• The Journal of Korean Academy of Prosthodontics
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• 제29권2호
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• pp.245-265
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• 1991

The purpose of this study was to observe the changes of the elemental transmission and bond strength between the metal and porcelain according to various kinds of ion beam mixing method. ion beam mixing of $meta1/SiO_2$ (silica), $meta1/Al_2O_3$(alumina) interfaces causes reactions when the $Ar^+$ was implanted into bilayer thin films using a 100KeV accelerator which was designed and constructed for this study. A vacuum evaporator used in the $10^{-5}-10^{-6}$ Torr vacuum states for the evaporation. For this study, three kinds of porcelain metal selected, -precious, semiprecious, and non-precious. Silica and alumina were deposited to the metal by the vacuum evaporator, separately. One group was treated by two kinds of dose of the ion beam mixing $(1\times10^{16}ions/cm^2,\;5\times10^{15}ions/cm^2)$, and the other group was not mixed, and analyzed the effects of ion beam mixing. The analyses of bond strength, elemental transmissions were performed by the electron spectroscopy of chemical analysis (ESCA), light and scanning electron microscope, scratch test, and micro Vickers hardness tests. The finding led to the following conclusions. 1. In the scanning electron and light microscopic views, ion beam mixed specimens showed the ion beam mixed indentation. 2. In the micro Vickers hardness and scratch tests, ion beam mixed specimens showed higher strength than that of non mixed specimens, however, nonprecious metal showed a little change in the bond strength between mixed and non mixed specimens. 3. In the scratch test, ion beam mixed specimens showed higher shear strength than that of non treated specimens at the precious and semiprecious groups. 4. In the ESCA analysis, Au-O and Au-Si compounds were formed and transmission of the Au peak was found ion beam mixed $SiO_2/Au$ specimen, simultaneously, in the higher and lower bonded areas, and ion beam mixed $SiO_2/Ni-Cr$ specimen, oxygen, that was transmitted from $SiO_2\;to\;SiO_2/Ni-Cr$ interface combined with 12% of Ni at the interface.

• The Journal of Korean Academy of Prosthodontics
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• 제30권2호
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• pp.135-154
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• 1992

This study was performed to analyze bond strength, the alterations of the interfaces between metal films which are populary used and considered to contribute to the chemical reaction with porcelain, according to constant ion- beam- mixing, and the relation between interfacial chemical reactions and bond strength in metal/porcelain specimens. For this study, three seperate metals : selected-gold, indium and tin were chosen ; each to be bonded to a seperate body porcelain. Bonding occurs when the metal is deposited to the body porcelain using a vacuum evaporator. The vacuum evaporator used $10^{-5}\sim10^{-6}$ Torr vacuum states for the evaporation of various metals (Au, Sn, In). Ion-beam-mixing of the porcelain/metal interfaces caused reactions when the Ar+ was implanted into thin films using a 80 KeV accelerator. These ion-beam-mixed specimens were then compared with an unmixed control group. An analysis of bond strength and ionic changes between the the metal and porcelain was performed by electron spectroscopy of chemical analysis (ESCA) and scratch test. The finding led to the following conclusions : 1. Light microscopic views of the scratch test : The ion-beam-mixed Au/porcelain specimen showed narrower scratched streams than the unmixed specimen. However, the Sn/porcelain, In/porcelain specimens showed no differences in the two conditions. 2. Acoustic emissions in scratch tests : The ion-mixed Au/porcelain, In/porcelain specimens showed signals closer to the metal/porcelain interfaces than unmixed specimens. Conversely, the ion-mixed Sn/porcelain specimen showed more critical signals in superficial portions than unmixed specimens. 3. After ion- beam-mixing, the Au/porcelain specimen showed apparently increased bond strength, and the In/porcelain specimen showed very slightly increased bond strength. However, the Sn/porcelain specimen showed no differences between ion mixed specimen and the unmixed one. 4. ESCA analysis : The ion-beam-mixed Au/porcelain specimen showed a higher peak separated value (4.3eV) than that of the unmixed specimen(3.65eV), the ion-beam-mixed In/porcelain specimen showed a higher peak separated value (9.43eV) than that of the unmixed specimen(7.6eV) and the ion-beam-mixed Sn/porcelain specimen showed a higher peak separated value (8.79eV) than that of the unmixed specimen(8.5eV). 5. Interfacial changes were observed in the ion-mixed Au/porcelain, In/porcelain and Sn/porcelain specimens. Especially, significant interfacial changes were measured in the ion- mixed Sn/porcelain specimen. Tin dioxide(SnO2) and a combination of pure tin and tin dioxide (Sn+SnO2) were produced. 6. In the Au/porcelain specimen, the interfacial chemical reaction showed increased bond strength between gold and porcelain substrate. But, in the In/porcelain, Sn/porcelain specimens, interfacial chemical reactions did not affected the bond strength between metal and porcelain substrate. Especially, bonding strength on the ion mixed Sn/porcelain specimen showed the least amount of difference.

• Journal of Mechanical Science and Technology
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• 제19권11호
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• pp.2016-2024
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• 2005

In this work, a mixed beam approach that combines both the stiffness and the flexibility methods has been performed to analyze the coupled composite blades with closed, two-cell cross-sections. The Reissner's semi-complementary energy functional is used to derive the beam force-displacement relations. Only the membrane part of the shell wall is taken into account to make the analysis simple and also to deliver a clear picture of the mixed method. All the cross section stiffness coefficients as well as the distribution of shear across the section are evaluated in a closed-form through the beam formulation. The theory is validated against experimental test data, detailed finite element analysis results, and other analytical results for coupled composite blades with a two-cell airfoil section. Despite the simple kinematic model adopted in the theory, an accuracy comparable to that of two-dimensional finite element analysis has been obtained for cases considered in this study.

• Proceedings of the Korean Vacuum Society Conference
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• 한국진공학회 1998년도 제14회 학술발표회 논문개요집
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• pp.133-133
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• 1998

In the thin film alloy formation of the transition metals ion-beam-mixing technique forms a metastable structure which cannot be found in the arc-melted metal alloys. Sppecifically it is well known that the studies about the electronic structure of ion-beam-mixed alloys pprovide the useful information in understanding the metastable structures in the metal alloy. We studied the electronic change in the ion-beam-mixed ppt-Ct alloys by XppS and XANES. These analysis tools pprovide us information about the charge transfer in the valence band of intermetallic bonding. The multi-layered films were depposited on the SiO2 substrate by the sequential electron beam evapporation at a ppressure of less than 5$\times$10-7 Torr. These compprise of 4 ppairs of ppt and Cu layers where thicknesses of each layer were varied in order to change the alloy compposition. Ion-beam-mixing pprocess was carried out with 80 keV Ae+ ions with a dose of $1.5\times$ 1016 Ar+/cm2 at room tempperature. The core and valence level energy shift in these system were investigated by x-ray pphotoelectron sppectroscoppy(XppS) pphotoelectrons were excited by monochromatized Al K ａ(1486.6 eV) The ppass energy of the hemisppherical analyzer was 23.5 eV. Core-level binding energies were calibrated with the Fermi level edge. ppt L3-edge and Cu K-edge XANES sppectra were measured with the flourescence mode detector at the 3C1 beam line of the ppLS (ppohang light source). By using the change of White line(WL) area of the each metal sites and the core level shift we can obtain the information about the electrons pparticippating in the intermetallic bonding of the ion-beam-mixed alloys.

• Journal of Mechanical Science and Technology
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• 제19권3호
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• pp.811-819
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• 2005

In this study, we present a new efficient hybrid-mixed composite laminated curved beam element. The present element, which is based on the Hellinger-Reissner variational principle and the first-order shear deformation lamination theory, employs consistent stress parameters corresponding to cubic displacement polynomials with additional nodeless degrees in order to resolve the numerical difficulties due to the spurious constraints. The stress parameters are eliminated and the nodeless degrees are condensed out to obtain the ($6{\times}6$) element stiffness matrix. The present study also incorporates the straightforward prediction of interlaminar stresses from equilibrium equations. Several numerical examples confirm the superior behavior of the present composite laminated curved beam element.

• Structural Engineering and Mechanics
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• 제69권4호
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• pp.427-437
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• 2019

In this study, an alternative solution procedure presented by using variational methods for analysis of shear deformable functionally graded material (FGM) beams with mixed formulation. By using the advantages of $G{\hat{a}}teaux$ differential approaches, a refined complex general functional and boundary conditions which comprises seven independent variables such as displacement, rotation, bending moment and higher-order bending moment, shear force and higher-order shear force, is derived for general thick-thin FGM beams via shear deformation beam theories. The mixed-finite element method (FEM) is employed to obtain a beam element which have a 2-nodes and total fourteen degrees-of-freedoms. A computer program is written to execute the analyses for the present study. The numerical results of analyses obtained for different boundary conditions are presented and compared with results available in the literature.

• Journal of Korean Vacuum Science & Technology
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• 제5권2호
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• pp.38-42
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• 2001

We investigated physical properties of ion-beam mixed Fe/si multilayerd films(MLF) prepared by rf sputtering onto glass substrates at room temperature. Such an ion-beam treatment has led to noticeable changes in the structural and physical properties of the MLF: the formation of a new phase which is characterized by a crystalline silicide with a low coercivity and Tc = 550 K. In contrast to the as-prepared state, the ion-beam mixed MLF contains two magnetic phases. One of them is a very soft (Hc < 2 Oe), but microscopically homogeneous one with M$\sub$eff/=6.7 kG.

• Fire Science and Engineering
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• 제23권6호
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• pp.126-134
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• 2009

In an attempt to control the spalling in high strength concrete, spalling reducer was mixed to identify the effect and thermal characteristics of concrete beam member at high temperature. The member was manufactured in such as way of adding 40~60MPa of high strength concrete into spalling reducer, and then fire resistance performance were monitored under the ISO standard fire load condition in accordance with KS F 2257. As a result of test, fore rate performance of 40MPa beam without spalling reducer was 180minutes, 50MPa was 174minutes and 60MPa was 152minutes, indicating that 50MPa and 60MPa beam appeared 6~28minutes short to become a 3-hour rate. However, 50 and 60MPa beam mixed with spalling reducer appeared to have satisfied the requirements for 180minutes. A spalling was occurred in surface of 50 and 60MPa beam mixed without spalling reducer, while no spalling or surface failure was occurred with 50 and 60MPa beam mixed with spalling reducer. Thus polypropylene fiber mixed with the concrete proved to be effective, but viewing that the surface of 60MPa was peeled off partially, the steel fiber mixed appeared not to be effective for the beam more than 60MPa.

• Composites Research
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• 제20권6호
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• pp.15-20
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• 2007

In this work, the structural response of thin-walled, composite beams with built-in twist angles is analyzed using a mixed beam approach. The analytical model includes the effects of elastic couplings, shell wall thickness, and torsion warping. Reissner's semi-complimentary energy functional is used to describe the beam theory and also to deal with the mixed-nature in the beam kinematics. The bending and torsion related warpings introduced by the non-zero pretwist angles are derived in closed-form through the proposed beam formulation. The theory is validated with available literature and detailed finite element analysis results for rectangular solid section beams with elastic couplings. Very good correlation has been obtained for the cases considered.

• Journal of the Korean Society of Safety
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• 제20권4호
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• pp.54-62
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• 2005

This Study is to find out how RC beam mixed with sawdust acts comparing with normal beam without sawdust mixture, and how they can be applied to the actual structural frame, despite a Int that they are mixed with waste material : saying sawdust. ED3H1, ED3H2, ED5H1, ED5H2, ED3H1UB, ED5H1UB, ED3H2L, ED5H2L and Normal without sawdust mixture are main factor to be tested here in order to apply them to the actual case. D and H means diameter 3cm or 5cm, and holes one and two respectively. And all variables are tested with each two for one variables. Test results are compared using crack diagrams and strain & loads. There are eleven(11)% capacity decrease between ED 3H1 and ED5H1 in rebar, strain. Left and right side crack shapes are much similar in variable ED3H2L having maximum capacity 14.5 tone. ED5H2L having maximum capacity thirteen(13)tone, in case of normal 19.6 tone. Two holes in beam rather on the longitudinal direction than on the forcing direction can be more effective to keep the original capacity of the beam because this case can distribute load more uniformly. There is 33% capacity decreased in case of diameter five(5)cm, compared to diameter three(3)cm. Two holes give thirty nine(39) percent capacity decrease than one of diameter three(3)cm.