• 한국분말재료학회지
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• 제11권6호
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• pp.472-476
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• 2004

The Fe-Ni compact bodies were fabricated using Fe-Ni mixed powders with 50 nm in diameter by injection molding process. The relationship between microstructure and material properties was characterized with respect to the volume ratio of powder/binder and sintering temperature with SEM and TEM. In the compact body having the volume percent ratio of 45(Fe-Ni) : 55(binder), which was sintered at $900^{\circ}C$ the values of relative density and hardness were low about 97.7% and 277.1 Hv, respectively. Using the composition of 50(Fe Ni) : 50(binder) and sintered at $900^{\circ}C$, the values of relative density and hardness were 98.5%, 294.4 Hv, respec-tively. The grain size of sintered bodies strongly depended on the sintering temperature. In both samples sintered at $600^{\circ}C$ and $900^{\circ}C$, the average grain sizes were about 150 nm and 500 nm in diameter, respectively.

• 열처리공학회지
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• 제23권1호
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• pp.10-16
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• 2010

The microstructure of Cu-Mg-P alloy sheet consisted of Cu matrix and very fine MgP precipitate, and it has been observed that the microstructure remains virtually unchanged by Ag additions up to 2%. Ag solutes were dissolved into the matrix and hardly found in the precipitates. The hardness increased with increase of the Ag content, while the conductivity slightly decreased. Strain hardening through cold rolling was found to be effective in improving the hardness, especially in high-Ag alloys. Aging treatment was conducted either before the first cold rolling or between the first and the final cold rolling, and the conductivity was significantly higher at the former case, regardless of the Ag content. Softening of Cu-Mg-P alloy sheet was remarkable above $400^{\circ}C$ and the Ag content did not show any significant effect on it.

• 한국안광학회지
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• 제12권2호
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• pp.19-23
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• 2007

안경렌즈 절삭용 탄화규소재료의 미세구조와 기계적 특성을 CaO를 첨가해서 연구하였다. 조성이 다른 4종류의 시편을 $1,880^{\circ}C$에서 4시간 일축가압소결 하였다. 주사전자현미경으로 미세구조를 분석하였고, X-ray를 통해 상분석을 하였다. 본 실험에서 연구된 안경렌즈 절삭공구의 대표적인 파괴인성은 $5.4MPa{\cdot}m^{1/2}$을 나타내었다. 또한, 경도값은 밀도값에 비례적인 경향성을 보여주었다.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2002년도 Proceedings of the International Welding/Joining Conference-Korea
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• pp.522-527
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• 2002

The microstructure and mechanical properties of friction stir welded OFC plates with 2mm in thickness were examined with the changing welding parameters such as welding speed, rotation speed in this study. The sounding welding conditions was acquired at the optimum welding conditions of the 41mm/min to 61mm/min of welding speed at 1250 rpm of rotation speed. The microstructure of weld zone was divided into four parts such as the base metal region (EM), thermal mechanical affected zone (TMAZ), heat affected zone (HAZ), stir zone (SZ). The grain size in the SZ and the width of weld nugget were increased with increasing welding speed. The hardness profiles of the base metal were distributed about 80HV. The HAZ is a slightly softened region of about 60~75 HV relative to the base metal. The hardness profiles of the SZ were higher than that of base metal. The tensile strength was increased with increasing welding speed. In case increasing rotation speed, tensile strength was decreased. The maximum tensile strength was about 220:MPa which was 110% of joint efficience of that of base metal at 41mm/min of welding speed, 1250rpm of rotation speed.

• 한국세라믹학회지
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• 제34권5호
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• pp.519-527
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• 1997

The effect of Al content and heating rate on the sintering behavior, microstructure, and mechanical properties of reaction bonded alumina (RBAO) was investigated. As the heating rate became slower a critical Al content which could be added to RBAO increased. The weight gain and linear shrinkage of RBAO containing of 55 vol% Al were 28% and 6.5%, respectively. The relative density of RBAO decreased from 96 to 94%, as the amount of Al increased from 15 to 55 vol%. The hardness of RBAO increased from 17.8 to 19.9 GPa and the bending strength enhanced from 370 to 570 MPa, as the amount of Al increased from 15 to 55 vol%. On the other hand, the wear rate of RBAO degraded from 6.7 to 3.39$\times$10-5 $\textrm{mm}^2$/kg and the fracture toughness decreased from 4.1 to 3.6 MPa.m1/2, as the amount of Al increased from 15 to 55 vol%. Fracture modes were shown to the mixed mode of inter/transgranular. However, transgranular fracture was dominant with increasing the content of Al.

• 대한기계학회논문집A
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• 제24권8호
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• pp.1910-1916
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• 2000

The five classes of the thermally aged CF8M specimen are prepared using an artificially accelerated aging method. Namely, after the specimens are held for 100, 300, 900, 1800, and 3600hrs at 430$^{\circ}C$ respectively, the specimens are water-cooled to room temperature. The impact energy variations are measures for both the aged and virgin specimens through the Charpy impact tests in addition to the microstructure observation, tensile, hardness and fatigue crack growth tests. From the present investigation the following results are obtained : 1) The difference among the thermally degraded specimens can be distinguished through their microstructures, 2) Hardness and tensile strength are increased to 300hrs, degradation specimen, while elongation and reduction area are decreased to 3600hrs degradation specimen, and impact energy is decreased to 1800hrs degradation specimen, 3) The FCG rates for thermally degraded specimens are larger than that of the virgin specimen.

• 한국공작기계학회논문집
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• 제15권4호
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• pp.49-55
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• 2006

This study deals with the friction welding of SM25C and SCNCrM-2B; The friction time was variable conditions under the conditions of spindle revolution 2,000rpm, friction pressure of 100MPa, upset pressure of l50MPa, and upset time of 4.0 seconds. Under these conditions, the microstructure of weld interface, tensile fracture surface and mechanical tests were studied, and so the results were as follows. 1. When the friction time is 2.0 seconds, the tensile strength of friction welds was 874MPa, which is around as much as 117% of the tensile strength of base metal(SM25C), the bending strength of friction welds was 1,354MPa, which is around as much as 108.9% of the bending strength of base metal(SM25C). 2. At the same condition, the maximum vickers hardness was Hv443 at SCNCrM-2B nearby weld interface, which is higher Hv20 than condition of the friction time 0.5 seconds. 3. The results of microstructure analysis show that the structures of two base materials have fractionated and rearranged along a column due to heating and axial force during friction, which has affected in raising hardness and tensile strength.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2010년도 춘계학술발표대회 초록집
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• pp.19-19
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• 2010

Mo 변화에 따른 Cr-Mo 강의 미세조직 및 물성병화를 알아보기 위해 새로 디자인된 용접봉을 사용하여 Flux cored arc welding(FCAW) 공정으로 용접하였다. 또한 고온에서의 용접부 물성을 알아보기 위하여 각각의 시편을 $400^{\circ}C$, $500^{\circ}C$, $600^{\circ}C$, $700^{\circ}C$에서 24시간 동안 열처리 하였다. 용접부의 미세조직은 미세한 베이나이트 및 침상 페라이트로 구성되었으며 Mo의 함량이 높아질수록 베이나이트 조직이 증가하여 경도 및 강도가 증가하였다. 높은 항복강도와 인장강도를 가지며 연신율이 매우 낮음을 관찰하였다. 열처리후의 미세조직은 $400^{\circ}C$, $500^{\circ}C$는 템퍼드 베이나이트 조직이 나왔으나 $600^{\circ}C$에서 베이나이트 조직이 성장하였다. $700^{\circ}C$ 로 갈수록 베이나이트가 감소하고 페라이트로 미세조직이 변태 하였으며 탄화물의 석출 및 성장이 관찰되었다. 이로 인하여 경도값이 $400^{\circ}C$, $;500^{\circ}C$ 에서 증가하였고 $600^{\circ}C$는 소폭 감소하였으며 $700^{\circ}C$의 경우 완전 페라이트 조직의 형성으로 경도가 크게 감소하고 Mo 함량에 따른 경도 차이 또한 보이지 않았다.

• Journal of Welding and Joining
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• 제32권3호
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• pp.102-107
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• 2014

Boiler equipment in power plant is always being operated in harsh conditions and severely exposed to the extreme environment of high temperature. Therefore periodically the state of devices should be checked, diagnosed, and analyzed to ensure the reliability of the equipment. Traditionally, such a diagnosis is based one or two physical properties of the sample taken from the equipment like hardness, microstructure, etc.. However, to enhance the confidence of the diagnosis, it is necessary to synthesize those properties together. This paper is to propose such a synthetic procedure for SA213-T12(1Cr-0.5Mo) which was developed to be used in $565^{\circ}C$ below condition. Creep test and accelerated degradation test were performed simultaneously, and the physical properties such as microstructure, tensile strength, yield strength, hardness, and indentation properties were measured. This paper proposes a method of determining the remaining life by quantitative comparison. It will provide the basis of evaluating life assessment more objective and reliable.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2001년도 춘계학술대회논문집A
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• pp.250-255
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• 2001

It is inevitable to evaluate the life of turbine rotor because the operating periods of power plants need to be extended. The magnetic methods utilizing Magnetic Barkhausen noise curve were applied to detect the degradation caused by thermal aging. The Magnetic property of material depends on the domain dynamics and it is affected by the microstructure of material. Therefore the magnetic property is very sensitive to the microstructure change of the material. It is, thus, very useful to detect the state of degradation of varying materials. The test specimen made of 1Cr-1Mo-0.25V steel was used widely for turbine rotor material, and seven kinds of specimens with different degradation levels were prepared by the isothermal heat treatment at $630^{\circ}C$. With the increase of degradation, BHN was decreased. The result was compared with coercive force and vickers hardness.