• 제목/요약/키워드: microstructural

검색결과 2,163건 처리시간 0.031초

서모트로픽 액정폴리머와 폴리아미드6으로 성형된 얇은 복합재료의 미세구조형태 (Microstructural Morphology of Molded Thin Composites of Thermotropic Liquid Crystalline Polymer and Polyamide 6)

  • 최낙삼;최기영;하성규
    • 대한기계학회논문집A
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    • 제24권7호
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    • pp.1703-1711
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    • 2000
  • Microstructural morphology of molded composites of thermotropic liquid crystalline polymer(LCP) and polyamide 6 (PA6) has been studied as a function of epoxy fraction. Injection-moulding of a thin composite plaque at a temperature below the melting point of the LCP fibrils by suing the extruded LCP/PA6 pellets produced multi-layered structures: 1) the surface skin layer with thickness of 65-120 ym exhibiting a transverse orientation, 2) the sub-skin layer with an orientation perpendicular to the surface skin, i.e. in the flow direction, 3) the core layer with arc-curved flow patterns. Similar microstructural orientations were observed in the respective layers for the composite plaques with different fractions of epoxy.

$MnO_2$ 첨가에 따른 (Pb)(La,Ce)$TiO_3$ 세라믹스의 미세구조특성 (Microstructural Properties of (Pb)(La,Ce)$TiO_3$ ceramics as a function of $MnO_2$ addition)

  • 오동언;민석규;윤광희;류주현;박창엽
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 추계학술대회 논문집 Vol.14 No.1
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    • pp.442-445
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    • 2001
  • In this study, microstructural and dielectric properties of $Pb_{0.83}(La_{0.2}Ce_{0.8})_{0.08}TiO_3$(PCT) ceramics as a function of $MnO_2$ addition were investigated for 30MHz ceramic resonator application. Grain size was gradually increased according to the increase of $MnO_2$ addition amount and showed the highest value of $1.502{\mu}m$ at the 0.9wt% $MnO_2$. Moreover, density showed the highest value of $7.582 g/cm^3$ at the 0.7wt% $MnO_2$.All the composition ceramics,curie temperature was nearly constant around $330^{\circ}C$

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초미립 복합분말로 제조된 W-Cu재료의 전기접점 특성 (Electrical Contact Property of W-Cu Materials Manufactured from Nanocomposite Powder)

  • 김태형
    • 한국분말재료학회지
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    • 제1권2호
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    • pp.174-180
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    • 1994
  • Electrical contact property of the W-20wt%Cu contact materials manufactured by liquid phase sintering of nanocomposite W-Cu powders was investigated and discussed in terms of microstructural development during performance test. Nanocomposite powders were prepared by hydrogen reduction of ball milled W-Cu oxide mixture. They underwent complete densification and microstructural homogenization during liquid phase sintering. As a consequence, the W-Cu contacts produced from nanocomposite powders showed superior contact property of lower arc erosion and stable contact resistance. This might be mostly due to the fact that the arc erosion by evaporation of Cu liquid droplets and surface cracking remarkably became weakened. It is concluded that the improvement of anti-arc erosion of the composite specimen is basically attributed to microstructural homogeneity.

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Alloy 718의 잉고트 파쇄공정시 재결정거동에 대한 해석 (Assessment of Recrystallization Behavior in Ingot-Breakdown Process of Alloy 718)

  • 염종택;이종수;김정한;김남용;박노광
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2007년도 추계학술대회 논문집
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    • pp.42-45
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    • 2007
  • Recrystallization behavior during ingot-breakdown process of Alloy 718 was investigated with finite element analysis and experimental approaches. In order to analyze microstructural changes during the cogging process of an Alloy 718 ingot, the side-pressing and heat treatment tests were performed at different temperatures and ram speed. From the side-pressing and heat treatment test results, it was found that microstructural changes during hot forging of Alloy 718 ingot greatly influenced on a close interaction between dynamic and static-recrystallization behaviors. A recrystallization model of Alloy 718 was used to predict the complex microstructural variation during continuous heating and forging processes of the cogging, and the predicted grain size and its distribution were compared with the actual cogged Alloy 718 billet.

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산화물 분산강화 동합금의 열처리에 따른 미세조직 및 기계적 특성 변화 (Effect of Annealing on Microstructural and Mechanical Property Variation of the Oxide-Dispersion-Strengthened Cu alloy)

  • 김용석
    • 한국분말재료학회지
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    • 제13권1호
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    • pp.25-32
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    • 2006
  • The alumina dispersion-strengthened (DS) C15715 Cu alloy fabricated by a powder metallurgy route was annealed at temperatures ranging from $800^{\circ}C\;to\;1000^{\circ}C$ in the air and in vacuum. The effect of the annealing on microstructural stability and room-temperature mechanical properties of the alloy was investigated. The microstructure of the cold rolled OS alloy remained stable until the annealing at $900^{\circ}C$ in the air and in vacuum. No recrystallization of original grains occurred, but the dislocation density decreased and newly formed subgrains were observed. The alloy annealed at $1000^{\circ}C$ in the air experienced recrystallization and grain growth took place, however annealing in vacuum at $1000^{\circ}C$ did not cause the microstructural change. The mechanical property of the alloy was changed slightly with the annealing if the microstructure remained stable. However, the strength of the specimen that was recrystallized decreased drastically.

Multiple Scale Processes in Microstructural Evolution: Case Study of Self-Reinforced β-Si3N4

  • Becher, Paul F.
    • 한국세라믹학회지
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    • 제53권6호
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    • pp.575-580
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    • 2016
  • Microstructural design of ceramics has generally focused on information gathered at the micro- and macro-scales and related this to how specific properties could be improved. Ceramic processing serves as the key to optimizes the final microstructure. However, the advent of nano-scale microstructures and highly advanced characterization tools are forcing us to develop new knowledge of what is occurring not just at the micro-scale but also at the atomic level. Thus we are now beginning to be able to address how microstructure is influenced by events at the atomic scale using atomic scale images and data. Theoreticians have joined us in interpreting the mechanisms involved in the "microstructural" evolution at multiple scales and how this can be used to enhance specific properties of ceramics. The focus here is on delving into the various layers the "microstructure" in order understand how atomic-scale events influence the structure and properties of ceramics.

$MnO_2$첨가에 따른 (Pb)(La,Ce)$TiO_3$세라믹스의 미세구조특성 (Microstructural Properties of (Pb)(LaCe)$TiO_3$ ceramics as a function of $MnO_2$ addition)

  • 오동언;민석규;윤광희;류주현;박창엽
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 추계학술대회 논문집
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    • pp.442-445
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    • 2001
  • In this study, microstructural and dielectric properties of P $b_{0.83}$(L $a_{0.2}$C $e_{0.8}$)$_{0.08}$Ti $O_3$PCT ceramics as a function of Mn $O_2$ addition were investigated for 30MHz ceramic resonator application. Grain size was gradually increased according to the increase of Mn $O_2$ addition amount and showed the highest value of 1.502${\mu}{\textrm}{m}$ at the 0.9wt% Mn $O_2$. Moreover, density showed the highest value of 7.582 g/$\textrm{cm}^2$ at the 0.7wt% Mn $O_2$. All the composition ceramics, curie temperature was nearly constant around 33$0^{\circ}C$.EX>.>.>.

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반용융 압출을 위한 AA7075 합금의 조직제어 (Microstructural Control of AA7075 Alloy for Thixoextrusion)

  • 윤영옥;김영직;김세광;조형호
    • 한국주조공학회지
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    • 제25권6호
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    • pp.249-253
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    • 2005
  • The present study focuses on 7075 aluminum wrought alloy to investigate the potential industrial applications of thixoextrusion process. The microstructural evolution of 7075 aluminum wrought alloy for thixoextrusion has been investigated as a function of isothermal holding temperature and time in the partially remelted semisolid state. The results showed that the liquid fraction increased with increasing isothermal holding temperature and time while the average grain size was inversely proportional to isothermal holding temperature and time up to 5min. However, there was no big change of liquid fraction and average grain size with respect to isothermal holding temperature and time. The important fact that the liquid fraction and average grain size were almost uniform after 5 min holding time is considered very useful for thixoextrusion in terms of process control.

MICROSTRUCTURAL AND MECHANICAL CHARACTERISTICS OF NON-EQUIATOMIC HIGH ENTROPY ALLOY FeMnCoCr PREPARED BY SPARK PLASMA SINTERING

  • NAMHYUK SEO;JUNHYUB JEON;SEUNGGYU CHOI;YOUNG HOON MOON;IN-JIN SHON;SEOK-JAE LEE
    • Archives of Metallurgy and Materials
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    • 제65권3호
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    • pp.1005-1009
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    • 2020
  • In this study, a non-equiatomic high entropy alloy was fabricated using the spark plasma sintering method, and its microstructural features and mechanical properties were investigated. The chemical composition of FeMnCoCr was determined by using the entropy calculation related to the design of high entropy alloys. A bulk sample with the same composition was also prepared using the conventional metallurgical processes of casting and hot rolling. The microstructures of the samples fabricated by these different processes were compared by microscope observation, and a quantitative phase analysis was carried out using FE-SEM. Hardness measurement was used to evaluate mechanical properties. Particular attention was paid to microstructural changes due to heat treatment, which was analyzed by considering how austenite stability is affected by grain refinement.

레이저 조사시킨 GeSbTe 금속간 화합물의 미세조직 (Microstructural features of Laser Radiated GeSbTe Intermetallic Compounds)

  • 박정우;김명룡
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1995년도 춘계학술대회 논문집
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    • pp.66-72
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    • 1995
  • Microstructural features of laser irradiated bulk target which consists of GeSbTe interrmertallic compounds were examined by analytical microscopy. It was found that in addition to vaporization, a liquid expulsion due to laer-material interatction is main contribution of materials removal in the sintered GaSbTe targets, The morphological change is qualitatively discussed in the present article.

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