• 비파괴검사학회지
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• 제22권2호
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• pp.132-139
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• 2002

최근 구속전단가공(Equal-Channel Angular Pressing)이라는 가공법을 이용하여 결정립을 미세화시키는 유효한 수단이 널리 이용되어지고 있다. 이러한 구속전단가공법을 이용해서 알루미늄합금의 결정립을 submicrometer 수준으로 미세화가 가능하게 되었다. 본 연구에서는 인장시험, 경도시험, 미세조직 관찰, 초음파탐상 및 음향방출 시험을 통해 알루미늄합금의 결정립 미세화 정도를 평가하였다. ECAP 가공 후 결정립 미세화에 의하여 강도 및 경도가 확실히 증가하였다. 초음파 탐상으로부터 초음파 음속은 ECAP 가공 후의 음속이 빠르게 나타났으며, 시간 -주파수 분석에서는 ECAF 가공 전의 시험편이 고주파수의 감쇠가 컸다. 그리고 ECAP 가공 후의 시험편에서 음향방출의 높은 중심주파수 대역이 나타났다. 본 논문은 비파괴적인 기법을 사용하여 결정립 미세화를 판단하는데 기초적인 자료로서의 활용이 기대된다.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2000년도 추계학술대회논문집A
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• pp.105-110
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• 2000

The Micromechanics test is new test method which uses comparatively smaller specimen than that required in conventional material tests. There are several methods, such as small-specimen creep test, the continuous indentation test, and small punch(SP) test. Among them, the small punch(SP) test method has been applied to many evaluation fields, such as a ductile-brittle transition temperature, stress corrosion cracking, hydrogen embrittlement, and fracture properties of advanced materials like FGM or MMC. In this study, the small punch(SP) test is performed to evaluate the mechanical properties at high/low temperature from $-196^{\circ}C$ to $650^{\circ}C$ and the material degradation for virgin and aged materials of 9Cr1MoVNb steel which has been recently developed. The ${\Delta}P/{\Delta}{\delta}$ parameter defined a slope in plastic membrane stretching region of SP load-displacement curve decreases according to the increase of specimen temperature, and that of aged materials is higher than the virgin material in all test temperatures. And the material degradation degrees of aged materials with $630^{\circ}C$ -500hrs and $630^{\circ}C$ -1000hrs are $36^{\circ}C$ and $38^{\circ}C$ respectively. These behaviors are good consistent with the results of hardness($H_v$) and maximum displacement(${\delta}_{max}$).

• 한국분말재료학회지
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• 제17권4호
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• pp.302-311
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• 2010

In this research, the refinement behavior of the coarse magnesium powders fabricated by gas atomization was investigated as a function of milling time using a short duration high-energy ball milling equipment, which produces fine powders by means of an ultra high-energy within a short duration. The microstructure, hardness, and formability of the powders were investigated as a function of milling time using X-ray diffraction, scanning electron microscopy, Vickers micro-hardness tester and magnetic pulsed compaction. The particle morphology of Mg powders changed from spherical particles of feed metals to irregular oval particles, then platetype particles, with increasing milling time. Due to having HCP structure, deformation occurs due to the existence of the easily breakable C-axis perpendicular to the base, resulting in producing plate-type powders. With increasing milling time, the particle size increased until 5 minutes, then decreased gradually reaching a uniform size of about 50 micrometer after 20 minutes. The relative density of the initial power was 98% before milling, and mechanically milled powder was 92~94% with increase milling time (1~5 min) then it increased to 99% after milling for 20 minutes because of the change in particle shapes.

• Tribology and Lubricants
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• 제32권5호
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• pp.160-165
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• 2016

AISI 4140 steel is widely used in various mechanical components owing to its superior mechanical properties. Surface hardening techniques are often used to further improve the properties, particularly for applications with moving components. The aim of this research is to understand the effect of heat treatment process on surface properties and tribological characteristics of AISI 4140 steel. In this work, we prepare two different AISI 4140 steel specimens- one cooled by air and one by oil- and determine surface properties such as surface topography and roughness using a confocal microscope. We also observe the cross-sections of the specimens using a scanning electron microscope to understand the difference in the material structure. In addition, we assess the hardness with respect to the distance from the surface using a micro-Vickers hardness tester. After characterizing the surfaces of the specimens, we investigate the wear characteristics of the specimens under hydrodynamic lubrication. The results show the presence of grooves on the surface of the oil-cooled specimens. It is likely that such grooves are formed during the cooling process using the oil. However, we observe no other significant differences in the surface properties of the specimens. The wear test results show the occurrence of severe wear on the oil-cooled specimens, which may be due to the groove formed on the surface. The results of this work may be helpful to improve surface properties using surface hardening techniques from a tribological perspective.

• 한국분말재료학회지
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• 제22권6호
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• pp.426-431
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• 2015

Microstructural examination of the Nb-Si-B alloys at Nb-rich compositions is performed. The Nb-rich corner of the Nb-Si-B system is favorable in that the constituent phases are Nb (ductile and tough phase with high melting temperature) and $T_2$ phase (very hard intermetallic compound with favorable oxidation resistance) which are good combination for high temperature structural materials. The samples containing compositions near Nb-rich corner of the Nb-Si-B ternary system are prepared by spark plasma sintering (SPS) process using $T_2$ and Nb powders. $T_2$ bulk phase is made in arc furnace by melting the Nb slug and the Si-B powder compact. The $T_2$ bulk phase was subsequently ball-milled to powders. SPS is performed at $1300^{\circ}C$ and $1400^{\circ}C$, depending on the composition, under 30 MPa for 600s, to produce disc-shaped specimen with 15 mm in diameter and 3 mm high. Hardness tests (Rockwell A-scale and micro Vickers) are carried out to estimate the mechanical property.

• 한국분말재료학회지
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• 제21권3호
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• pp.207-214
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• 2014

In this study, nano-scale copper powders were reduction treated in a hydrogen atmosphere at the relatively high temperature of $350^{\circ}C$ in order to eliminate surface oxide layers, which are the main obstacles for fabricating a nano/ultrafine grained bulk parts from the nano-scale powders. The changes in composition and microstructure before and after the hydrogen reduction treatment were evaluated by analyzing X-ray diffraction (XRD) line profile patterns using the convolutional multiple whole profile (CMWP) procedure. In order to confirm the result from the XRD line profile analysis, transmitted electron microscope observations were performed on the specimen of the hydrogen reduction treated powders fabricated using a focused ion beam process. A quasi-statically compacted specimen from the nano-scale powders was produced and Vickers micro-hardness was measured to verify the potential of the powders as the basis for a bulk nano/ultrafine grained material. Although the bonding between particles and the growth in size of the particles occurred, crystallites retained their nano-scale size evaluated using the XRD results. The hardness results demonstrate the usefulness of the powders for a nano/ultrafine grained material, once a good consolidation of powders is achieved.

• 한국안전학회지
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• 제20권1호
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• pp.18-23
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• 2005

This study deals with the friction and wear characteristics of C-N coated SCM415 steel. The PSII(plasma source ion implantation) apparatus was built and a SCM415 test piece with steel substrate was treated with carbon nitrogen by this apparatus. The composition and structure of the surface layer were analyzed and compared with that of PVD(physical vapor decomposition) coated TiN layer. It was found that both of friction coefficient of C-N coating and TiN coating decreased with increasing load, however, C-N coating showed relatively lower faction coefficient than that of TiN coating. The micro-vickers hardness of C-N film is 3200 Hv, which is $32\~43\%$ higher than that of TiN film. The critical load of C-N film is 52N, which is $25\%$ higher than that of TiN film. The hardness of C-N film fabricated by Plasma ion implantation is $61\~70\%$ higher than that of base material, and faction coefficient is $14\~50\%$ lower than that of base material. It is also interesting to note that the friction was changed from adhesive wear mode to light oxidizing wear mode.

• 한국금형공학회:학술대회논문집
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• 한국금형공학회 2008년도 하계 학술대회
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• pp.23-26
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• 2008

In order to examine the deformation characteristics of Al circular pipe underthe biaxial compression, the horizontal biaxial compression die for the experiment was manufactured. From this, in the various compressive strain rate (1 mm/min. ${\sim}$ 400 mm/min.)conditions, the circular pipes, which were made by Al materials, were investigated based on the properties change of cross section area, punch load and deformation behavior. The tensile and compressive strains were evaluated from micro Vickers hardness tester. From these results, the punch load and deformation characteristic of Al circular pipes were highly changed in the compressive strain rate about 200 mm/min. The Al circular pipes had the tendency that the punch load decreased with increasing the compressive strain rate. In addition, following as the change of the shape and position of neutral axis due to the deformation proceeding of the circular pipe, the special point of the internal circular pipe at maximum load showed the maximum deformation strain and the maximum measured hardness value. The CAE (computer aided engineering) simulation using Deform-2D program was performed on the circular pipe in order to know and verify the exact compressive deformation behavior. From these results, the experimentally measured results were reasonably in good agreement with the simulation results.

• 열처리공학회지
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• 제27권6호
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• pp.281-287
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• 2014

Microstructural and mechanical characteristics of Al-6Si-2Cu alloy for engine mount bracket prepared by gravity casting (as-cast) and die-casting (as-diecast) process have been investigated. For the microstructural characterization, the inductively coupled plasma mass spectrometry (ICP-MS), optical microscope (OM), scanning electron microscope (SEM) and electron probe microanalysis (EPMA) analyses are conducted. For the intermetallic phases, the X-ray diffraction (XRD) and energy dispersive spectroscopy (EDS) are also conducted with quantitative and qualitative analysis. Micro Vickers hardness and static tensile test are achieved in order to measure mechanical properties of alloys. Secondary dendrite arm spacing (SDAS) of as-cast and as-diecast show 37um and 18um, respectively. A large amount of coarsen eutectic Si, $Al_2Cu$ intermetallic phase and Fe-rich phases are identified in the Al-6Si-2Cu alloy. Mechanical properties of gravity casting alloy are much higher than those of die-casting alloy. Especially, yield strength and elongation of gravity casting alloy show 2 times higher than die-casting alloy. After shot peening, shot peening refined the surface grains and Si particles of the alloys by plastic deformation. The surface hardness value shows that shot peening alloy has higher value than unpeening alloy.

• 보존과학연구
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• 통권24호
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• pp.187-213
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• 2003

Sungseonsa Temple site in Chungju city in Chungcheongbuk-doProvince is written in "Goryeosa" as a building for Queen Sinmyeongsunseong, the mother of Gwangjong in AD 954 in Goryeo Dynasty. The museum in Chungcheong University takes charge of the excavation for 3 times from 2000 to 2002 and identified that its construction was carried out till Joseon Dynasty. Among the iron artifacts from the first excavation such as a weeding hoe, a hand knife, a lock, two nails and a plow which had conservation treatments, the sample was collected. Its micro-structure and method of manufacture were investigated. Excavation report for those artifacts has not published yet, therefore, the date of each artifacts is not clearly confirmed. The samples were collected from each part of the objects and then embedded in epoxy resin and etched with nitric acid. The examination of its microstructure is carried out under the microscope and the hardness values were measured by Vickers hardness tester. From the results, some artifacts show different manufacture method sin the each parts. The forming processes of the iron weeding hoe and the iron sickle are similar but the blade of iron weeding hoe was strengthened by carbonization whereas the blade of the iron sickle was done by quenching. The hand knife and the nails were produced through almost same methods and shows similar microstructures. The hand knife seems to be made by repeated beating and folding in low temperature resulting in fine crystallization, but the nail shows large crystallization due to processes in high temperature. Lock is made of white cast iron, that does not show any heat treatment.