• Title/Summary/Keyword: mixing mill

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Mixed Grinding Effect on Kaolinite-Aluminum Trihydroxide Mixture and Its Influence on Mullite Formation (Kaolinite-Aluminum Trihydroxide의 혼합물의 혼합분쇄효과 및 Mullite의 생성에 미치는 영향)

  • 류호진
    • Journal of the Korean Ceramic Society
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    • v.34 no.2
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    • pp.195-201
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    • 1997
  • The present paper describes the effect of dry mixed grinding on kaolinite-aluminum trihydroxide mixture with a planetary ball mill before sintering and its influence on mullite formation during sintering. The size reduction of the mixture is market in the early stage of grinding and the obtained fine particles agglomerate subsequently with an increase of grinding time. The crystal structure of the mixture is collapsed easily into an amorphous one by planetary ball milling, of which amount increases with an increase of grinding time. Only mullite phase except for anatase as an inherent impurity in kaolinite appeared in the sintered body of the mixtures with mixed grinding as relatively lower temperature 1523K, while corundum, cristobalite, and Al-Si spinel phases, besides mullite were formed in the sintered body of the mixture without mixed grinding. Therefore, the mixed grinding treatment is very effective to improve the homogeneous mixing and disp-ersion of the mixture of raw materials on a micro scale and to decrease the thermal decomposition tem-perature by crystal structure change of them so as to obatin direct preparation of mullite with high purity at relatively low temperature.

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Preparation of High-Fiber Bread with Barley Flour (보리가루를 이용한 고식이섬유 빵의 제조)

  • Cho, Mi-Kyung;Lee, Won-Jong
    • Korean Journal of Food Science and Technology
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    • v.28 no.4
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    • pp.702-706
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    • 1996
  • Husked barley contained 17.2% dietary fiber and naked barley contained 14.9% dietary fiber. The barley was ground in a Udy cyclotec mill having a 0.5 mm screen and sieved with a 400-mesh screen (38 m openings). Coarse material of naked barley retained by the screen, with a weight yield of 54.1%, contained 7.0% soluble dietary fiber, 13.9% insoluble dietary filer and 20.9% total dietray fiber. As the naked barley flour level increased in bread baking, the water absorption, mixing time, and loaf weight increased, but the loaf volume decreased. Barley flour was added to wheat flour at a replacement level of 10% without a large adverse effect on bread quality, and the dietary fiber content of bread was increased from 3.0% to 5.0%. The soluble dietary fiber content was not changed, but the insoluble dietary fiber content was increased during the baking process.

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Study on the Wastewater treatment as a Coagulant Using the Waste Oyster Shells and Loess (폐굴껍질과 황토로 제조한 응집제를 利用한 폐수처리에 관한 연구)

  • 고현웅;장성호;성낙창
    • Resources Recycling
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    • v.11 no.2
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    • pp.45-51
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    • 2002
  • This study was performed to investigate removal efficiency of wastewater by the prepared coagulant using waste oyster shell and loess. Waste oyster shell and loess contain respectively high CaO(55.43% by weight), $SiO_2$(45.30% by weight). Waste oyster shell was calcined to improve the purity of CaO at the calcination condition of $900^{\circ}C$ for 2hours, and then crushed 0.074 mm(200mesh) size by ball mill. Also, coagulant was prepared with calcined waste oyster shell and loess powder by hydration reaction. Calcined waste oyster shell and loess powder were combined with mixing ratio of 6 : 4, 7:3, 8:2 and 9:1. Though comparison experiment between prepared coagulant and chemical )$Ca(OH_2$, prepared coagulant was proved as having replaceable possibility of chemical )$Ca(OH_2$in wastewater treatment plant.

A Study on the Millbase Dispersion for LCD Color Filters (LCD 컬러필터용 밀베이스의 분산 연구)

  • Jung, Il-Bong;Ahn, Suk-Chul;Nam, Su-Yong
    • Clean Technology
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    • v.14 no.1
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    • pp.21-28
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    • 2008
  • The properties of the dispersion of the red, green, and blue pigments were investigated for the manufacture of the millbase of LCD color filters. Their physical properties and viscosity were controlled to apply to the screen printing in order to substitute the existing photolithography method. The best dispersion properties were obtained with dispersant BYK-2000 and monomer EB-140. The millbase was pre-mixed at 500 rpm for 30 min, and dispersed at 4000 rpm for 5 - 6 hour by Torus Mill. The resulting particle sizes were $100{\sim}110\;nm$ for red, $50{\sim}70\;nm$ for green, and $60{\sim}80\;nm$ for blue. When the millbase viscosity was 200-300 cps in the low viscosity formulation, an efficient impact of the beads on pigments was achieved. The dispersion properties were confirmed from the rheological behavior and color characteristics.

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Growth pf Plug Seedlings of Capsicum annuum and Lycopersicum esculentum as Affected by the Mixing Ratio of Aquafarm Waste Water Sludge in the Growing Medium (담수양어장 슬러지의 배지내 혼합비율이 고추(Capsicum annuum)와 토마토(Lycopersicum esculentum) 공정묘의 생장에 미치는 영향)

  • Lee, Eun-Ju;Hwang, Seung-Jae;Kim, Ik-Joon;Park, Young-Hoon;Jeong, Byoung-Ryong
    • Journal of Bio-Environment Control
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    • v.12 no.4
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    • pp.184-189
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    • 2003
  • This research was conducted to determine the effect of mixing ratio of aquafarm waste water sludge (AWWS) in the growing medium as a source of fertilizers on growth of plug seedlings of pepper (Capsicum annuum L.) and tomato (Lycopersicum esculentum Mill.). Increased mixing ratio of AWWS resulted in increased fresh and dry weights, leaf area, plant height, and total chlorophyll content, although there were slight differences in growth characteristics at 20 and 40 days after sowing. Concentration of AWWS affected insignificantly the percent dry matter, number of leaves, and length of the longest root. The addition of AWWS increased pH and decreased EC in the medium as compared to that of chemical fertilizer. Compared to the control of a liquid fertilizer, 4 or 8 kg AWWS${\cdot}45L^{-1}$ medium (Sludge 4) gave a similar or slightly better growth. Above results suggested that addition of about 4 kg AWWS${\cdot}45L^{-1}$medium is sufficient for seedling growth and the AWWS can be used as a substitute for the liquid fertilizer in plug seedling production.

Impurity Pick-Up for the Preparation of NiCuZn Ferrite Powder Using Ball Milling Process (NiCuZn Ferrite 분말제조에 있어서 Ball Mill 분쇄 공정 중에 혼입되는 불순물의 함량)

  • 고재천;류병환
    • Journal of the Korean Magnetics Society
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    • v.9 no.4
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    • pp.217-222
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    • 1999
  • The pick up impurity was studied for preparing the NiCuZn ferrite powder by a ball milling method that usually uses in the industrial ceramic process. The raw materials of NiO, CuO, ZnO, and $Fe_2O_3$ powder were weighted according to various spinel composition and mixed for 18 hrs by a wet ball milling method after that the slurry was followed by spray dried and calcined at $700^{\circ}C$ 3 hrs. The calcined NCZF powder was finally ball milled during 65 hrs as same method. The stainless steel ball and jar are used as mixing and milling equipment and the solid concentration of the slurry was 25 vol%. The impurities, stainless steel pickup, were effected by the composition of raw materials especially iron oxide, nickel oxide in the mixing process and by the rate of calcine of NiCuZn ferrite in final milling process. The empirical equation of stainless steel pickup was driven in the wet ball milling system. Finally, the composition of NiCuZn ferrite could be controlled by the empirical equation.

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Formation of Non-equilibrium Cu-Ta-Mo Alloy Powders by Mechanical Alloying (기계적 합금화법에 의한 비평형 Cu-Ta-Mo계 합금분말의 제조)

  • 이충효;이상진
    • Journal of Powder Materials
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    • v.6 no.4
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    • pp.314-319
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    • 1999
  • The solid state reaction by mechanical alloying(MA) generally proceeds by lowering the free energy as the result of a chemical reaction at the interface between the two adjacent layers. However, Lee et $al.^{1-5)}$ reported that a mixture of Cu and Ta, the combination of which is characterized by a positive heat of mixing of +2kJ/mol, could be amorphized by mechanical alloying. This implies that there exists an up-hill process to raise the free energy of a mixture of pure Cu and la to that of an amorphous phase. It is our aim to investigate to what extent the MA is capable of producing a non-equilibrium phase with increasing the heat of mixing. The system chosen was the ternary $Cu_{30}Ta_{ 70-x}Mo_ x$ (x=35, 10). The mechanical alloying was carried out using a Fritsch P-5 planetary mill under Ar gas atmosphere. The MA powders were characterized by the X-ray diffraction with Cu-K $\alpha$ radiation, thermal analysis, electron diffraction and TEM micrographs. In the case of x=35, where pure Cu powders were mixed with equal amount of pure Ta and Mo powders, we revealed the formation of bcc solid solution after 150 h milling but its gradual decomposition by releasing fcc-Cu when milling time exceeded 200 h. However, an amorphous phase was clearly formed when the Mo content was lowered to x=10. It is believed that the amorphization of ternary $Cu_{30}Ta_{60}Mo_{10}$ powders is essentially identical to the solid state amorphization process in binary $Cu_{30}Ta_{70}$ powders.

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Carbon Nano Tube Dispersion Evaluation in B-stage Resin Films (B-stage 레진 필름의 카본나노튜브 분산도 평가 및 제조공정 최적화)

  • Oh, Young-Seok;Park, Tea-Hoon;Byun, Joon-Hyung;Yi, Jin-Woo;Kim, Byung-Sun;Joe, Chee-Ryong
    • Composites Research
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    • v.29 no.6
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    • pp.353-357
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    • 2016
  • An appropriate way to fabricate a hybrid composite containing evenly dispersed carbon nano tubes(CNTs) is to stacking B-stage resin films that contain evenly dispersed CNTs and various reinforcing fiber layers alternatively. In the present study, B-stage resin films are manufactured via shear mixing and three-roll milling. CNT dispersion in resin via these two processes are evaluated by SEM on their fracture surfaces. For more efficient process, the dispersivities are evaluated according to the number of calendering passes. Samples are made for different number of passes during calendering, and their dispersions are evaluated via SEM fractographs as well as by measuring their electrical conductivities. Additionally, the optimal process conditions are obtained by measuring the electrical conductivity and evaluating their dispersivity of the samples prepared by gap mode and force mode.

A Study on the Quality Improvement of Bread Using the Whole Waxy Sorghum Flours Prepared with Different Milling Methods (분쇄방법을 달리한 통곡 찰수수가루를 이용한 수수빵의 제조 및 품질 개선)

  • Ryu, Bog-Mi;Kim, Chang-Soon
    • Korean journal of food and cookery science
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    • v.30 no.3
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    • pp.262-270
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    • 2014
  • This study was conducted in order to investigate the properties of bread making and quality improvement when wheat flour is replaced with whole waxy sorghum flour. Sorghum flour, which was prepared with two types of milling methods of pin mill and ultra fine pulverization, was used at different levels ranging from 10, 20 and 30%, respectively. The pasting properties of peak viscosity, setback viscosity and pasting temperature of the composite flour containing pin-milled sorghum flour were higher than those of ultra fine pulverized sorghum flour. The volumes of sorghum bread were lower than that of wheat bread; moreover, they gradually decreased with increasing amounts of sorghum flour, which has inferior dough properties and therefore collapses in the oven. The use of vital gluten (12% based on sorghum flour weight) and emulsifier (SSL; sodium stearoyl lactylate) increased the extensibility and resistance to the extension of the dough, thereby improving its rheological properties. Thus, the oven spring of bread containing sorghum was improved, demonstrating as loaf volume increase up to 15%. However, in the case of breads containing 30% sorghum flour, the loaf volumes were still unacceptably low. Therefore, the formula and the bread making process were further modified as follows: An increase of vital gluten ($12%{\rightarrow}18%$) and shortening ($3%{\rightarrow}6%$), a decrease of mixing time and dough fermentation temperature, and the addition of sorghum flour after gluten development during mixing. The above modifications resulted in the improvement of sorghum bread quality. Therefore, we suggest that pin-milled sorghum flour is more appropriate than ultra fine pulverized sorghum flour for making bread.

Treatment of Phenol Contaminated Soil Using Sulfidated Zero-Valent Iron as a Persulfate Activator for Advanced Oxidation Process (황화영가철 기반의 과황산 고도산화공정을 이용한 페놀 오염토양 처리)

  • Hyuk Sung Chung;Nguyen Quoc Bien;Jae Young Choi;Inseong Hwang
    • Journal of Soil and Groundwater Environment
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    • v.28 no.1
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    • pp.15-24
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    • 2023
  • A persulfate(PS)/sulfidated microscale zero-valent iron(S-mZVI) system was tested for treating a soil contaminated with phenol. Sulfidation of bare mZVI was conducted using a mechanochemical process utilizing a ball mill in order to improve persulfate activation capacity and stability of unmodified mZVI. The synthesized S-mZVI performed markedly better than the bare mZVI in activating PS. The optimum molar ratio of sulfur to mZVI was around 0.12. In the soil slurry experiments, a very rapid and complete removal of phenol was observed at the optimum molar ratios of PS to S-mZVI of 2:1 and PS to phenol of 16:1. The phenol removal efficiencies decreased as the water content of the slurries decreased. This was believed to be due to increased soil oxidant demand as the amount of soil was increased as relative to the water content. To evaluate the field applicability of the process, slurry experiments adopting high soil contents were carried out that simulated in-situ soil mixing conditions. These experiments resulted in substantially compromised degradation efficiencies of 54.3% and 43.8% within 4 hours. The current study generally shows that the PS/S-mZVI process has a potential to be developed into a remediation technology for soils contaminated with organics.