• Title/Summary/Keyword: micro-segregation

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A Study of Preventing Chevron Crack in Cold Extrusion (냉간 압출시 Chevron Crack 방지에 대한 고찰)

  • 최영순;이정환
    • Transactions of Materials Processing
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    • v.6 no.3
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    • pp.221-226
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    • 1997
  • Chevron crack in cold extrusion has been studied in view of deformation conditions and material characteristics. There is V formed chevron crack is occasionally occurred in core part of shaft by multistage free extrusion. Although many research results were reported and theoretical analyses were accompanied, in this study we discussed practical method to prevent chevron crack in the field of working conditions and material characteristics. We have found that chevron crack is eliminated under condition of high hydrostatic state in deformation and decreased segregation, refinement of micro structure of materials.

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Analysis on the non-equilibrium dendritic solidification of a binary alloy with back diffusion (역확산을 고려한 이원합금의 비평형 수지상응고 해석)

  • Jeong, Jae-Dong;Yu, Ho-Seon;Lee, Jun-Sik
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.20 no.10
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    • pp.3361-3370
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    • 1996
  • Micro-Macro approach is conducted for the mixture solidification to handle the closely linked phenomena of microscopic solute redistribution and macroscopic solidification behavior. For this purpose, present work combines the efficiency of mixture theory for macro part and the capability of microscopic analysis of two-phase model for micro part. The micro part of present study is verified by comparison with experiment of Al-4.9 mass% Cu alloy. The effect of back diffusion on the macroscopic variables such as temperature and liquid concentration, is appreciable. The effect, however, is considerable on the mixture concentration and eutectic fraction which are indices of macro and micro segregation, respectively. According to the diffusion time, the behavior near the cooling wall where relatively rapid solidification permits short solutal diffusion time, approaches Scheil equation limit and inner part approaches lever rule limit.

Mechanical Characteristics and Macro-and Micro-structures on Friction Stir Welded Joints with 5083O Al Alloys (Al 5083O합금의 마찰교반용접부의 조직과 특성평가)

  • Jang, Seok-Ki;Park, Jong-Seek
    • Journal of Advanced Marine Engineering and Technology
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    • v.33 no.1
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    • pp.104-111
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    • 2009
  • This paper shows the behaviors of macro- and micro-structures and mechanical properties for specimen's welding region welded by FSW. according to welding conditions with 5mm thickness aluminum 5083O alloy plate. It apparently results in defect-free weld zone in case traverse speed was changed to 32 mm/min under conditions of anti-clockwise direction and tool rotation speed such as 800 and 1250 rpm with tool's pin diameter of 5 ${\Phi}mm$ and shoulder diameter of 20 ${\Phi}mm$, pin length of 4.5 mm and tilting angle of $2^{\circ}$. The ultimate stress of ${\sigma}_T=331$ MPa and the yield point of 147 MPa are obtained at the condition of the travel speed of 32 mm/min with the tool rotation speed of 1250 rpm. There is neither voids nor cracks on bended surface of $180^{\circ}$ after bending test. The improvement of toughness after impact test was found. The lower rotating and traverse speed became, the higher were yield point, maximum stress and elongation(%) with the stresses and the elongation(%) versus the traverse speed diagram. Vickers hardness for cross section of welding zone were also presented. The typical macro-structures such as dynamically recrystallized zone, thermo-mechanically affected zone and heat affected zone and the micro-structures of the transverse cross-section were also showed. However, the author found out that the region of 6mm far away from shoulder circumference was affected by friction heat comprehensively, that is, hardness softened and that part of micro-structures were re-solid-solution or recrystallized, the author also knew that there is no mechanically deformation on heat affected zone but there are the flow of plastic deformation of $45^{\circ}$ direction on thermo-mechanically affected zone and the segregation of Al-Mg on nugget. The solid solution wt(%) of parent material as compared against of friction stir welded zone was comprehensively changed.

Uptake of Isolated Lyophyllum ulmarium Chromosomes by Ganoderma applanatum Protoplasts (잔나비걸상버섯 원형질체(原形質體)에 의(依)한 만가닥버섯 염색체(染色體)의 섭입(攝入))

  • Yoo, Young-Bok;You, Chang-Hyun;Chang, Kwon-Yawl
    • The Korean Journal of Mycology
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    • v.16 no.4
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    • pp.247-252
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    • 1988
  • The uptake of isolated Lyophyllum ulmarium chromosomes by Ganoderma applanatum protoplasts was induced with polyethylen $glycol+CaCl_2+glycine$. Uptake products of chromosomes by protoplasts showed micro-and macrotransgenome type. The former was slowly growing and unstable, the latter was outgrowing and stable mycelial colonies which made thick hyphae of width and segregation of mycelial colony on GCM containing benomyl. A comparison of macrotransgenome type was using isozyme analysis of esterase. The enzyme pattern of two transformants was distinct in position and quantity compared with parents.

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Segregation Mechanism in Si1-xGex Single Crystal Fiber Growth by Micro-pulling Down Method

  • Uda, Satoshi;Kon, Junichi;Shimamura, Kiyoshi;Fukuda, Tsuguo
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1996.06a
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    • pp.399-421
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    • 1996
  • (1) The solute distribution mechanism was analyzed for the Si0.95Ge0.05 single crystal fiber by u-PD method. (2) The steady-state solutions were obtained for the molten zone and the capillary zone. (3) The effect of the convection in the molten zone on partitioning was not significant for many cases. (4) Intermediate transient rise of Ge was shown by the sudden change of the growth velocity or molten zone height. (5) Periodic compositional modulation can be designed by using the intermediate transient.

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Investigating the use of wollastonite micro fiber in yielding SCC

  • Sharma, Shashi Kant;Ransinchung, G.D.;Kumar, Praveen
    • Advances in concrete construction
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    • v.6 no.2
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    • pp.123-143
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    • 2018
  • Self compacting concrete (SCC) has good flowability, passability and segregation resistance because of voluminous cementitious material & high coarse aggregate to fine aggregate ratio, and high free water availability. But these factors make it highly susceptible to shrinkage. Fibers are known to reduce shrinkage in concrete mixes. Until now for conserving cement, only pozzolanic materials are admixed in concrete to yield a SCC. Hence, this study compares the use of wollastonite micro fiber (WMF), a cheap pozzolanic easily processed raw mineral fiber, and flyash in yielding economical SCC for rigid pavement. Microsilica was used as a complimentary material with both admixtures. Since WMF has large surface area ($827m^2/kg$), is acicular in nature; therefore its use in yielding SCC was dubious. Binary and ternary mixes were constituted for WMF and flyash, respectively. Paste mixes were tested for compatibility with superplasticizer and trials were performed on a normal concrete mix of flexural strength 4.5 MPa to yield SCC. Flexural strength test and restrained shrinkage test were performed on those mixes, which qualified self compacting criteria. Results revealed that WMF admixed pastes have high water demand, and comparable setting times to flyash mixes. Workability tests showed that 20% WMF with microsilica (5-7.5%) is efficient enough in achieving SCC and higher flexural strength than normal concrete at 90 days. Also, stress rate due to shrinkage was lesser and time duration for final strain was higher in WMF admixed SCC which encourages its use in yielding a SCC than pozzolanic materials.

Corrosion Characteristics of a 5Cr-1Mo Steel Specimen by Sodium-Water Reaction (나트륨-물 반응에 의한 5Cr-1Mo Steel 시편의 부식특성)

  • Jeong, Kyung-Chai;Jeong, Ji-Yeong;Park, Jin-Ho;Hwang, Sung-Tai;Kim, Eui-Sik
    • Applied Chemistry for Engineering
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    • v.9 no.7
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    • pp.1023-1029
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    • 1998
  • Small water leak experiment was carried out for the 5Cr-1Mo steel specimen in sodium atmosphere. Perfect re-open time for the leak path of a specimen, by micro leak, was 129 minutes, and its size observed about 2 mm diameter at sodium side. The halos phenomena appeared around of leak spot before the leak path has re-opened, and the size of halos observed was different from the real re-open size of a specimen. Also, the corrosion of a specimen initiated from sodium side, but it did not occur at steam side. In AES analysis, the segregation phenomena of Cr in the specimen was found much more than those of other elements. And also, the sodium compounds formed by sodium-water reaction and deposited onto the leak site of specimen were observed by EPMA analysis and SEM photograph. It is postulated that the corrosion products could be precipitated to form mixed Na Fe Cr compounds.

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Influence of Ge addition on AC loss and micro-structure in $Nb_{3}Sn$ wires (Ge를 첨가한 Nb$_3$Sn 초전도 선에서의 교류손실 및 미세조직 변화)

  • 하도우;이남진;오상수;하홍수;송규정;권영길;류강식
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2001.07a
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    • pp.104-107
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    • 2001
  • In order to investigate the effect of Ge addition to the Cu matrix on the microstructure and the critical current density, four kinds of internal tin processed Nb$_3$Sn strands with pure Cu and Cu 0.2, 0.4, 0.6 wt % Ge alloys were drawn to 0.8 mm diameter. The microstructure and critical current of internal tin processed Nb$_3$Sn wires that were heat treated at temperatures ranging from 68$0^{\circ}C$ to 74$0^{\circ}C$ for 240h were investigated. The Ge addition to the matrix did not make workability worse. A Ge rich layer in the Cu-Ge matrix suppressed the growth of the Nb$_3$Sn layer and promoted grain coarsening. The greater the Ge content in the matrix, the lower the net Jc result after Nb$_3$sn reaction heat treatment. There was no significant variation in Jc observed with heat treatment temperature ranging from 68$0^{\circ}C$ to 74$0^{\circ}C$. The values of AC loss of Ge added wires were decreased to 40 % compare with no addition wire. Low AC loss was due to segregation of Ge rich layer in the Cu-Ge matrix. If Ge added wire with thin Nb filaments were fabricated, slow diffusion rate of Sn would be overcome and decreased AC loss that is weak Point of internal tin method.

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