 0.68 to 11.3 ng/L, and prometryn was present at levels between 0.12 and 7.06 ng/L. The highest diuron and prometryn concentrations were recorded along the southeastern and western coasts, respectively. These findings underscore the critical need for continuous monitoring and regulations to manage these contaminants in marine ecosystems, thereby safeguarding ecological integrity and public health. This study establishes a robust analytical framework for the comprehensive assessment of multiple marine contaminants.

• Biomedical Engineering Letters
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• 제8권4호
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• pp.383-392
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• 2018

For prompt gamma ray imaging for biomedical applications and environmental radiation monitoring, we propose herein a multiple-scattering Compton camera (MSCC). MSCC consists of three or more semiconductor layers with good energy resolution, and has potential for simultaneous detection and differentiation of multiple radio-isotopes based on the measured energies, as well as three-dimensional (3D) imaging of the radio-isotope distribution. In this study, we developed an analytic simulator and a 3D image generator for a MSCC, including the physical models of the radiation source emission and detection processes that can be utilized for geometry and performance prediction prior to the construction of a real system. The analytic simulator for a MSCC records coincidence detections of successive interactions in multiple detector layers. In the successive interaction processes, the emission direction of the incident gamma ray, the scattering angle, and the changed traveling path after the Compton scattering interaction in each detector, were determined by a conical surface uniform random number generator (RNG), and by a Klein-Nishina RNG. The 3D image generator has two functions: the recovery of the initial source energy spectrum and the 3D spatial distribution of the source. We evaluated the analytic simulator and image generator with two different energetic point radiation sources (Cs-137 and Co-60) and with an MSCC comprising three detector layers. The recovered initial energies of the incident radiations were well differentiated from the generated MSCC events. Correspondingly, we could obtain a multi-tracer image that combined the two differentiated images. The developed analytic simulator in this study emulated the randomness of the detection process of a multiple-scattering Compton camera, including the inherent degradation factors of the detectors, such as the limited spatial and energy resolutions. The Doppler-broadening effect owing to the momentum distribution of electrons in Compton scattering was not considered in the detection process because most interested isotopes for biomedical and environmental applications have high energies that are less sensitive to Doppler broadening. The analytic simulator and image generator for MSCC can be utilized to determine the optimal geometrical parameters, such as the distances between detectors and detector size, thus affecting the imaging performance of the Compton camera prior to the development of a real system.

• 대한원격탐사학회:학술대회논문집
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• 대한원격탐사학회 2007년도 Proceedings of ISRS 2007
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• pp.493-495
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• 2007

Future sub-meter resolution LEO missions require simultaneous dual-polarization downlink and/or multiple channel downlinks in single polarization. Especially, dual-polarization is needed to cope with bandwidth limitation due to high speed data transmission. Current KARI 13m X-Band antenna system needs to be upgraded to cope with such downlink schemes. This paper describes brief discussions on engineering work regarding how to meet the new requirements with minimum impact on current system as well as C&M (Control and Monitoring) software.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2000년도 하계학술대회 논문집
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• pp.532-535
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• 2000

We have fabricated a sensor system for on-line monitoring the oxygen permeability and diffusivity of six different polymer films using the miniaturized 6 cathode(Ag)-single anode(Ag/AgCl) type hexagonal oxygen electrode. This system consists of multiple input front-end electronics, signal conditioning circuit using the embedded microcontroller 80C196KC, PC interface circuit and PC with the OS for microcontroller and the operating program for this system. The digital low-[ass filter was programmed and the simulated filter characteristics were enough to eliminate the noise from sensor signal. According to the experimental results, the linearity coefficients of the output voltage to oxygen partial pressure for each sensor electrode of six cathode type oxygen sensor are 0.998, 0.997, 0.998, 0.997, 0.997, 0.997 respectively, and the response times are all within 4 minutes.