• Title/Summary/Keyword: microwave discharge

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DECOMPOSITION OF HIGHER ORGANIC COMPOUND IN AN ATMOSPHERIC PRESSURE NON-EQUILIBRIUM PLASMA

  • Kitokawa, Kazutoshi;Itou, Akihito;Sugiyama, Kazuo
    • Journal of the Korean institute of surface engineering
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    • v.29 no.5
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    • pp.593-598
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    • 1996
  • Previously, in trying to prepare perovskite type oxide powders by microwave heating, we found out a non-equilibrium argon plasma is generated around the powders and discharge continues stable at atmospheric pressure. In this study, we tried the plasma decomposition of heat-stable higher organic compound such as palmitic acid which is the principal constituent of the fimger fats. It was proved that suitable amount of coexistence of oxygen radicals into the argon flow accelerates the decomposition of palmitic acid. The argon-oxygen mixed gas plasma was able to perform a complete elimination of higher organic compound.

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A Study on Plasma Display Panel Barrier Rib Fabrication by Mold and Electromagnetic Wave (몰드와 전자기파에 의한 PDP격벽의 성형에 관한 연구)

  • Son, Jae-Hyeok;Im, Yong-Gwan;Jeong, Yeong-Dae;Jeong, Seong-Il;Jeong, Hae-Do
    • Journal of the Korean Society for Precision Engineering
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    • v.19 no.6
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    • pp.176-183
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    • 2002
  • Plasma Display Panel(PDP) is a type of flat panel display utilizing the light emission produced by gas discharge. Barrier Ribs of PDP separating each sub-pixel prevents optical and electrical crosstalks from adjacent sub-pixels. The mold for forming the barrier ribs has been newly researched to overcome the disadvantages of conventional manufacturing processes such as screen printing, sand-blasting and photosensitive glass methods. The mold for PDP barrier ribs have stripes of micro grooves transferring glass-material wall. In this paper , Stripes of grooves of which width 48$\mu$m, depth 124$\mu$m , pitch 274$\mu$m was acquired by machining of single crystal silicon with dicing saw blade. Maximum roughness of the bottom of the grooves was 59.6 nm Ra in grooving Si. Barrier ribs were farmed with silicone rubber mold, which is transferred from grooved Si forming hard mold. Silicone rubber mold has the elasticity, which enable to accommodate the waviness of lower glass plate of PDP. The methods assisted by the microwave and UV was adopted for reducing the forming time of glass paste.

Synthesis of size-controlled ZnO tetrapods sizes using atmospheric microwave plasma system and evaluation of its photocatalytic property (대기압 마이크로웨이브 플라즈마를 이용한 다양한 크기의 ZnO tetrapod 합성 및 광촉매 특성 평가)

  • Heo, Sung-Gyu;Jeong, Goo-Hwan
    • Journal of the Korean institute of surface engineering
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    • v.54 no.6
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    • pp.340-347
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    • 2021
  • Among various metal oxide semiconductors, ZnO has an excellent electrical, optical properties with a wide bandgap of 3.3 eV. It can be applied as a photocatalytic material due to its high absorption rate along with physical and chemical stability to UV light. In addition, it is important to control the morphology of ZnO because the size and shape of the ZnO make difference in physical properties. In this paper, we demonstrate synthesis of size-controlled ZnO tetrapods using an atmospheric pressure plasma system. A micro-sized Zn spherical powder was continuously introduced in the plume of the atmospheric plasma jet ignited with mixture of oxygen and nitrogen. The effect of plasma power and collection sites on ZnO nanostructure was investigated. After the plasma discharge for 10 min, the produced materials deposited inside the 60-cm-long quartz tube were obtained with respect to the distance from the plume. According to the SEM analysis, all the synthesized nanoparticles were found to be ZnO tetrapods ranging from 100 to 600-nm-diameter depending on both applied power and collection site. The photocatalytic efficiency was evaluated by color change of methylene blue solution using UV-Vis spectroscopy. The photocatalytic activity increased with the increase of (101) and (100) plane in ZnO tetrapods, which is caused by enhanced chemical effects of plasma process.

Improvement study of river discharge measurement system using PDA (PDA를 이용한 유량측정시스템 개선방안 연구)

  • Hwang, Eui-Ho;Yang, Jae-Rheen;Lee, Geun-Sang;Koh, Deuk-Koo
    • Proceedings of the Korea Water Resources Association Conference
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    • 2006.05a
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    • pp.942-947
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    • 2006
  • In KOWACO, flow measurement system using PDA has been developed and used since 2004. Even though this system has improved the reliability of the measured flow data, it still has some problems caused by the internet-based data manipulation scheme. We found that this kind of data handling method is not suitable because it causes frequent communication problems especially in fringe areas. To solve this problem, the structure and algorithms of existing system has been analyzed and an improved system is proposed. Besides, improvement study on the rate of change and the uncertainty of the flow data have been performed as well as the communication method between the Microwave Water Surface Current Meter and PDA adopting the state-of-the-art IT technology.

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Fe3O4 Nanoparticles on MWCNTs Backbone for Lithium Ion Batteries

  • Lee, Kangsoo;Shin, Seo Yoon;Yoon, Young Soo
    • Journal of the Korean Ceramic Society
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    • v.53 no.3
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    • pp.376-380
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    • 2016
  • A composite electrode made of iron oxide nanoparticles/multi-wall carbon nanotube (iNPs/M) delivers high specific capacity and cycle durability. At a rate of $200mAg^{-1}$, the electrode shows a high discharge capacity of ${\sim}664mAhg^{-1}$ after 100 cycles, which is ~ 70% of the theoretical capacity of $Fe_3O_4$. Carbon black, carbon nanotube, and graphene as anode materials have been explored to improve the electrical conductivity and cycle stability in Li ion batteries. Herein, iron oxide nanoparticles on acid treated MWCNTs as a conductive platform are combined to enhance the drawbacks of $Fe_3O_4$ such as low electrical conductivity and volume expansion during the alloying/dealloying process. Enhanced performance was achieved due to a synergistic effect between electrically 3D networks of conductive MWCNTs and the high Li ion storage ability of $Fe_3O_4$ nanoparticles (iNPs).

Non-thermal plasma technology for abatement of pollutant emission from marine diesel engine

  • Panomsuwan, Gasidit;Rujiravanit, Ratana;Ueno, Tomonaga;Saito, Nagahiro
    • Journal of Advanced Marine Engineering and Technology
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    • v.40 no.10
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    • pp.929-934
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    • 2016
  • Plasma technology has long been regarded as a key essential tool in many industrial and technological sectors. However, the advancement of plasma technology in marine applications has not been fully realized yet. Herein, we present a short overview on the recent trends in utilization of plasma technology for air-pollution treatment in marine diesel exhaust. Four non-thermal plasma system, including electron beam dry scrubber (EBDS), dielectric barrier discharge (DBD), electron beam-microwave (EB-MW) plasma hybrid system, and plasma-catalytic hybrid system, are described with emphasis on their efficiency in removals of $NO_x$ and $SO_x$ gases. Non-thermal plasma has the great potential to be an efficient and environmentally compatible technique in simultaneous removals of $NO_x$ and $SO_x$ gases from the exhaust of marine diesel engine in the future.

PERMEATION OF PURE AND MIXED GASES THROUGH COMPOSITE MEMBRANES PREPARED BY PLASMA POLYMERLZATION OF FLUOROCARBONS

  • Koo, Ja-Kyoung;Kim, Byoung-Sik
    • Proceedings of the Membrane Society of Korea Conference
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    • 1997.04b
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    • pp.13-16
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    • 1997
  • The permeation, solution and diffusion of simple gases ($He, H_2, O_2, N_2$ and CH$_4$) and condensible vapers($CO_2, SO_2, C_2H_4$ and $C_3H_8$), and the mixed gases ($O_2/N_2$ mixtures and $CO_2/CH_4$ mixtures) through composite membrane was studied. Composit membranes were made by deposition of aromatic fluorocarbons onto polymer substrams of porous Celgard in a microwave discharge. In the both cases of simple gases and condensible vapors, as the kinetic molecular diameter of the permeant molecules increased, the permeability decreased. However, when the kinetic molecular dimemr are similar, the condensible vapors showed higher permeabilities than that of permanent gases. The vapor solubility increased with increasing critical temperature of the vapors. However, in the case of propane, despite its high critical temperature, it showed lower solubility than other vapors. The vapor diffusivity decreased with increasing kinetic diameter of the molecule. Compared to conventional polymers, the plasma polymers showed much lower values for vapor diffusivities. The pressure of the permeant did not affect the permeability. The permeability was also not affected by the composition in cases of mixed gases.

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Preparation of Bucky Paper using Single-walled Carbon Nanotubes Purified through Surface Functionalization and Investigation of Their Field Emission Characteristics (기능화에 의한 단일벽 탄소나노튜브 정제 및 페이퍼 제조와 전계방출 특성 연구)

  • Goak, Jeung-Choon;Lee, Seung-Hwan;Lee, Han-Sung;Lee, Nae-Sung
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.5
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    • pp.402-410
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    • 2008
  • Single-walled carbon nanotubes (SWCNTs) were currently produced together with some contaminants such as a metallic catalyst, amorphous carbon, and graphitic nanoparticles, which should be sometimes purified for their applications. This study aimed to develop efficient, scalable purification processes but less harmful to SWCNTs. We designed three-step purification processes: acidic treatment, surface functionalization and soxhlet extraction, and heat treatment. During the soxhlet extraction using tetrahydrofuran, specifically, carbon impurities could be easily expelled through a glass thimble filter without any significant loss of CNTs. Finally, SWCNTs were left as a bulky paper on the filter through membrane filtration. Vertically aligned SWCNTs on one side of bulky paper were well developed in a speparation from the filter paper, which were formed by being sucked through the filter pores during the pressurized filtration. The bucky paper showed a very high peak current density of field emission up to $200\;mA/cm^2$ and uniform field emission images on phosphor, which seems very promising to be applied to vacuum microelectronics such as microwave power amplifiers and x-ray sources.

Adoption of Wireless Near Field Communication Method in the Discharge Measurements using Microwave Water Surface Current Meter (전자파표면유속계를 이용한 유량측정시 근거리 통신의 적용)

  • Kim, Young-Sung;Yang, Jae-Rheen
    • Proceedings of the Korea Water Resources Association Conference
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    • 2008.05a
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    • pp.1784-1788
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    • 2008
  • 전자파표면유속계는 여러 측정지점을 가능한 신속하게 이동하면서 홍수시 유속을 측정하는데 그 목적이 있다. 또한 홍수시 유속은 시간대 별로 급격히 변하는 속성을 가지고 있으므로 유량측정 지점의 유량을 실시간으로 획득하기 위해서는 현장 측정에서 측정한 유량데이터가 실시간으로 집계 되어야한다. 현재의 시스템은 측정 정보를 실시간으로 전송하기 위하여 현장 측정자에게 PDA가 보급되어 있으며 CDMA망을 통해서 유량 측정을 위한 각종 정보 및 측정결과를 실시간 전송하도록 되어있다. 그러나 전자파표면유속계를 비롯한 각종 유속계가 PDA와 무선으로 통신을 할 수 있게 되어있지 않기 때문에 열악한 여건의 현장에서 측정한 데이터를 야장에 수기로 기록한 후 이를 다시 PDA에 수동으로 입력시켜야하는 불편함이 있다. 전자파표면 유속계를 제외한 다른 측정 장비는 제조회사가 수자원공사와 독립적인 업체이므로 통신 접속을 하기위한 특정 인터페이스를 알아내기가 어려운 실정이다. 그러나 전자파표면유속계는 수자원공사에서 개발한 장비로서 핵심기술을 수자원공사에서 보유하고 있으므로 PDA와 통신을 가능하게 하는 장치의 개발이 가능하다. 이에 이러한 불편한 문제점을 개선하여 현장에서 홍수 유량 측정시 작업자들의 편이성을 증대시키고자 전자파표면유속계와 PDA간에 근거리통신기법을 적용하였다. 이를 위하여 Bluetooth, UWB(Ultra-Wide Band, 초광대역통신), Zigbee 등 적용가능한 근거리 통신기법을 조사하였다. 그 결과 Zigbee가 소비전력이 적어 현장에서 홍수유량측정에 이용되는 전자파표면유속계에 적용성이 가장 뛰어난 것으로 나타났다. 무선통신 모듈과 연동되는 전자파표면유속계는 이동식을 기준으로 적용하였으며 기존 신호처리부에 무선통신 모듈을 장착할 수 있는 구조로 설계하였다. 장착 방식은 기존 이동식 유속계의 신호처리부의 RS-232 포트에 무선통신 모듈을 장착하면 사용할 수 있는 구조로 되어있다. 신호처리부 RS-232 포트는 현재까지는 측정한 유속값을 PC로 전송받는 용도로 활용되었으나 무선모듈 장착 시에는 무선통신 할 수 있는 이중화 구조를 채택하였다. 두 가지 방식에 대한 통신구별은 초기에 송수신하는 데이터에 따라 구별되도록 하였다. 신호처리부에서 무선통신 추가에 따른 운용 방식은 별도의 수자원공사 모드를 추가하여 운용하도록 수정하였다. 유속 측정 시에는 무선통신 모듈을 제거한 상태에서 측정한 후, 측정한 데이터를 PDA로 전송할 때 아를 부착하여 사용할 수 있는 구조를 갖도록 제작하였다. 이러한 방식을 적용시킨 이유는 기존에 보급된 유속계에 무선모듈을 장착한 후, 신호처리부 운용 프로그램을 업그레이드하면 바로 사용할 수 있도록 하기 위함이다.

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Effect of defects on lifetime of silicon electrodes and rings in plasma etcher (플라즈마 에쳐용 실리콘 전극과 링의 수명에 미치는 결함의 영향)

  • Eum, Jung-Hyun;Chae, Jung-Min;Pee, Jae-Hwan;Lee, Sung-Min;Choi, Kyoon;Kim, Sang-Jin;Hong, Tae-Sik;Hwang, Choong-Ho;Ahn, Hak-Joon
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.20 no.2
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    • pp.101-105
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    • 2010
  • Silicon electrode and ring in a plasma etcher those are in contact with harsh plasma suffer from periodic heating and cooling during their lifetime. This causes the silicon components failure due to thermal stress remaining the persistent slip bands (PSBs) on their surfaces. The factors that determine the lifetime of silicon electrode and ring were discussed with respect to silicon ingot. The impurity level and the average defect concentration measured with glow discharge mass spectrometer (GDMS) and microwave photo-conductance decay (${\mu}$-PCD) were compared with the grade of silicon ingots those are divided to slip-free and slip-allowed ingot. Some silp-allowed samples showed planar defects along <110> direction on {001} surface. The role of these defects was suggested from the viewpoint of the lifetime of silicon components.