• 제목/요약/키워드: microstructural development

검색결과 214건 처리시간 0.029초

Mechanical and microstructural investigations on cement-treated expansive organic subgrade soil

  • Nazerke Sagidullina;Jong Kim;Alfrendo Satyanaga;Taeseo Ku;Sung-Woo Moon
    • Geomechanics and Engineering
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    • 제38권4호
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    • pp.353-366
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    • 2024
  • Organic soils pose significant challenges in geotechnical engineering due to their high compressibility and low stability, which can result in issues like differential settlement, rutting, and pavement deformation. This study explores effective methods for stabilizing organic soils. Rather than conventional ordinary Portland cement (OPC), the focus is on using environmentally friendly calcium sulfoaluminate (CSA) cement, known for its rapid setting, high early strength development, and environmental benefits. Mechanical behavior is analyzed through 1-D free swell, unconfined compressive strength (UCS), and bender element (BE) tests. Microstructural analyses, including Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM), characterize the soil mixed with CSA cement. Experimental results demonstrate improved soil properties with increasing cement dosage and curing periods. A notable strength increase is observed in soil samples with 15% cement content, with UCS doubling after 7 days. This trend aligns with shear wave velocity results from the BE test. SEM and FTIR spectroscopy reveal how CSA cement hydration forms hydrated calcium silicate gel and ettringite, enhancing soil properties. CSA cement is recommended for reinforcing organic subgrade soil due to its eco-friendly nature and rapid strength gain, contributing to improved durability.

A study on the improvement of thickness accuracy in a plate mill

  • Lee, Duk-Man
    • 제어로봇시스템학회:학술대회논문집
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    • 제어로봇시스템학회 2003년도 ICCAS
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    • pp.723-727
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    • 2003
  • In this paper, two methods are discussed for good rolling force prediction in a plate mill. One is about the development of a long and a short learning scheme using a Neural Network for normal rolling and the other is about a mathematical model improvement by considering microstructural changes for controlled rolling. The research results are implemented in a on-line system of Pohang Works in POSCO and the field tests have showed that the prediction accuracies of rolling force are highly improved.

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플라이애시를 함유한 고강도 콘크리트의 조기 강도와 속도 발현 특성 (Characteristics of Early Strength and Velocity Development in High Strength Concrete Containing Fly Ash)

  • 이회근;윤태섭;이광명
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2001년도 봄 학술발표회 논문집
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    • pp.43-48
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    • 2001
  • The use of fly ash in cement and concrete industries has many benefits including engineering, economic, and ecological aspects. However, it has a disadvantage of low strength development, especially at early ages. In this study, in order to overcome this problem, the early strength accelerating agent($NA_{2}$ $SO_{4}$) was selected and applied to the production of high strength concrete(HSC) containing fly ash. It was found that the compressive strength of fly ash concrete incorporating TEX>$NA_{2}$ $SO_{4}$ has greater than that of concrete containing fly ash only until 7 days after casting. From the microstructural point of view, ettringite increased and pores decreased in fly ash concrete incorporating TEX>$NA_{2}$ $SO_{4}$ , leading to the development of early age strength. It was also found that the velocity vs. strength relationship of HSC is considerably different from that of low-strength concrete(LSC). Therefore, in order to predict early age strength of HSC, a estimation equation different from that for LSC is needed.

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석출강화형 Ni 기 초내열합금의 천이액상확산접합 (Transient Liquid Phase Bonding of Gamma Prime Precipitation Strengthened Ni Based Superalloy)

  • 김정길;박해지;심덕남
    • Journal of Welding and Joining
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    • 제35권3호
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    • pp.52-61
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    • 2017
  • Transient liquid phase (TLP) bonding is essential technology to repair micro-cracking on the airfoil of blades and vanes for gas turbines. Understanding of the characteristics of TLP bonding of the superalloys is necessary in the application of the technology for repairing these components. In this study, the focus was on investigating TLP bonding characteristics of ${\gamma}^{\prime}$ precipitation strengthened Ni based superalloy. TLP bonding was carried out with an amorphous filler metal in various bonding conditions, and the microstructural characterization was investigated through optical microscopy (OM) and electron probe micro-analysis (EPMA). The experimantal results explained clearly that bonding temperatures had critical effects on the TLP bonding behaviors, and that isothermal solidication of the joints made at higher temperatures than $1170^{\circ}C$ was controlled by Ti diffusion instead of B.

합성 수산화아파타이트의 미세구조 발달 (Microstructural Development in Synthetic Hydroxyapatite)

  • Kim, Jong-Hee;Park, Young-Min;Yang, Tae-Young;Yoon, Seog-Young;Park, Hong-Chae
    • 한국세라믹학회지
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    • 제41권4호
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    • pp.289-296
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    • 2004
  • 양론조성에 근접하는 (Ca/P=1.62-1.67, molar ratio) 휘스커 및 짧은 막대형상의 수산화아파타이트 (Ca$_{10}$(PO$_4$)$_{6}$(OH)$_2$$\alpha$-Ca$_3$(PO$_4$)$_2$($\alpha$-TCP) 수용액 (pH 11)의 가수분해와 수열반응으로 각각 합성하였다. 생성된 HAp의 입자형상은 합성방법에, 미세구조의 발달은 반응조건에 주로 의존하였다 가수분해의 경우 반응시간의 경과와 더불어 휘스커 입자들의 상호 교차와 장축방향에서의 응집이 일어났다 반면에, 수열처리에 있어서는 반응과정 중 임계크기(길이 0.75$mu extrm{m}$, 지름 0.3$\mu\textrm{m}$) 이상으로의 입성장은 일어나지 않았으며 과다한 반응시간(20$0^{\circ}C$, $\geq$3시간)은 입자들의 심한 응집을 유발하였다.

CD 침탄 및 Subzero 처리가 STS 304 스테인리스강의 미세조직에 미치는 영향 (Microstructural Changes of STS304 Steel during the Carbide Dispersion (CD) Carburization and Subzero Treatment)

  • 공정현;이해정;성장현;김상권;김성완
    • 열처리공학회지
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    • 제20권2호
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    • pp.65-71
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    • 2007
  • Microstructural changes and hardness variations in STS 304 steel have been investigated during the processes of carbide dispersion (CD) carburization; carburization, austenitization, subzero treatment and tempering. The carbon content of the surface layer increased up to maximum 4.0% after carburization, and the content was homogenized with the value of 2.3% to the $95{\mu}m$ from the surface after austenitization. The carbide appeared during CD carburization process was $Cr_7C_3$ type, which was composed network carbides along the austenite grain boundaries, square type carbides in the interior of the grain and fine nano-sized carbides. The fine nano-sized carbides precipitated at the austenitization stage and possibly subzero treatment stage were coarsened after tempering at $200^{\circ}C$, resulting the hardness decrease. The tempered steel without subzero treatment increased hardness with increasing time due to the continuous precipitation of fine carbides during tempering. The nano-sized carbide appeared square type morphology.

Al-B-C 조제 β-SiC의 스파크 플라즈마 소결에 미치는 α-SiC seed 첨가 영향: 미세 구조 변화 (Influence of α-SiC Seed Addition on Spark Plasma Sintering of β-SiC with Al-B-C: Microstructural Development)

  • 조경식;이현권;이상우
    • 한국분말재료학회지
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    • 제17권1호
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    • pp.13-22
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    • 2010
  • The unique features of spark plasma sintering process are the possibilities of a very fast heating rate and a short holding time to obtain fully dense materials. $\beta$-SiC powder with 0, 2, 6, 10 wt% of $\alpha$-SiC particles (seeds) and 4 wt% of Al-B-C (sintering aids) were spark plasma sintered at $1700-1850^{\circ}C$ for 10 min. The heating rate, applied pressure and sintering atmosphere were kept at $100^{\circ}C/min$, 40 MPa and a flowing Ar gas (500 CC/min). Microstructural development of SiC as function of seed content and temperature during spark plasma sintering was investigated quantitatively and statistically using image analysis. Quantitative image analyses on the sintered SiC ceramics were conducted on the grain size, aspect ratio and grain size distribution of SiC. The microstructure of SiC sintered up to $1700^{\circ}C$ consisted of equiaxed grains. In contrast, the growth of large elongated SiC grains in small matrix grains was shown in sintered bodies at $1750^{\circ}C$ and the plate-like grains interlocking microstructure had been developed by increasing sintering temperature. The introduction of $\alpha$-SiC seeds into $\beta$-SiC accelerated the grain growth of elongated grains during sintering, resulting in the plate-like grains interlocking microstructure. In the $\alpha$-SiC seeds added in $\beta$-SiC, the rate of grain growth decreased with $\alpha$-SiC seed content, however, bulk density and aspect ratio of grains in sintered body increased.

마이크로 PIM용 Fe 마이크로-나노 복합분말 피드스톡 제조시 혼합거동과 미세구조 변화 (Mixing Behavior and Microstructural Development During Fabrication of Fe Micro-nano-powder Feedstock for Micro-PIM)

  • 유우경;이재성;고세현;이원식
    • 대한금속재료학회지
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    • 제48권7호
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    • pp.630-638
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    • 2010
  • The present investigation has been performed on the mixing behavior and microstructural development during fabrication of Fe micro-nano powder feedstock for a micro-powder injection molding process. The mixing experiment using a screw type blender system was conducted to measure the variations of torque and temperature during mixing of Fe powder-binder feedstock with progressive powder loading for various nano-powder compositions up to 25%. It was found that the torque and the temperature required in the mixing of feedstock increased proportionally with increasing cumulative powder loading. Such an increment was larger in the feedstock containing higher content of nano-powder at the same powder loading condition. However, the maximum value was obtained at the nano-powder composition of not 25% but 10%. It was owing to the 'roller bearing effect' of agglomerate type nano-powder acting as lubricant during mixing, consequently leading to the rearrangement of micro-nano powder in the feedstock. It is concluded that the improvement of packing density by rearrangement of nano-powders into interstices of micro-powders is responsible for the maximum powder loading of about 71 vol.% in the nano-powder composition of 25%.

변형지도 모델링을 통한 몰리브데늄의 고온 변형에 따른 미세조직 변화 연구 (Microstructural Evolution during Hot Deformation of Molybdenum using Processing Map Approach)

  • 김영무;이성호;이성;노준웅
    • 한국분말재료학회지
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    • 제15권6호
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    • pp.458-465
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    • 2008
  • The hot deformation characteristics of pure molybdenum was investigated in the temperature range of $600{\sim}1200^{\circ}C$ and strain rate range of $0.01{\sim}10.0/s$ using a Gleeble test machine. The power dissipation map for hot working was developed on the basis of the Dynamic Materials Model. According to the map, dynamic recrystallization (DRX) occurs in the temperature range of $1000{\sim}1100^{\circ}C$ and the strain rate range of $0.01{\sim}10.0/s$, which are the optimum conditions for hot working of this material. The average grain size after DRX is $5{\mu}m$. The material undergoes flow instabilities at temperatures of $900{\sim}1200^{\circ}C$ and the strain rates of $0.01{\sim}10.0/s$, as calculated by the continuum instability criterion.

W-Cu와 Cu의 고속 충돌에 의한 연강의 미세조직 변화 (A Study on the Microstryctural Evoulution of the Reagion Aheas of Craters Created by Copper and W-Cu Shaped Charge Jets)

  • 이성;홍문희;백운형
    • 한국분말재료학회지
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    • 제6권1호
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    • pp.69-74
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    • 1999
  • The microstructure of the reagion of carters, created by Cu and W-Cu shaped charge jets, in a 1020 mild steel target has been intestiaged. The region ahead of the crater created by the Cu shaped charge jet, reveals dramatic grain refinement implying the occurrence of a dynamic recrystallization, while that of W-Cu one dose a martensitic transformation indicative of heating up to an austenitic region followed by rapid cooling.The impacting pressure calculated when the W-Cu shaped charge jet encounters the target is higher than that of the Cu one. The micro-hardness of the region ahead of the crater created by the W-Cu shaped charge jet is also higher than that of the Cu one. The microstructure of W-Cu slug remained in the inside of the craters depicts the occurrence of the remarkable elongation of W particles during the liner collaphse. From these results, the microstructural variation of the region ahead of the crater with Cu and W-Cu shaped charge jets is discussed in trems of the pressure dependency of the transformation region of ferrite and austenite phases.

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