• Journal of the Korean Society for Precision Engineering
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• v.21 no.8
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• pp.89-96
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• 2004

Micro-tensile testing system, consisting of a micro tensile loading system and micro-ESPI(Electronic Speckle Pattern Interferometry) system, has been developed for measurement of micro-tensile properties of thin micro-materials. Micro-tensile loading system had a load cell with the maximum capacity of 50N and micro actuator with resolution of 4.5nm in stroke. The system was used to apply a tensile load to the micro-sized specimen. During tensile loading, the micro-ESPI system acquired interferornetric speckle patterns in the deformed specimen and measured the in-plane tensile strain. The ESPI system consisted of a CCD-camera with a lens and the window-based program developed for this experiment. Using this system, stress-strain curves for 4 kinds of electrolytic copper foil 18$\square$m thick were obtained. From these curves, tensile properties, including the elastic modulus. yielding strength and tensile strength, were determined and also values of the plastic exponent and coefficient based on Ramberg-Osgood relationship were evaluated.

• Proceedings of the KSME Conference
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• 2004.04a
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• pp.240-245
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• 2004

Tensile properties of hard coating material, TiN, were evaluated using micro-tensile testing system. TiN has been known as a hard coating material commonly used today. Micro-tensile testing system consisted of a micro tensile loading system and a micro-ESPI(Electronic Speckle Pattern Interferometry) system. Micro-tensile loading system had a maximum load capacity of 500mN and a resolution of 4.5 nm in stroke. TiN thin film $1{\mu}m$ thick was deposited on the Si wafer pre-deposited of $Si_3N_4$ film substrate by the closed field unbalanced magnetron sputtering (CFUBMS) process. Three kinds of micro-tensile specimen with the respective width of $50{\mu}m$, $100{\mu}m$ and $500{\mu}m$ were fabricated by MEMS process. The mechanical properties including tensile strength and elastic modulus were determined using the micro-tensile testing system and compared by those obtained by nano-indentation

• Transactions on Electrical and Electronic Materials
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• v.13 no.5
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• pp.248-251
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• 2012

In order to develop a high voltage insulation material, epoxy/micro-silica composites (EMC) and epoxy/micro-silica/nano-silica composites (EMNC) with three different particle sizes in ${\mu}m$ and one particle size in nm were prepared and their tensile and flexural tests were carried out and the data was estimated by Weibull statistical analysis. The tensile strength of the neat epoxy was 82.8 MPa and those of the EMCs were larger than that of the neat epoxy, and they were much more advanced by the addition of 10 nm sized nano-silica to the EMCs. Flexural strength showed the same tendency of the tensile strength. As the micro-particle size decreased, tensile and flexural strength increased.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.10a
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• pp.132-136
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• 2009

The importance and interests for saving of energy and cost in industry has been steadily grown up. Therefore, process optimization to reduce the processing step and energy is one of the most important things. The micro-alloyed steel of which post-heat-treatment is not necessary, has attractive points for high strength materials. However, for the application of non-heat-treated steel to structural parts, it is necessary to confirm the reliability of mechanical properties. In order to estimate mechanical properties. The microstructure, hardness, tensile strength, compressive strength and tensile fatigue strength of micro-alloyed steel having 900MPa tensile strength has been investigated.

• Advances in nano research
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• v.15 no.6
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• pp.495-511
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• 2023

In this research, the impact of micro-silica, nano-silica, and polypropylene fibers on the fracture energy of self-compacting concrete was thoroughly examined. Enhancing the fracture energy is very important to increase the crack propagation resistance. The study focused on evaluating the self-compacting properties of the concrete through various tests, including J-ring, V-funnel, slump flow, and T50 tests. Additionally, the mechanical properties of the concrete, such as compressive and tensile strengths, modulus of elasticity, and fracture parameters were investigated on hardened specimens after 28 days. The results demonstrated that the incorporation of micro-silica and nano-silica not only decreased the rheological aspects of self-compacting concrete but also significantly enhanced its mechanical properties, particularly the compressive strength. On the other hand, the inclusion of polypropylene fibers had a positive impact on fracture parameters, tensile strength, and flexural strength of the specimens. Utilizing the response surface method, the relationship between micro-silica, nano-silica, and fibers was established. The optimal combination for achieving the highest compressive strength was found to be 5% micro-silica, 0.75% nano-silica, and 0.1% fibers. Furthermore, for obtaining the best mixture with superior tensile strength, flexural strength, modulus of elasticity, and fracture energy, the ideal proportion was determined as 5% micro-silica, 0.75% nano-silica, and 0.15% fibers. Compared to the control mixture, the aforementioned parameters showed significant improvements of 26.3%, 30.3%, 34.3%, and 34.3%, respectively. In order to accurately model the tensile cracking of concrete, the authors used softening curves derived from an inverse algorithm proposed by them. This method allowed for a precise and detailed analysis of the concrete under tensile stress. This study explores the effects of micro-silica, nano-silica, and polypropylene fibers on self-compacting concrete and shows their influences on the fracture energy and various mechanical properties of the concrete. The results offer valuable insights for optimizing the concrete mix to achieve desired strength and performance characteristics.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2003.06a
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• pp.1059-1062
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• 2003

Micro-tensile testing system has been developed and micro-tensile tests for copper foil have been carried out. The system consisted of a micro tensile loading system and a micro-ESPI system for measuring strain. The loading system has a maximum loading capacity of 50N and a stroke resolution of 4.5nm. Stress-strain curves for the electro-deposited copper foil with the thickness of 18$\mu\textrm{m}$ were obtained, and tensile properties, including elastic modulus, yielding strength and tensile strength, were determined. The tensile properties obtained under three different conditions of testing speed showed a dependency on the speed.

• Structural Engineering and Mechanics
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• v.18 no.5
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• pp.691-707
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• 2004

This paper presents the micro-mechanical modeling for predicting concrete behavior under compressive loading. The model is able to represent the heterogeneities in the microstructure up to three phases, i.e., aggregate particles, matrix and interfaces. The smeared crack concept based on non-linear fracture mechanics is implemented in order to formulate the constitutive relation for each component. The splitting tensile strength is considered as a fracture criterion for cracking in micro-level. The finite element method is employed to simulate the model based on plane stress condition by using quadratic triangular elements. The validation of the model is verified by comparing with the experimental results. The influence of tensile strength from both aggregate and matrix phases on the concrete compressive strength is demonstrated. In addition, a guideline on selecting appropriate tensile strength for each phase to obtain specified concrete compressive strength is also presented.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.31 no.7
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• pp.496-501
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• 2018

In this study, we prepared 40, 45, 50, 55, 60, 65, and 70 wt% content composites filled in epoxy matrix for two micro silica and three micro alumina types for use as a GIS heavy electric machine. As a filler type of epoxy composite, micro silica composites showed excellent AC breakdown strength properties compared to micro alumina composites in the case of electrical properties of micro silica and alumina. The electrical breakdown properties of micro silica composites increased with increasing filler content, whereas those of micro alumina decreased with increasing filler content. In the case of mechanical properties, the micro silica composite showed improved tensile strength and flexural strength compared with the micro alumina composite. In addition, mechanical properties such as tensile strength and flexural strength of micro silica and alumina composites decreased with increasing filler content. This is probably because O-H groups are present on the surface of silica in the case of micro silica but are not present on the surface of alumina in the case of micro alumina.

• Steel and Composite Structures
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• v.39 no.4
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• pp.401-417
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• 2021

This study experimentally reveals the influence of welding on grade S690Q high strength steel (HSS) butt joints from both micro and macro levels. Total eight butt joints, taking plate thickness and welding heat input as principal factors, were welded by shielded metal arc welding. In micro level, the microstructure transformations of the coarse grain heat affected zone (CGHAZ), the fine grain heat affected zone (FGHAZ) and the tempering zone occurred during welding were observed under light optical microscopy, and the corresponding mechanical performance of those areas were explored by micro-hardness tests. In macro level, standard tensile tests were conducted to investigate the impacts of welding on tensile behaviour of S690Q HSS butt joints. The test results showed that the main microstructure of S690Q HSS before welding was tempered martensite. After welding, the original microstructure was transformed to granular bainite in the CGHAZ, and to ferrite and cementite in the FGHAZ. For the tempering zone, some temper martensite decomposed to ferrite. The performed micro-hardness tests revealed that an obvious "soft layer" occurred in HAZ, and the HAZ size increased as the heat input increased. However, under the same level of heat input, the HAZ size decreased as the plate thickness increased. Subsequent coupon tensile tests found that all joints eventually failed within the HAZ with reduced tensile strength when compared with the base material. Similar to the size of the HAZ, the reduction of tensile strength increased as the welding heat input increased but decreased as the thickness of the plate increased.

• The Transactions of The Korean Institute of Electrical Engineers
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• v.67 no.9
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• pp.1181-1188
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• 2018

In order to develop new insulating materials for GIS Spacer using environmentally friendly insulating gas, three kinds of dispersed liquid nano composites of solid epoxy /nano layered silicate filled material were prepared. And the epoxy/nano/micro silica composite was prepared by mixing epoxy/nano 3 phr dispersion/4 kinds of filler contents(40,50,60, 70wt%). The electrical insulation breakdown strengths of the nano and nano/micro mixed composites were evaluated by using 8 kinds of samples including the original epoxy. The mechanical tensile strength of the epoxy / nano / micro silica composite were evaluated, also. The TEM was measured to evaluate the internal structure of nano/micro composites. As a result, it was confirmed that the layered silicate nano particles was exfoliated through the process of inserting epoxy resin between silicate layers and the layers. In addition, dispersion of nano / micro silica resulted in improvement of electrical insulation breakdown strength with increase of filling amount of dense tissue with nanoparticles inserted between microparticles. In addition, the tensile strength showed a similar tendency, and as the content of microsilica filler increased, the mechanical improvement was further increased.