• Title/Summary/Keyword: microwave emission

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Study of Enhancing Dye Affinity of Fabric using Microwave

  • Kim, Ji-Hyun;Choi, In-Ryu
    • The International Journal of Costume Culture
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    • v.13 no.1
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    • pp.62-66
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    • 2010
  • Of all the ways that energy is consumed within textile industry, few are as high energy-expending as dyeing process. The energy consumption in dyeing process amounts to 77% of total fuel consumption, 54% of total electricity use. A technical development in terms of efficient saving energy and time as well is required in the process of dyeing textiles. Recently, dyeing experts are investigating new technologies can conserve energy grafting into microwaves, radio waves, infrared lights, etc. Dyeing industry in Korea, however, the research related to energy conservation has been rarely conducted. Accordingly, this study aims to examine the possibility where especially microwaves could be applied to reduce the energy use and enhance dyeing process skill. This study performs the experiment in which microwave is employed as heating condition in dyeing and figures out as color yield being promoted, bathochromic effect would be achieved. Applying microwaves in dyeing process is expected to lower the carbon emission, energy and time wasted, ultimately exalt economic efficiency.

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Synthesis of Carbon Nanowalls by Microwave PECVD for Battery Electrode

  • Kim, Sung Yun;Shin, Seung Kwon;Kim, Hyungchul;Jung, Yeun-Ho;Kang, Hyunil;Choi, Won Seok;Kweon, Gi Back
    • Transactions on Electrical and Electronic Materials
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    • v.16 no.4
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    • pp.198-200
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    • 2015
  • The microwave plasma enhanced chemical vapor deposition (PECVD) system was used to grow a carbon nanowall (CNW) on a silicon (Si) substrate with hydrogen (H2) and methane (CH4) gases. To find the growth mechanism of CNW, we increased the growth time of CNW from 5 to 30 min. The vertical and surficial conditions of the grown CNWs according to growth time were characterized by field emission scanning electron microscopy (FE-SEM). Energy dispersive spectroscopy (EDS) measurements showed that the CNWs consisted solely of carbon.

Field emission of diamond films grown on glass substrates at low temperatures

  • Lee, S.W.;Han, I.T.;Lee, N.;Choi, W.B.;Kim, J.M.;Jeon, D.
    • Journal of Korean Vacuum Science & Technology
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    • v.3 no.1
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    • pp.43-48
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    • 1999
  • Using microwave plasma-enhanced chemical vapor deposition, diamond films were successfully grown on Ti-coated glass substrates at temperatures as low as around 500$^{\circ}C$ in behalf of practical applications to field emitters. Electron emission was observed at turn-on fields below 18V-$\mu\textrm{m}$. Field emission characteristics of diamond films were discussed in terms of their crystalline qualities. diamond films with poorer crystalline qualities showed better field emission properties.

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Field Emission Characteristics of Deffctive Diamond Films

  • Koh, Ken-Ha;Park, Kyung-Ho;Lee, Soon-Il
    • Journal of the Korean Vacuum Society
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    • v.7 no.s1
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    • pp.160-166
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    • 1998
  • The field emission characteristics of defective diamond films grown by microwave plasma enhanced chemical vapor deposition (MPECVD) have been studied. X-ray diffraction, the poor crystal quality and/or small grain sizes of the diamond phase and the inclusion of the non-diamond carbon phases in these films have been condirmed by raman spectroscopy, scanning electron microscopy, atomic force microscopy, and the reflectance measurements. The degrees of the film defectiveness and the emission characteristics were dependent on the methane concentration. Current-versus-voltage measurements have demonstrated that the defective diamond films have good electron emission characteristics. characteristics strongly suggests the defect-related electron-emission mechanism. The defective diamond films deposited on Si substrates show the field emission current density of 1$\mu\textrm{A}/\textrm{cm}^2$ and 1mA/$\textrm{cm}^2$ have been measured at electric fields as low as 4.5V/$\mu\textrm{m}$ and 7.6V/$\mu\textrm{m}$, respectively. We also observed the similar emission characteristics from the defective diamond film deposited on Cr/Si substrate and could decrease the deposition temperature to $600^{\circ}C$.

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Simultaneous Determination of Sulfur, Phosphorus, and Zine in Lubricating Oils by Microwave Digestion System and ICP-AES (마이크로파 분해장치와 유도결합 플라스마 원자방출분광법을 이용한 윤활유 시료 중 S, P 및 Zn의 동시 분석)

  • Cho, Sung-Ill;Lim, Heon-Sung;Lee, Sueg-Geun
    • Analytical Science and Technology
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    • v.14 no.4
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    • pp.324-330
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    • 2001
  • For the analysis of S, P and Zn in lubricating oil, microwave digestion method was studied by using inductively coupled plasma-atomic emission spectrometry(ICP-AES). Lubricating oil was completely decomposed with nitric acid or a mixture of nitric acid and hydrogen peroxide using and closed microwave digestion system. Digestions are completed within 50 min, a factor of at least 3~4 times faster than for the conventional digestion. A gradual heating program operated by the pulsed mode was found suitable for decomposing the lubricating oil matrix safely. The proposed method of digestion gave relative standard deviations(RSD) less than 3% for the elements determined.

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SPATIO-SPECTRAL MAXIMUM ENTROPY METHOD: II. SOLAR MICROWAVE IMAGING SPECTROSCOPY

  • Bong, Su-Chan;Lee, Jeong-Woo;Gary Dale E.;Yun Hong-Sik;Chae Jong-Chul
    • Journal of The Korean Astronomical Society
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    • v.38 no.4
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    • pp.445-462
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    • 2005
  • In a companion paper, we have presented so-called Spatio-Spectral Maximum Entropy Method (SSMEM) particularly designed for Fourier-Transform imaging over a wide spectral range. The SSMEM allows simultaneous acquisition of both spectral and spatial information and we consider it most suitable for imaging spectroscopy of solar microwave emission. In this paper, we run the SSMEM for a realistic model of solar microwave radiation and a model array resembling the Owens Valley Solar Array in order to identify and resolve possible issues in the application of the SSMEM to solar microwave imaging spectroscopy. We mainly concern ourselves with issues as to how the frequency dependent noise in the data and frequency-dependent variations of source size and background flux will affect the result of imaging spectroscopy under the SSMEM. We also test the capability of the SSMEM against other conventional techniques, CLEAN and MEM.

Application of the Microwave-assisted Process to the Fast Extraction of Isoflavone from the Waste Residue of the Soybeans

  • Hua, Li;Guoqin, Hu;Dan, Li
    • Bulletin of the Korean Chemical Society
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    • v.30 no.11
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    • pp.2687-2690
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    • 2009
  • Due to the importance of isoflavone content in soybean extracts, the microwave-assisted process (MAP) was compared to the conventional extraction methods. For comparison of the three methods, all extraction parameters (solvent, sample to solvent ratio, temperature, etc.) were kept the same; the microwave extractor was operated at 187.5 W with an emission frequency of 2450 MHz under atmospheric pressure conditions and the extractions were carried out at 75 ${^{\circ}C}$ for 3 min while the conventional reflux was at 75 ${^{\circ}C}$ for 3 h. Total yield and crude isoflavone content were determined by ultraviolet spectrophotometric and compared with the three methods. Results indicated that the MAP was comparable to the conventional method in its capability to extract target compounds without causing any degradation; in addition it dramatically reduced the extraction time from 3 h to a few minutes, suggesting that it can be an alternative technique to the time-consuming conventional reflux method.

A Study on the Carbonization and Strengthening of PAN Fiber by Microwave Plasma (마이크로웨이브 플라즈마를 이용한 탄화공정 및 PAN fiber의 강도 향상에 관한 연구)

  • Choi, Ji-Sung;Joo, Jung-Hoon;Lee, Hun-Su
    • Journal of the Korean institute of surface engineering
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    • v.45 no.2
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    • pp.89-94
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    • 2012
  • A study to replace a high temperature thermal carbonization process with microwave plasma process is carried for PAN fiber as a starting material. Near atmospheric pressure microwave plasma (1 Torr~45 Torr) was used to control to get the fiber temperature up to $1,000^{\circ}C$. Even argon is an inert gas, its plasma state include high internal energy particles; ion (15.76 eV) and metastable (11.52 eV). They are very effective to lower the necessary thermal temperature for carbonization of PAN fiber and the resultant thermal budget. The carbonization process was confirmed by both EDS (energy dispersive spectroscopy) of plasma treated fibers and OES (optical emission spectroscopy) during processing step as a real time monitoring tool. The same trend of decreasing oxygen content was observed in both diagnostic methods.

Characteristics of Microwave Air Plasma With a Wide Range of Operating Pressures (운전압력 변화에 따른 마이크로파 공기 플라즈마의 특성연구)

  • 조정현;장봉철;박봉경;김윤환;정용호;김곤호
    • Journal of the Korean Vacuum Society
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    • v.11 no.1
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    • pp.68-75
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    • 2002
  • It is observed the characteristic of the microwave air plasma in the wide range of the operating pressure, 1 mTorr ~ 760 Torr. The microwave air plasma was generated by an AC-type microwave source manufactured with a magnetron taken from a commertial microwave oven and the input power was fixed at 370 W. Characteristics of the plasmas were observed by an injection Langmuir probe and an OES(Optical Emission Spectroscopy). The breakdown electric field is drastically changed at 500 mTorr. For < 500 mTorr, the ratio of the breakdown electric field and the pressure decreased inversely to the pressure, $5.7\times10^4$V/m-Torr.However, the ratio increased linearly as 43 V/m-Torr for the operating pressure, > 500 mTorr. The minimum breakdown electric field was observed about 12. kV/m at 500 mTorr. It corresponds that the input frequency equals to the collision frequency. The effective collision cross section of the air at this pressure was calculated as $9.23\times10^{-l6}\textrm{cm}^2$.The results of the OES measurement revealed that the main ions were composed of the oxygen, argon, and nitrogen for > 500 mTorr. In contrast, only oxygen and argon ions were dominated for < 500 mTorr. ion temperature of oxygen (O(II)) in the air was decreased from about 1.2 eV to 0.5 eV as the pressure increased. Langmuir probe data shows that the plasma density for < 500 mTorr was higher that for > 500 mTorr.