• Title/Summary/Keyword: moisture stability

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Changes in the Moisture Stability of $CaS:Eu^{2+}$ Phosphors with Surface Coating Methods

  • Yoo, Sun-Hwa;Kim, Chang-Keun
    • Macromolecular Research
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    • v.17 no.11
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    • pp.907-911
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    • 2009
  • To improve the moisture stability of the $CaS:Eu^{2+}$ red phosphor, surface coatings with silica nanoparticles were performed using five different methods, i.e., $P_1$, $P_2$, $P_3$, $P_4$, and $P_5$. The phosphors were coated with silica nanoparticles using a dip coating method ($P_1$) and sol-gel method ($P_2$). The phosphors were coated using a solution containing silica nanoparticles and poly(1-vinyl-2-pyrrolidone), PVP, $(P_3$). The phosphors were also coated with silica nanoparticles by reacting with the 1-vinyl-2-pyrrolidone (VP) monomer ($P_4$) or by reacting with mixtures containing VP and tetraethylorthosilicate ($P_5$). A decrease in the photoluminescence (PL) intensity was observed regardless of the coating methods. However, the moisture stability of the phosphors was enhanced by the coating when aged in a temperature-controlled humidity chamber. Among these methods, the $P_4$ (or $P_5$) method exhibited the greatest increase in moisture stability of the phosphors. The coated phosphors showed a relatively constant intensity with aging time, whereas the uncoated phosphor showed a decrease.

The Study on the Surface Properties of Concrete Tile According to the Autoclave Curing (오토클레이브 양생에 따른 콘크리트 마감재의 표면특성에 관한 연구)

  • Choi Sun-Mi;Jung Ji-Yong;Jung Eun-Hye;Kawg Eun-Gu;Kim Jin-man
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2005.05a
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    • pp.77-80
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    • 2005
  • The surface of concrete tiles is weak in moisture that it occurrenced efflorescence, but in the former study we found that it is possible to ensure moisture stability of concrete surface by autoclaving. So this study is to discuss the moisture stability and Physical Properties of high-strength glossy concrete according to time and temperature of autoclave curing. As the results, by increasing time and temperature of autoclave curing, compressive strength and surface hardness increased and glossiness decreased. In the case to 3 hour and $180^{\circ}C$ of autoclave curing, there is not effloescences in mosture stability test.

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Improved Stability against Moisture of Amlodipine Maleate Tablets using Microcrystalline Cellulose and Pregelatinized Starch (미세결정셀룰로오스와 호화전분을 이용한 암로디핀말레이트 정제의 수분에 대한 안정성 개선)

  • Park, Ho-Seock;Hwang, Woo-Sin;Bang, Kyu-Ho;Park, Jeong-Sook;Cho, Cheong-Weon;Hwang, Sung-Joo
    • Journal of Pharmaceutical Investigation
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    • v.38 no.3
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    • pp.157-162
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    • 2008
  • The aim of the study was to formulate the stable amlodipine maleate tablet by selecting and combining of suitable ingredients. Amlodipine tablets were designed by using different manufacturing methods or formulations. Dissolution rate at 30 min of newly formulated tablets was over 98% in 0.1 M HCl medium. After 4 months storage under accelerated condition, the changes of appearance, loss on drying, content and total impurity were investigated. For long-term stability tests, two formulations of K017 (direct compressed tablets consisting of microcrystalline cellulose and pregelatinized starch) and K018 (wet granulated tablets by OpadryAMB) were stored under $25^{\circ}C$, 60% RH for 24 months. Under the accelerated condition, moisture content in K017 formulation was increased as 5.96% for 4 months, while other formulations with anhydrous monobasic phosphoric potassium or by wet granulation showed higher increase in moisture content compared to K017. In addition, K017 formulation showed a low decrease in contents and total relative substance as 0.8% and 0.7%, respectively. Similar stability of amlodipine in K017 was obtained under the long-term stability test. These results indicate that the K017 combined with microcrystalline cellulose and pregelatinized starch as ingredients is very stable formulation to protect active substance from moisture contact and sustain stability. Therefore, suitable combination of ingredients such as microcrystalline cellulose and pregelatinized starch could attribute to enhance the stability of moisture-labile drug such as amlodipine maleate.

Fabrication and Characterization of Gastrodia elata-loaded Particles for Increased Moisture Stability (수분 안정성 향상을 위한 천마 추출물 함유 분말의 제조 및 평가)

  • Jung, Jae Hwan;Jin, Sung Giu
    • Journal of Powder Materials
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    • v.27 no.3
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    • pp.241-246
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    • 2020
  • To develop Gastrodia elata (GE)-loaded particles for herbal extract dosage forms, various GE-loaded particles containing dextrin, isomalt, maltodextrin, and silicon dioxide as solidifying carriers in the GE water extract are prepared using the spray drying method. Their physical properties are evaluated using the repose angle, Hausner ratio, Carr's index, weight increase rate at 40℃/75% RH condition, and scanning electron microscopy (SEM). Particles made of dextrin improve the fluidity, compressibility, and water stability. In addition, 2% silicon dioxide increases the fluidity and moisture stability. The best flowability and compressibility of GE-loaded particles are observed with TP, dextrin, and silicon dioxide amounts in the ratio of 6/4/0.2 (34.29 ± 2.86°, 1.48 ± 0.03, and 38.29 ± 2.39%, repose angle, Hausner Ratio, and Carr's index, respectively) and moisture stability with a 2% weight increase rate for 14 h at 40℃/75% RH condition. Therefore, our results suggest that the particles prepared by the spray drying method with dextrin and 2% silicon dioxide can be used as powerful particles to improve the flowability, compressibility, and moisture stability of GE.

The finite element analysis on structural stability of road with infiltration trench (침투도랑 설치에 따른 도로 구조 안정성의 유한요소 해석)

  • Jung, Jong-Suk;Hyun, Kyoung-Hak;Kim, In-Tae;Song, Jin-Woo
    • Journal of Korean Society of Water and Wastewater
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    • v.29 no.1
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    • pp.107-122
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    • 2015
  • The purpose of this study is to analyze the structural stability of pavement due to water infiltration at the road with infiltration trench as using the FEM(finite element analysis). Five cases for FEM is divided considering the amount of rainfall and rain duration time. The results of FEM show that the more rainfall in a short period time is faster the change of moisture content. Also, it is the proportional relationship between and changing area of moisture content of more than 40% due to rainfall. Case 3 and 4 are necessary to check the installation of infiltration trench because of moisture content of more than 40%, recovery time of initial moisture content, and changing area of more than 40%. Case 1,2, and 5 have no a significant effect on road pavement structure due to lower moisture content and shorter duration time of higher moisture content.

Aerobic Stability and Effects of Yeasts during Deterioration of Non-fermented and Fermented Total Mixed Ration with Different Moisture Levels

  • Hao, W.;Wang, H.L.;Ning, T.T.;Yang, F.Y.;Xu, C.C.
    • Asian-Australasian Journal of Animal Sciences
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    • v.28 no.6
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    • pp.816-826
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    • 2015
  • The present experiment evaluated the influence of moisture level and anaerobic fermentation on aerobic stability of total mixed ration (TMR). The dynamic changes in chemical composition and microbial population that occur after air exposure were examined, and the species of yeast associated with the deterioration process were also identified in both non-fermented and fermented TMR to deepen the understanding of aerobic deterioration. The moisture levels of TMR in this experiment were adjusted to 400 g/kg (low moisture level, LML), 450 g/kg (medium moisture level, MML), and 500 g/kg (high moisture level, HML), and both non-fermented and 56-d-fermented TMR were subjected to air exposure to determine aerobic stability. Aerobic deterioration resulted in high losses of nutritional components and largely reduced dry matter digestibility. Non-fermented TMR deteriorated during 48 h of air exposure and the HML treatment was more aerobically unstable. On dry matter (DM) basis, yeast populations significantly increased from $10^7$ to $10^{10}cfu/g$ during air exposure, and Candida ethanolica was the predominant species during deterioration in non-fermented TMR. Fermented TMR exhibited considerable resistance to aerobic deterioration. Spoilage was only observed in the HML treatment and its yeast population increased dramatically to $10^9cfu/g$ DM when air exposure progressed to 30 d. Zygosaccharomyces bailii was the sole yeast species isolated when spoilage occurred. These results confirmed that non-fermented and fermented TMR with a HML are more prone to spoilage, and fermented TMR has considerable resistance to aerobic deterioration. Yeasts can trigger aerobic deterioration in both non-fermented and fermented TMR. C. ethanolica may be involved in the spoilage of non-fermented TMR and the vigorous growth of Z. bailii can initiate aerobic deterioration in fermented TMR.

Analysis of Time-Dependent Deformation of CFRP Considering the Anisotropy of Moisture Diffusion

  • Arao, Yoshihiko;Koyanagi, Jun;Hatta, Hiroshi;Kawada, Hiroyuki
    • Advanced Composite Materials
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    • v.17 no.4
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    • pp.359-372
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    • 2008
  • The moisture absorption behavior of carbon fiber-reinforced plastic (CFRP) and its effect on dimensional stability were examined. Moisture diffusivity in CFRP was determined by measuring a specimen's weight during the moisture absorption test. Three types of CFRP specimens were prepared: a unidirectionally reinforced laminate, a quasi-isotropic laminate and woven fabric. Each CFRP was processed into two geometries - a thin plate for determination of diffusivity and a rod with a square cross-section for the discussion of two-dimensional diffusion behavior. By solving Fick's law expanded to 3 dimensions, the diffusivities in the three orthogonal directions were obtained and analyzed in terms of the anisotropy of CFRP moisture diffusion. Coefficients of moisture expansion (CMEs) were also obtained from specimen deformation caused by moisture absorption. During moisture absorption, the specimen surfaces showed larger deformation near the edges due to the distribution of moisture contents. This deformation was reasonably predicted by the finite element analysis using experimentally determined diffusivities and CMEs. For unidirectional CFRP, the effect of the fiber alignment on CME was analyzed by micromechanical finite element analysis (FEA) and discussed.

Effect of the Moisture Content in Sodium Silicate Binder on Bending Strength of Sand Core (규산나트륨 바인더 수분함량이 중자 굽힘강도에 미치는 영향)

  • Panseong Kim;Min A Ber;Man Sig Lee;Jae Ho Baek
    • Journal of Korea Foundry Society
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    • v.44 no.3
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    • pp.70-76
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    • 2024
  • Sodium silicate binder is eco-friendly inorganic binder to substitute organic binder in foundry industry, but it has low stability at moisture. In this study, the bending strength of sand cores with sodium silicate binder at various curing condition was measured for confirm the effect of moisture content in cured sodium silicate binder on the strength and stability. The sodium silicate binder generates stable binder bridge with silicate structure of Q3 and Q2 at 130℃. The maximum bending strength of sand cores was not affected by curing conditions, because the silicate structure of binder bridges was similar. However, the lower moisture content of cured sodium silicate binder, stability of strength was enhanced. Therefore, it was confirmed that the moisture content of cured sodium silicate binder is important factor at stability of sodium silicate binder.

Relationship between Equilibrium Moisture Contents and Dimensional Stability of Handsheet Depending on Fibers Hornification (섬유의 각질화에 따른 수초지의 평형함수율과 치수안정성의 관계)

  • Park, Chang-Soon;Lee, Jin-Ho;Kil, Jung-Ha;Park, Jong-Moon
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.43 no.3
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    • pp.11-20
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    • 2011
  • The conditions to which pulp fibers are exposed during paper production, converting, storage, use, and recycling can induce various changes in fiber morphology, surface characteristics, and suitability for paper production by recycled fibers. Most of those changes can be described by hornification. Paper has highly hygroscopic properties which affect dimensional change by relative humidity variation of surrounding condition. The purpose of this study was to investigate the dimensional stability, moisture contents and dip elongation of handsheets at different relative humidity conditions of recycled kraft pulp and BCTMP. By using recycled fibers, dimensional stability was increased because hygroscopic properties of fibers decreased with repeated recycling treatment. Dip elongation of recycled pulp was higher than that of virgin pulp because of its weak fiber-to-fiber bonding. By recycling pulp, the relative bonded area was decreased because fiber could not swell more than virgin pulp. Dimensional stability largely depended on the equilibrium moisture contents of paper, the fiber-to-fiber bonding strength, and the relative bonded area.

The Study on the Engineering Properties of High-Strength Glossy Concrete Tiles Using Waste Concrete Powders (재생 미분말을 적용한 고강도 광택 콘크리트 마감재의 공학적 특성에 관한 연구)

  • Choi Sun Mi;Jung Ji Yong;Jung Eun Hye;Kim Jin Man
    • Proceedings of the Korea Concrete Institute Conference
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    • 2005.05b
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    • pp.465-468
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    • 2005
  • This Study is concerned workability and the physical properties for practical use of waste concrete powder originated from the manufacturing progress of waste concrete aggregate and it apply to concrete tile. Also because it is important that concrete tile has to ensure the surface moisture stability, for solving the problems aplied curing method is air-dried and autoclave curing. As the result, the physical properties, such as fluent properties, compressive strength, surface hardness and surface glossiness, were decreased with increase of replacement ratio of waste concrete powder, also surface stability was weaked about moisture. But by autoclave curing, it is possible that compressive strength and surface hardness increased, and surface moisture stability is ensured.

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