• The Journal of Korean Academy of Prosthodontics
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• v.46 no.6
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• pp.577-585
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• 2008

STATEMENT OF PROBLEM: The discoloration of anterior teeth restoration is one of the material problems demanding retreatment. OBJECTIVES: To evaluate the color stability and affecting factors on esthetic restorative materials when subjected to accelerated aging. MATERIAL AND METHODS: This study was conducted using porcelain disks (IPS Empress 2-glazed, IPS Empress 2-polished), direct restorative resin disks (SYNERGY Duo) and indirect restorative resin disks (Sinfony, TESCERA ATL). Accelerated aging was done by precipitating the specimens in 38.C distilled water and irradiating with xenon light, and the total irradiation was 397.98 KJ/mm. Color and microhardness change of the specimens were measured before accelerated aging and after 100 hours, 200 hours and 300 hours of accelerated aging, and Surface of the specimens were examined with SEM before and after 300 hours of accelerated aging. RESULTS: 1. After 300 hours' accelerated aging, a ${\Delta}E$ value was 3.3 or lower in IPS Empress 2-glazed, IPS Empress 2-polished and Sinfony. 2. After 300 hours' accelerated aging, gloss was lost and surface changes including microcracks were observed in TESCERA ATL and SYNERGY Duo, and color changes of them ranged between 3.58 and 6.40 ${\Delta}E$ units. 3. During 300 hours' accelerated aging, the microhardness of surface was increased by 3.21 - 19.64% in all kinds of composites resin. CONCLUSION: After 300 hours' accelerated aging, SEM images IPS Empress 2-glazed, IPS Empress 2-polished and Sinfony showed little morphological change and their color changes were considered to be clinically acceptable. And there was significant correlation between microhardness changes and color changes of composites (P < .05).

• KSCE Journal of Civil and Environmental Engineering Research
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• v.4 no.2
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• pp.55-64
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• 1984

Presented is a nonlinear constitutive model for progressive tensile fracturing of concrete. The model is incremental, path-dependent, and tensorialy invariant. The total strain tensor is assumed to be a sum of a purely elastic component and an inelastic component. The material is considered to contain weak planes of all directions which characterize the planes of the microcracks. A one-to-one functional dependence is assumed between the normal stress and the normal strain across each of the weak planes. The tangential stiffness of concrete is then derived form the principle of virtual work. The present theory can be applied to loading histories which are nonproportional or during which the principal directions rotate. Good agreement with the available direct tensile test data which cover strain-softening is demonstrated.

• Computers and Concrete
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• v.22 no.1
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• pp.93-100
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• 2018

It is seldom possible that geotechnical materials like rocks and concretes found without joints, cracks, or discontinuities. Thereby, the impact of micro-cracks on the mechanical properties of them is to be considered. In the present study, the effect of micro-crack on the failure mechanism of rock specimens under uniaxial compression was investigated experimentally. For this purpose, thermal stress was used to induce micro-cracks in the specimens. Several cylindrical and disk shape specimens were drilled from granite collected from Zanjan granite mine, Iran. Some of the prepared specimens were kept in room temperature and the others were heated by a laboratory furnace to different temperature levels (200, 400, 600, 800 and 1000 degree Celsius). During the experimental tests, Acoustic Emission (AE) sensors were used to monitor specimen failure at the different loading sequences. Also, Scanning Electron Microscope (SEM) was used to distinguish the induced micro-crack by heating in the specimens. The fractographic analysis revealed that the thin sections heated to $800^{\circ}C$ and $1000^{\circ}C$ contain some induced micro-fractures, but in the thin sections heated to $200^{\circ}C$, $400^{\circ}C$ and $600^{\circ}C$ have not been observed any micro-fracture. In the next, a comprehensive experimental investigation was made to evaluate mechanical properties of heated and unheated specimens. Results of experimental tests showed that induced micro-cracks significantly influence on the failure mode of specimens. The specimens kept at room temperature failed in the splitting mode, while the failure mode of specimens heated to $800^{\circ}C$ are shearing and the specimens heated to $1000^{\circ}C$ failed in the spalling mode. On the basis of AE monitoring, it is found that with increasing of the micro-crack density, the ratio of the number of shear cracks to the number of tensile cracks increases, under loading sequences.

• Proceedings of the Korea Concrete Institute Conference
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• 1997.10a
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• pp.3-23
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• 1997

The growth in fast-track construction and repair has prompted major efforts to develop high-early-strength concrete mix compositions. Such mixtures rely on the use of relatively high cement contents and accelerator dosages to increase the rate of strength development. The measures, however, seem to compromise the long-term performance of concrete in applications such as full-depth patches as evidenced by occasional premature deterioration of such patches. The hypothesis successfully validated in this research was that traditional methods of increasing the early-age strength of concrete, involving the use of high cement and accelerator contents, increase the moisture and thermal movements of concrete. Restraint of such movements in actual field conditions, by external or internal restraining factors, generates tensile stresses which introduced microcracks and thus increase the permeability of concrete. This increase in permeability accelerates various processes of concrete deterioration, including freeze-thaw attack. Fiver reinforcement of concrete is an effective approach to the control of microcrack and crack development under tensile stresses. Fibers, however, have not been known of accelerating the process of strength gain in concrete. The recently developed specialty cellulose fibers, however, were found in this research to be highly effective in increasing the early-age strength of concrete. This provides a unique opportunity to increase the rate of strength gain in concrete without increasing moisture an thermal movements, which actually controlling the processes of microcracking and racking in concrete. Laboratory test results confirmed the desirable resistance of specialty cellulose fiber reinforced High-early-strength concrete to restrained shrinkage microcracking an cracking, and to different processes of deterioration under weathering effects.

• The Journal of Korean Academy of Prosthodontics
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• v.29 no.2
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• pp.85-101
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• 1991

The purpose of this study was to determine the optimum range of laser energy density to the enamel surface of permanent incisors when they are irradiated with the pulsed Nd : YAG laser, Laser impacts on each experimental group were made at energy density of $20\sim50J/cm^2$ by 20 pulses of the pulse width 1.2 msec. The author investigated the enamel surface with the sunning electron microscope(SEM) and the surface roughness tester, and measured the shear bond strength between electrolytically etched Ni-Cr-Be alloy casting and composite resin. The obtained results were as follows: 1. The surface roughness of enamel after laser irradiation showed the significant difference level from the energy density $40J/cm^2(P<0.05)$. 2. The mean shear bond strength of etched-metal resin-bonded specimens were $154.23{\pm}33.30kg/cm^2$ at unlased enamel surface and $195.72{\pm}29.56kg/cm^2$ at lased energy density $30J/cm^2$, and showed a significant difference(P<0.05). 8. SEM photographs showed the irregular microcracks and the structural changes of lased enamel surface. 4. SEM photographs of the fracture surface after testing the shear bond strength showed the aspect of interfacial fracture between bonding agent and composite resin at the metal sides.

• Geomechanics and Engineering
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• v.15 no.1
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• pp.615-620
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• 2018

In order to analyze the healing effectiveness of rock salt cracks affected by the applied stresses and time, we used the ultrasonic technology to monitor the ultrasonic pulse velocity (UPV) variations for different initial stress-damaged rock salts during self-healing experiments. The self-healing experiments were to create different conditions to improve the microcracks closure or recrystallized, which the self-healing effect of damaged salt specimens were analyzed during the recovery period about 30 days. We found that: The ultrasonic pulse velocity of the damaged rock salts increases rapidly during the first 9 days recovery, and the values gradually increase to reach constant values after 30 days. The damaged value and the healed value were identified based on the variation of the wave velocity. The damaged values of the specimens that are subject to higher initial damage stress are still keeping in large after 30 days recovery under the same recovery condition It is interesting that the damage and the healing were not in the linear relationship, and there also existed a damage threshold for salt cracks healing ability. When the damage degree is less than the threshold, the self-healing ratio of rock salt is increased with the increase in damage degree. However, while the damage degree exceeds the threshold, the self-healing ratio is decreased with the increase in damage.

• Proceedings of the KSME Conference
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• 2000.04a
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• pp.31-36
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• 2000

High temperature and pressure materials in power plant are degraded by creep damage, if they are exposed to constant loads for long times, which occurs in the load bearing structures of pressurized components operating at elevated temperatures. Many conventional measurement techniques such as replica method, electric resistance method, and hardness test method for measuring creep damage have been used. So far, the replica method is mainly used for the Inspection of High temperature and pressure components. This technique is, however, restricted to applications at the surface of the testpieces and cannot be used to material inside. In this paper, ultrasonic evaluation for the detection of creep damage in the form of cavaties on grain boundaries or integranular microcracks are carried out. And the absolute measuring method of quantitative ultrasonic velocity technique for Cr-Mo material degradation is analyzed. As a result of ultrasonic tests for crept specimens, we find that the sound velocity is decreased as the increase of creep life fraction$({\Phi}_c)$ and also, confirmed that hardness is decreased as the increase of creep life fraction$({\Phi}_c)$ but the coefficient of ultrasonic attenuation is increased as the increase of creep life fraction$({\Phi}_c)$. Finally based on the result in this paper, it can be recognized that the ultrasonic techniques using velocities and attenuation coefficient factor are very useful non-destructive methods to evaluate the degree of material degradation in fossile power plants.

• Journal of the Mineralogical Society of Korea
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• v.19 no.4 s.50
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• pp.383-392
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• 2006

Calcium carbonate stone deterioration has been intensified in urban area, mainly due to the action of atmospheric pollutant. Samples from the black surface layer were examined under petrographic and scanning electron microscope, coupled with energy dispersive X-ray analyser X-ray fluorescence and X-ray diffraction analysis was also carried out for chemical composition and mineral phase analysis, respectively. Moreover, sulphur isotope ratio was measured, in order to identify the origin of sulphate compounds in the black surface layer. Optical and electronic petrographic analysis indicated that gypsum and Quartz were contained in the black surface layer and led to microcracks. Microstructure and chemical composition analysis showed that the interface between black layer and original stone is not black but its characteristic is similar to black layer The results indicated that during deterioration process the black layer can be expanded gradually into the interface by adsorption of atmospheric pollutants. The sulphur isotope analysis demonstrates that there are different origins of the sulphur component in black surface layer.

• Korean Journal of Materials Research
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• v.10 no.7
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• pp.505-514
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• 2000

The carburizing behavior and fatigue properties of the plasma carburized low carbon Cr-Mo steel(0.176C-1.014Cr-0.387Mo) have been investigated. The effective case depth in plasma carburized steel increased up to 50% in comparison with that of gas carburizing, and this case depth increased with the increasing surface carbon content. With increasing time in plasma carburizing, the surface carbon content increased but its increasing rate decreased. Fatigue properties were studied in terms of microstructure, case depth, retained austenite and residual stress near the surface. The fatigue limit of the plasma carburized steel was higher than that of gas carburized one. The initiation of microcracks and initial crack propagation were retarded due to a relatively little surface and internal oxidation layer in plasma carburized steel. Fractography showed the crack initiated at the surface, and transgranular fracture at surface layer was more predominant in plasma carburized steel compared to that of gas carburized steel.

• International Journal of Highway Engineering
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• v.3 no.2 s.8
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• pp.123-130
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• 2001

This study was performed to enhance mechanical properties of high-early-strength concrete using regulated-set cement for early traffic opening with various mixtures. Restraint of moisture and thermal movements of concrete pavement in actual field conditions, by external or internal restraining factors, generates tensile stresses which introduce microcracks and thus reduce the mechanical properties of concrete. Fiber reinforcement of concrete is an effective approch to the control of microcrack and crack development under tensile stresses. Three different types of regulated-set cement which recently have been used in Korea and two different types of fiber were adopted. Fibers were added and their mixtures are compared with plain high-early-strength concrete mixture. From the test results, fiber reinforced concrete was increased mechanical properties of high-early-strength concrete using regulated-set cement than the plain concrete.