• The Korean Journal of Ceramics
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• v.1 no.1
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• pp.1-6
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• 1995

Submicrometer, monosized ceramic powder of $Al_2TiO_5$$Al_2O_3$ ethanolic solutions. All particles produced by sol-gel-process were amprphous, monodispersed and with a narrow particle-size distribution. Compacts fired above $1300^{\circ}C$ formed aluminium titanate. Mullite formed first at $1480^{\circ}C$. After decomposition test at $1100^{\circ}C$, and cyclic thermal decomposition test at 750-1400-$750^{\circ}C$ for 100hrs., aluminium titanate was well stablized by composition with mullite.

• Journal of the Korean Ceramic Society
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• v.24 no.5
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• pp.477-483
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• 1987

Cr2O3 doped Pb(Zr0.525 Ti0.475)O3 piezoelectric ceramics were prepared from reagent grade oxide mixture, PbO, ZrO2, TiO2 and Cr2O3. Piezoelectric and aging properties of specimens were measured for various additions of Cr2O3. Generally, it has been known that aging rate decreased with Cr2O3 addition by stabilizing the domain wall. But hysteresis loops showed that the domain destabilization was occurred at high electric field (larger than 10KV/cm). In smaller additions of Cr2O3 (0-0.2mol%), aging rate increased and microcracks were created with increasing poling filed due to increasing internal stress. In larger additions of Cr2O3(0.4∼0.6mol%), aging rate decreased with increasing poling field.

• Proceedings of the KIEE Conference
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• 2011.07a
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• pp.1318-1319
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• 2011

In this paper, we analyzed of growth and electrical characteristics of micro-cracks with thermal effect in PV module. The micro-cracks are increasing the breakage risk over the whole value chine from the wafer to the finished module, because the wafer or cell is exposed to mechanical stress. we experimentally analyze the direct impact of micro-cracks on the module power and the consequences after artificial aging. The first step, we made micro-cracks in PV module by mechanical load test according to IEC 61215. Next, PV modules applied the thermal cycling test, because microcracks accelerated aging by thermal cycling test. according to IEC61215. Before every test, we checked output and EL image of PV module.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 1991.11a
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• pp.54-58
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• 1991

It is well known that metal cutting leaves a plastically deformed layer in the machined surface. This residual phenomenon affects in various forms the physical properties of machined components such as the fatigue strength, the dimensional instability, microcracks, and the stress corrosion cracking. These physical properties, so called surface integrity, are very important for designing highly stressed and critically loaded components. Typical plastic strains in the machined surface are very difficult to measure, since they are located within a very short distance from the surface and they change very rapidly. There is an alternative way to determine the residual strain in plastically deformed materials by measuring the grain size after a subsequent recrystallization process. Although, this technique has been successfully applied by several researchers to find the plastic zone around notches and cracks in various materials and welding beads, few works have been reported using the recrystallization method to determine the residual strains in machined surface. Therefore, the purpose of this investigation Is to explore the effectiveness of the recrystallization technique in machining applications, and in particular, to find the effect of cutting parameters, i.e., depth of cut and rake angle on the plastic strains.

• Journal of the Korean Ceramic Society
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• v.29 no.5
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• pp.335-340
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• 1992

Undoped PbTiO3 ceramics was successfully prepared by using sol-gel process, which had not been fabricated due to its microcracks created by anisotropic stress during phase transition from cubic to tetragonal phase. Fabrication of undoped PbTiO3 ceramics via sol-gel processing was very much affected by the PbO content of the samples as well as PbO vapor from sintering atmosphere. Excess PbO was found to promote rapid grain growth in PbTiO3 ceramics. After sintering at 1100$^{\circ}C$ average grain size of PbTiO3 ceramics with excess PbO was about 8 times greater than that of stoichiometric composition, which may be due to PbO liquid phase from excess PbO.

• Tunnel and Underground Space
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• v.9 no.4
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• pp.364-372
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• 1999

In this paper, mechanical characteristics of micro-defects in granitic rock was studied. Crack spacing and length were investigated by scanline survey in specimen of granite. To estimate the direction and distribution of potential microcrack in granite, thin sections were made for three direction of Rift, Grain and Hardway axis of the rock specimen. The density and length of microcrack were investigated quantitatively. Three directions of microcracks are comparatively perpendicular. Crack density varies as direction differs, but crack length doesn't show influence of direction.

• International Journal of Automotive Technology
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• v.1 no.2
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• pp.71-77
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• 2000

High temperature materials in service are subjected to mechanical damage due to operating load and metallurgical damage due to operating temperature. Therefore, when designing or assessing life of high temperature components, both factors must be considered. In this paper, the effect of tensile hold time on high temperature fatigue crack growth and long term prior thermal aging heat treatment on creep rupture behavior were investigated using STS 316L and STS 316 austenitic stainless steels, which are widely used for high temperature components like in automotive exhaust and piping systems. In high temperature fatigue crack growth tests using STS 316L, as tensile hold time increased, crack growth rate decreased in relatively short tensile hold time region. In long term aged specimens, cavity type microcracks have been observed at the interface of grain boundary and coarsened carbide.

• Journal of the Korean Society for Heat Treatment
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• v.18 no.5
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• pp.297-304
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• 2005

This study was performed to determine the repair weldability of the damaged Ni type superalloy used for gas turbine blade. The experimental works included the evaluation of the microstructures of the damaged blade, selection of the repair welding procedure, characterization of repair weldment and finding the heat treatment procedures for repaired weldment. The morphology of the microstructure for the base metal was composed of austenite matrix with cubical ${\gamma}^{\prime}$ phase, MC type coarse precipitates located within grain and fine $M_{23}C_6$ type precipitates decorated at grain boundaries. The repair welding process using 90 amp current exhibited the best weld properties showing no weld microcracks. The solution and aging heat treatments of the repaired weldment could recover the original service properties of the damaged blade.

• Journal of Powder Materials
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• v.9 no.3
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• pp.148-152
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• 2002

The microstructures and indentation fracture of pressureless-sintered $DyNbO_4$ crystalline were investigated as a basic study for the application of weak phase of fibrous monolithic composites. They were comprised with many lamella twins as well as micro-cracks at the grain boundaries. The hardness at room temperature was remarkably low value(575 Hv) due to the low relative density and existence of microcracks at grain boundaries. The main fracture mode was a typical intergranular fracture, and showed remarkable micro-cracking effect. The heavy plastic deformation was observed around the site of indentation. In addition, the $DyNbO_4$ was expected to apply as a weak phase in the fibrous monolithic composites because of the low hardness and easily plastic deformation that could be led the preferable pulled-out and microcracking toughening under the failure.

• Korean Journal of Materials Research
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• v.7 no.8
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• pp.650-653
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• 1997

In large generators in power plants, stator winding insulations is exposed to a combination of thermal, electrical, mechanical, environmental stresses in service. These combined stresses cause insulation aging which leads to final insulation breakdown. In order to identify the breakdown mechanism, the stator winding insulation materials which are composed of mica-epoxy is analyzed by the component of materials with EDS, SEM techniques. We concluded that the potassium ions of mica are replaced by hydrogen ions at boundary area of mica-epoxy and/or mica-mica. It is proposed that through these phenomena, the conductive layers of potassium ions enable high voltage fields of multiple stresses to create voids and microcracks.