• Title/Summary/Keyword: modulus

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Rheological Properties of Antiphlamine-S® Lotion (안티푸라민-에스® 로션의 레올로지 특성 연구)

  • Kuk, Hoa-Youn;Song, Ki-Won
    • Journal of Pharmaceutical Investigation
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    • v.39 no.3
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    • pp.185-199
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    • 2009
  • Using a strain-controlled rheometer [Advanced Rheometric Expansion System (ARES)], the steady shear flow properties and the dynamic viscoelastic properties of $Antiphlamine-S^{(R)}$ lotion have been measured at $20^{\circ}C$ (storage temperature) and $37^{\circ}C$ (body temperature). In this article, the temperature dependence of the linear viscoelastic behavior was firstly reported from the experimental data obtained from a temperature-sweep test. The steady shear flow behavior was secondly reported and then the effect of shear rate on this behavior was discussed in detail. In addition, several inelastic-viscoplastic flow models including a yield stress parameter were employed to make a quantitative evaluation of the steady shear flow behavior, and then the applicability of these models was examined by calculating the various material parameters. The angular frequency dependence of the linear viscoelastic behavior was nextly explained and quantitatively predicted using a fractional derivative model. Finally, the strain amplitude dependence of the dynamic viscoelastic behavior was discussed in full to elucidate a nonlinear rheological behavior in large amplitude oscillatory shear flow fields. Main findings obtained from this study can be summarized as follows : (1) The linear viscoelastic behavior is almostly independent of temperature over a temperature range of $15{\sim}40^{circ}C$. (2) The steady shear viscosity is sharply decreased as an increase in shear rate, demonstrating a pronounced Non-Newtonian shear-thinning flow behavior. (3) The shear stress tends to approach a limiting constant value as a decrease in shear rate, exhibiting an existence of a yield stress. (4) The Herschel-Bulkley, Mizrahi-Berk and Heinz-Casson models are all applicable and have an equivalent validity to quantitatively describe the steady shear flow behavior of $Antiphlamine-S^{(R)}$ lotion whereas both the Bingham and Casson models do not give a good applicability. (5) In small amplitude oscillatory shear flow fields, the storage modulus is always greater than the loss modulus over an entire range of angular frequencies tested and both moduli show a slight dependence on angular frequency. This means that the linear viscoelastic behavior of $Antiphlamine-S^{(R)}$ lotion is dominated by an elastic nature rather than a viscous feature and that a gel-like structure is present in this system. (6) In large amplitude oscillatory shear flow fields, the storage modulus shows a nonlinear strain-thinning behavior at strain amplitude range larger than 10 % while the loss modulus exhibits a weak strain-overshoot behavior up to a strain amplitude of 50 % beyond which followed by a decrease in loss modulus with an increase in strain amplitude. (7) At sufficiently large strain amplitude range (${\gamma}_0$>100 %), the loss modulus is found to be greater than the storage modulus, indicating that a viscous property becomes superior to an elastic character in large shear deformations.

A Possible Test Method Proposed for Resilient Modulus (MR) and Analysis of Correlation between Resilient Modulus and Shear Modulus of Track Subgrade Soil (흙노반재료의 회복탄성계수(MR) 결정을 위한 반복삼축압축시험법 제시 및 변형계수 상관성 분석)

  • Park, Jae Beom;Choi, Chan Yong;Lim, Sang Jin;Lim, Yu Jin
    • Journal of the Korean Society for Railway
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    • v.20 no.1
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    • pp.85-98
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    • 2017
  • In general, under the repetitive dynamic load generated by rail cars running on the track, subgrade soil experiences changes of stress conditions such as deviatoric stress (${\sigma}_d$) and bulk stress (${\theta}$). Due to the repetitive change of deviatoric stress (${\sigma}_d$) with number of loadings, the resilient modulus ($M_R$) can be obtained by using the measured resilient strain (${\varepsilon}_r$) after a sufficient number of loadings. At present, no plausible and unified test method has been proposed to obtain the resilient modulus of railway track subgrade soil. In this study, a possible test method for obtaining the resilient modulus ($M_R$) of railway track subgrade soil is proposed; this test, by utilizing repetitive triaxial compression testing, can consider all the important parameters, such as the confining stress, deviatoric stress, and number of loadings. By adapting and using the proposed test method to obtain $M_R$, $M_R$ values for compacted track subgrade soil can be successfully determined using soil obtained in three field sites of railway track construction with changing water content range from OMC. In addition, shear modulus (G) ~ shear strain (${\gamma}$) relation data were also obtained using a mid-size RC test. A correlation analysis was performed using the obtained G and $M_R$ values while considering the strain levels and modes of strain direction.

Studies on the Elasticity, Young Modulus, and Breaking Tension of the Tympanic Membrane in Dog (고막(鼓膜)의 탄성도(彈性度)와 파열장력(破裂張力)에 관(關)한 연구(硏究))

  • Lee, Young-Shik
    • The Korean Journal of Physiology
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    • v.2 no.1
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    • pp.39-45
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    • 1968
  • Recently, in this department, pressure-displacement curve and breaking tension of dog and human tympanic membrane were studied using intact, fresh or dried tympanic membrane attached to external auditory meatus. However, physical property, proper elasticity-Young Modulus, of the tympanic membrane has not been clarified yet. Present study is attempted to further clarify proper Young Modulus of tympanic membrane, and to distinguish possible difference between layer of stratum radiatum and layer of stratum circulare of tympanic membrane in breaking tension and in Young Modulus. Tympanic membrane was excised from sacrificed dog, and preparation was made into the size of approximately 1 mm in width and 3 mm in length. In fresh or dried tympanic membrane, which was dried at $80^{\circ}C$ for 24 hrs., some preparations were made along the long axis parallel to the fibers of radial direction, and others were made along the long axis perpendicular to the radial fibers-circular direction. Breaking tension and displacement according to loading, were measured and Young Modulus was calculated in tympanic membrane preparations under the different experimental conditions. Results obtained are summarized as follows : 1. Young Modulus of fresh tympanic membrane in radial direction was $6.57{\times}10^8\;dyne/cm^2$, and that of fresh preparation in circular direction was $1.68{\times}10^8\;dyne/cm^2$. The Young Modulus of fresh tympanic membrane in radial direction resembles to that of silk and whale moustache. In dried tympanic membrane, Young Modulus of preparation of radial direction was $30.2{\times}10^8\;dyne/cm^2$ and that of preparation in circular direction was $25.0{\times}10^8\;dyne/cm^2$. 2. Breaking tension of fresh tympanic membrane was 44.9 gm/mm in radial preparation, and 7.9 gm/mm in circular preparation. In dried tympanic membrane, breaking tension was 46.7 gm/mm in preparation of radial direction, and 17.2 gm/mm in preparation of circular direction. 3. Much smaller breaking tension of the circular preparation-one fifth to the radial preparation-seemed to be responsible for the higher incidence of circular fiber breaking in tympanic membrane performation caused by trauma or sudden change in atmospheric pressure. 4. The correlation seemed to be very close between breaking tension and Young Modulus in tympanic membrane.

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Residual Stress and Elastic Modulus of Y2O3 Coating Deposited by EB-PVD and its Effects on Surface Crack Formation

  • Kim, Dae-Min;Han, Yoon-Soo;Kim, Seongwon;Oh, Yoon-Suk;Lim, Dae-Soon;Kim, Hyung-Tae;Lee, Sung-Min
    • Journal of the Korean Ceramic Society
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    • v.52 no.6
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    • pp.410-416
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    • 2015
  • Recently, a new $Y_2O_3$ coating deposited using the EB-PVD method has been developed for erosion resistant applications in fluorocarbon plasma environments. In this study, surface crack formation in the $Y_2O_3$ coating has been analyzed in terms of residual stress and elastic modulus. The coating, deposited on silicon substrate at temperatures higher than $600^{\circ}C$, showed itself to be sound, without surface cracks. When the residual stress of the coating was measured using the Stoney formula, it was found to be considerably lower than the value calculated using the elastic modulus and thermal expansion coefficient of bulk $Y_2O_3$. In addition, amorphous $SiO_2$ and crystalline $Al_2O_3$ coatings were similarly prepared and their residual stresses were compared to the calculated values. From nano-indentation measurement, the elastic modulus of the $Y_2O_3$ coating in the direction parallel to the coating surface was found to be lower than that in the normal direction. The lower modulus in the parallel direction was confirmed independently using the load-deflection curves of a micro-cantilever made of $Y_2O_3$ coating and from the average residual stress-temperature curve of the coated sample. The elastic modulus in these experiments was around 33 ~ 35 GPa, which is much lower than that of a sintered bulk sample. Thus, this low elastic modulus, which may come from the columnar feather-like structure of the coating, contributed to decreasing the average residual tensile stress. Finally, in terms of toughness and thermal cycling stability, the implications of the lowered elastic modulus are discussed.

A Study on Anticipation System of Shudder Distinction by the Physical Shape Alteration in Static Condition (고정상태에서 신체 형태변화에 따른 떨림 판별의 예측시스템 연구)

  • Kim, Jeong-Lae;Choi, Jae-Sil;Hwang, Kyu-Sung
    • The Journal of the Institute of Internet, Broadcasting and Communication
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    • v.17 no.3
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    • pp.115-120
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    • 2017
  • Moving techniques is made up the physical moving status of the flow distinction modulus (FDM) and stream distinction modulus (SDM) on the shudder moving shape. Condition of the distinction modulus by the shudder moving shape is organized the dangle moving system. As to define the physical moving of special signal on the matter, we compared a shudder value of the flow distinction modulus on the flow state. The concept of stream distinction modulus is analyzed the reference of stream distinction signal and stream distinction signal by the stream state. For detecting a variation of the FDM-SDM of the maximum-minimum and average in terms of the moving shape, and shudder moving value that is a shudder value of the top variation of the $Top-{\varepsilon}$ MAX-MIN-AVG with $(-0.817){\pm}0.15$ units, that is a shudder value of the peripheral variation of the $Per-{\varepsilon}$ MAX-MIN-AVG with $(-2.53){\pm}(-0.11)$ units, that is a shudder value of the limbus variation of the $Lim-{\varepsilon}$ MAX-MIN-AVG with $(-0.29){\pm}0.03$ units, that is a shudder value of the center variation of the $Cen-{\varepsilon}$ MAX-MIN-AVG with $(-0.09){\pm}(-0.01)$ units. The dangle moving will be to assess at the capacity of the physical moving shape for the control degree of distinction modulus on the FDM-SDM that is showed the flow and stream shape by the distinction modulus system. Dangle distinction system is adjusted of a shape by the special moving and is included a shudder data of dangle moving modulus.

The Measurement Errors of Elastic Modulus and Hardness due to the Different Indentation Speed (압입속도의 변화에 따른 탄성계수와 경도의 오차 연구)

  • Lee, Kyu-Young;Lee, Chan-Bin;Kim, Soo-In;Lee, Chang-Woo
    • Journal of the Korean Vacuum Society
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    • v.19 no.5
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    • pp.360-364
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    • 2010
  • Most research groups used two analysis methods (spectroscopy and nanotribology) to measure the mechanical properties of nano-materials: NMR (Nuclear Magnetic Resonance), IR (Infrared Spectroscopy), Raman Spectroscopy as the spectroscopy method and AFM (Atomic Force MicroScope), EFM (Electrostatic Force Microscope), KFM (Kelvin Force Microscope), Nanoindenter as the nanotribological one. Among these, the nano-indentation technique particularly has been recognized as a powerful method to measure the elastic modulus and the hardness. However, this technique are prone to considerable measurement errors with pressure conditions during measurement. In this paper, we measured the change of elastic modulus and hardness of an Al single crystal with the change of load, hold, and unload time, respectively. We found that elastic modulus and hardness significantly depend on load, hold, and unload time, etc. As the indent time was shortened, the elastic modulus value decreased while the hardness value increased. In addition, we found that elastic modulus value was more sensitive to indent load, hold, and unload time than the hardness value. We speculate that measurement errors of the elastic modulus and the hardness originate from the residual stress during indenting test. From our results, the elastic modulus was more susceptible to the residual stress than the hardness. Thus, we find that the residual stress should be controlled for the minimum measurement errors during the indenting test.

Characteristics of Hardness and Elastic Modulus of PMMA Film using Nano-Tribology (Nanotribology를 이용한 PMMA 박막의 Hardness와 Elastic Modulus 특성 연구)

  • Kim, Soo-In;Kim, Hyun-Woo;Noh, Seong-Cheol;Yoon, Duk-Jin;Chang, Hong-Jun;Lee, Jong-Rim;Lee, Chang-Woo
    • Journal of the Korean Vacuum Society
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    • v.18 no.5
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    • pp.372-376
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    • 2009
  • In the modern semiconductor industry, lithography process is used to construct specific patterns. However, due to the decreasing of line width, these days, more and more researchers are interested in PMMA(Poly Methyl Methacrylate) lithography by using e-beam instead of the prior method, PR(Photoresist) lithography by using UV(Ultra-Violet). Additionally, the patterns constructed by lithography are collapsed during the process of cleansing remnants and the resistance against the breakdown of the patterns is known to be proportional to the elastic modulus of pattern-constructing materials. In this research, we measured the change of hardness and elastic modulus of PMMA film surface according to the change of time spent to soft-bake the PMMA film. During the measurement, we controlled the tip pressure from $25{\mu}N$ to $8,500{\mu}N$ having intervals that are $134.52{\mu}N$. For these measurements, we used the Triboindenter from Hysitron to gauge the hardness and elastic modulus and the tip we used was Berkovich diamond Tip.

Comparison of Elastic Moduli of Subgrade Soils Using Plate Loading Test, Soil Stiffness Gauge and Dynamic Cone Penetrometer (평판재하시험, 흙강성측정기 및 동적콘관입시험기를 이용한 노상토의 탄성계수 비교)

  • Kim, Kyu-Sun
    • Journal of the Korean Geotechnical Society
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    • v.31 no.3
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    • pp.63-72
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    • 2015
  • This paper describes the correlation and relationship between elastic moduli measured by three stiffness measurement methods with different mechanical characteristics to evaluate the compaction characteristics of subgrade soils. The Soil Stiffness Gauge (SSG) with very small strain (${\approx}0.001%$) ranges, static Plate Loading Test (PLT) with mid-level strain (${\approx}0.01{\sim}0.1%$) ranges, and Dynamic Cone Penetrometer (DCP) using penetration resistance were implemented to measure the elastic modulus. To use the elastic modulus measured by different measurement methods with a wide range of strain in practice, it is required to identify the correlation and relationship of measured values in advance. The comparison results of the measured elastic moduli ($E_{SSG}$, $E_{PLT}$, $E_{DCP}$) using the three measurement methods for domestic and overseas subgrade soils under various conditions indicate that the evaluated elastic modulus relies on the types of soils and the level of stress condition. The correlation analysis of the measured elastic moduli except the data of cement treated soils indicates that the static elastic modulus ($E_{PLT}$) is evaluated as about 60 to 80% of the dynamic elastic modulus ($E_{SSG}$). Unusual soils such as cement treated soils are required to be corrected by the stress correction during the correlation analysis with typical soils, because these types of soils are sensitive to the stress condition when measuring the static elastic modulus ($E_{PLT}$) of soils. In addition, when considering the use of DCP data for the evaluation of the elastic modulus ($E_{DCP}$), the measured data of the elastic modulus less than 200 MPa show more reliable correlation.

Comparison of flexural strength and modulus of elasticity in several resinous teeth splinting materials (여러 레진계 치아고정 재료의 굴곡강도 및 탄성계수 비교)

  • Yoo, Je-In;Kim, Soo-Yeon;Batbayar, Bayarchimeg;Kim, Jin-Woo;Park, Se-Hee;Cho, Kyung-Mo
    • Journal of Dental Rehabilitation and Applied Science
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    • v.32 no.3
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    • pp.169-175
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    • 2016
  • Purpose: Direct splinting material should have high flexural strength to withstand force during mastication and low modulus of elasticity to provide some movement while force applied for relief of stress. The purpose of this study was to compare flexural strength and modulus of elasticity of several resinous splinting materials. Materials and Methods: Four materials; Super-Bond C&B, G-FIX, G-aenial Universal Flo, FiltekTM Z350 XT; were used in this study. Fifteen rectangular bar specimens of each material were prepared. Three-point bending test were performed to determine physical properties. Maximum load at fracture was recorded and flexural strength and modulus of elasticity were calculated. One-way analysis of variance (ANOVA) and Scheffe's tests at a 0.05 level of significance were conducted on all test results. Results: Statistical analysis reveals that Super-Bond C&B had significant low mean value for flexible strength and the other three materials showed no significant difference. For modulus of elasticity, Super-Bond C&B exhibited statistically lower modulus of elasticity. G-FIX presented intermediate result, showing statistically higher modulus of elasticity than Super-Bond C&B but lower than G-aenial Universal Flo and FiltekTM Z350 XT. There was no significant difference on modulus of elasticity between G-aenial Universal Flo and FiltekTM Z350 XT. Conclusion: Using a G-FIX, the newly commercially available splinting material, which shows higher fracture resistance properties comparable to flowable and restorative composite resin and a relatively flexible nature might be a beneficial for stabilizing teeth mobility.