• Applied Biological Chemistry
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• v.47 no.1
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• pp.1-16
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• 2004

The purpose of this paper is to review the occurrence, analytical methods and reduction methods of aflatoxins in foods. Aflatoxins are produced by the secondary metabolism of various fungal species and have the highest toxicity among mycotoxins. Due to their toxicity including carcinogenic activity, aflatoxins affect not only the health of humans ana animals but also the economics of agriculture and food. As a food-importing country, because aflatoxins could contaminate raw commodities and foodstuffs, there should be inspection on the exposure and the regulation of risk assessment as a food safety measure. In addition, studies on rapid analytical methods and reduction of toxicity by various processes for aflatoxins should be carried out in conjunction with those of the risk assessment of aflatoxins.

• Proceedings of the Korean Geotechical Society Conference
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• 2006.03a
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• pp.949-959
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• 2006

Despite of the popularity of using empirical methods for support design, empirical rules suffer from the inherent problem of providing no indication of the safety degree of the design. For the support design of large span tunnel, it was considered that the empirical design guidelines should be augmented by more explicit design methods. This paper presents an overview of the analytical support design methodology that is used to refine initial empirical recommendations. The initial support design supplemented by analytical methods is validated by probabilistic and deterministic approach applied to stress-induced and structurally controlled gravity-driven instability problem each. As a result, the extent of the potential failure zone is sorted out and numerical parametric studies were performed to gain insight into the overall behavior of tunnel in the potential failure zone. Concequently, it was decided that additional conservation techniques have to be planed as a reserved support pattern.

• Journal of the Society of Naval Architects of Korea
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• v.57 no.6
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• pp.353-364
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• 2020

This paper presents the semi-analytical ice load calculation methods that are useful to simulate the ice-breaking process. Since the semi-analytical methods rely on the previously developed closed form equations or numerical analysis results, the user's exact understanding for the equations must be supported in order to use the methods properly. In this study, various failure modes of ice such as local crushing, in-plane splitting failure, out-of-plane bending failure and radial or circumferential cracking with rotation of the broken ice floe are considered. Based on the presented methods, the fracture modes were evaluated according to the size and thickness of ice. In addition, time series analysis for the ice-breaking process was performed on several ice conditions and the results were analyzed.

• Nuclear Engineering and Technology
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• v.49 no.3
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• pp.562-568
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• 2017

Background: The chemical characterization of metallic alloys and oxides is conventionally carried out by wet chemical analytical methods and/or instrumental methods. Instrumental neutron activation analysis (INAA) is capable of analyzing samples nondestructively. As a part of a chemical quality control exercise, Zircaloys 2 and 4, nimonic alloy, and zirconium oxide samples were analyzed by two INAA methods. The samples of alloys and oxides were also analyzed by inductively coupled plasma optical emission spectroscopy (ICP-OES) and direct current Arc OES methods, respectively, for quality assurance purposes. The samples are important in various fields including nuclear technology. Methods: Samples were neutron irradiated using nuclear reactors, and the radioactive assay was carried out using high-resolution gamma-ray spectrometry. Major to trace mass fractions were determined using both relative and internal monostandard (IM) NAA methods as well as OES methods. Results: In the case of alloys, compositional analyses as well as concentrations of some trace elements were determined, whereas in the case of zirconium oxides, six trace elements were determined. For method validation, British Chemical Standard (BCS)-certified reference material 310/1 (a nimonic alloy) was analyzed using both relative INAA and IM-NAA methods. Conclusion: The results showed that IM-NAA and relative INAA methods can be used for nondestructive chemical quality control of alloys and oxide samples.

• Geotechnical Engineering
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• v.13 no.3
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• pp.53-62
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• 1997

Analytical studies were conducted to develop the Spectral-Analysis-of-Surface-Waves (SASW) method for underwater use. For the precise estimation of the in-situ soil stiffness profile from SASW measurements, it is essential to determine economical and reasonable theoretical dispersion curves reflecting various experimental conditions. In this paper, therefore, analytical methods are mainly discussed, which were developed to determine theoretical dispersion curves of surface waves propagated along the soil-water interface. Application of the analytical methods is then illustrated by an example involving estimation of a stiffness profile through a forward modeling process of SASW measurements. Applicabilities of the SASW method as well as the developed analytical methods are evaluated, respectively, from the example.

• International Journal of Aeronautical and Space Sciences
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• v.4 no.2
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• pp.17-25
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• 2003

Simple methods are developed to predict temperatures of a satellite box during launch stage. The box is mounted on outer surface of satellite and directly exposed to space thermal environment for the time period from fairing jettison to separation. These simple methods are to solve a 1st order ordinary differential equation (ODE) which is simplified from the governing equation after applying several assumptions. The existence of analytical solution for the 1st order ODE is determined depending on treatment of time-dependent molecular heating term. Even for the case that the analytical solution is not available due to the time dependent term, the 1st order ODE can be solved by relatively simple numerical techniques. The temperature difference between two different approaches (analytical and numerical solutions) is relatively small (Jess than $1^{\circ}C$ along the time line) when they are applied to STSAT-I launch scenario. The present methods can be generally used as tools to quickly check whether a satellite box is safe against space environment during the launch stage for the case that the detailed thermal analysis is not available.

• Progress in Superconductivity and Cryogenics
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• v.20 no.4
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• pp.16-19
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• 2018

This paper presents analytical and numerical simulation approaches on charging characteristics of no-insulation (NI) REBCO pancake coil by using the equivalent circuit model to estimate magnetic performance response in the coil. The analytical methods provide closed form or definite solution in the form of complete mathematical expressions but they are hard to solve the complex problems. Numerical methods have become popular with the development of the computing capabilities to solve the problems which are impossible or very hard to solve analytically. First of all, the equivalent circuit model are proposed to develop the simulation code for both analytical and numerical method. The charging test was performed under critical current to obtain magnetic field induced and terminal voltage through the radial as well as spiral current paths within the coil. To verify the validity of both proposed methods, the simulation results were compared and discussed with the experimental results.

• Structural Engineering and Mechanics
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• v.82 no.3
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• pp.401-416
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• 2022

The aim of this study is to examine the frictionless double receding contact problem for two functionally graded (FG) layers pressed with a uniformly distributed load and resting on a homogeneous half plane (HP) using analytical and numerical methods. The FG layers are made of a non-homogeneous material with an isotropic stress-strain law with exponentially varying properties. It is assumed that the contact at the FG layers and FG layer-HP interface is frictionless. The body force of the FG layers and homogeneous HP are ignored in the study. Firstly, an analytical solution for the contact problem has been realized using the theory of elasticity and the Fourier integral transform techniques. Then, the problem modeled and two-dimensional analysis was carried out by using the ANSYS package program based on FEM. Numerical results for contact lengths and contact pressures between FG layers and FG layer-HP were provided for various dimensionless quantities including material inhomogeneity, distributed load width, the shear module ratio, and the heights of the FG layers for both methods. The results obtained using FEM were compared with the results found using the analytical formulation. It was found that the results obtained from analytical formulation were in perfect agreement with the FEM study.

• Analytical Science and Technology
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• v.23 no.3
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• pp.278-283
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• 2010

This study was performed to compare the analytical results among L2000DX and two GC/ECD methods (rapid and conventional). 15 samples of transformer oils were collected to compare the analytical results. In the analytical results of PCBs-containing transformer oil, the PCBs concentrations were in the range of 4.4 mg/L to 182.8 mg/L with L2000DX, N.D. to 14.63 mg/L with conventional GC/ECD, and N.D. to 13.03 mg/L using rapid GC/ECD. The PCB concentrations detected with the L2000DX showed a large difference to those detected with GC/ECD methods. Otherwise, little difference was shown between the two GC/ECD methods at a concentration range lower than 4 mg/L, although the rapid GC/ECD method tended to detect a slightly lower concentration near the regulation criteria of Korea for 2 mg/L.

• Environmental Analysis Health and Toxicology
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• v.17 no.2
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• pp.95-107
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• 2002

This study was designed to investigate the characteristics of atmospheric concentrations of toxic volatile organic compounds (VOCs) in Korea. Target compounds included 1,3-butadiene, aromatics such as BTEX, and a number of carbonyl compounds. In this paper, as the first part of the study, the performance of sampling and analytical methods was evaluated for the measurement of selected VOCs and carbonyl compounds in the ambient air. VOCs were determined by the adsorbent tube sampling and automatic thermal desorption coupled with GC/MSD analysis, while carbonyls by the DNPH-silica cartridge sampling with HPLC analysis. The methodology was investigated with a wide range of performance criteria such as repeatability, linearity. lower detection limits, collection efficiency, thermal conditioning, breakthrough volume and calibration methods using internal standards. In addition, the sampling and analytical methods established in this study were applied to real field samples duplicately collected in various ambient environments. Precisions for the duplicate samples appeared to be comparable with the performance criteria recommended by USEPA TO-17. The overall precision of the sampling and analytical methods was estimated to be within 20 ∼ 30% for major aromatic VOCs such as BTEX, whereas the precision for major carbonyl compounds such as formaldehyde and acetaldehyde was within 10 ∼ 20% for field samples. This study demonstrated that the adsorbent sampling and thermal desorption method can be reliably applied for the measurement of BTEX in ppb levels frequently occurred in common indoor and ambient environments.