• Title/Summary/Keyword: metallic particle

검색결과 208건 처리시간 0.049초

혼합 전도체 $\beta-LiAl$의 전자구조, 결합과 Li 이온 이동에 따른 영향 (Electronic Structure, Bonding and Kithium Migration Effects of the Mixed Conductor $\beta-LiAl$)

  • Jang, Gun-Eik;I.M Curelaru
    • 한국진공학회지
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    • 제5권3호
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    • pp.194-198
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    • 1996
  • Detailed expermental studies of theelectronic structure of the valence and conduction bands of the mixed conductor $\beta$-LiAlindicate that a quasi-gap opens at the Fermi level, and the conduction states are highlylocalized, as opposed to the theoretical band structure calculations that predict predominant metallic behavior. Evidence for complex lithium migration effects involving the surface of Lial , induced by particle (electron or ion) bombardment and mechanical treatment , has been obtained as a byproduct of these experiments.

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공침법에 의한 MnZn Ferrite 분말제조 연구 (MnZn Ferrite Preparation by Coprecipitation Method)

  • 엄태형;고성만;서동수;양준환;박균하
    • 한국세라믹학회지
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    • 제30권6호
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    • pp.478-484
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    • 1993
  • The influence of reaction conditions on the MnZn ferrite coprecipitation process were investigated using mixed metla sulfate solution and ammonium oxalate. In order to minimize the metallic ion losses and to control the particle size, the optimum reaction conditions were as follows; reaction temperature $25^{\circ}C$, metal sulfate concentration 0.3M, molar ratio of ammonium oxalate/mixed metal sulfate 1.1:1. The production yield was as high as 97.6% of theoretical yield at optimum reaction condition.

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AFM을 이용한 나노 입자의 조립에 관한 연구

  • 박준기;한창수
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2004년도 춘계학술대회 논문요약집
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    • pp.152-152
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    • 2004
  • 카본나노튜브(Carbon Nanotube)는 다른 물질과 구별되는 날카로움(Sharpness), 고세장비(High Aspect Ratio), 높은 기계적 강성(Stiffness), 고탄성(high Elasticity), 그리고 반도체(semi-conducting)와 도체(Metallic) 성질 때문에, 카본나노튜브는 많은 연구에 적용되고 있으며, 카본나노튜브가 부착된 AFM(Atomic Force Microscope) 팁을 이용한 AFM 측정은 CNT 응용에 있어서 매우 큰 효과를 내는 응용분야 중 하나이다. AEM 팁에 카본나노튜브를 붙이는 이전 연구는 대부분 화학증착법(Chemical Vapor Deposition)에 의해 이루어 졌으며, 매우 효과적인 방법이지만 고가의 장비와 고온의 챔버내에서 이루어진다는 문제점을 가지고 있다.(중략)

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분진의 입경분포에 마른 중금속 농도 및 cascade impactor의 효율 (Concentrations of metallic elements and efficiency of cascade impactor by particle size distribution)

  • 김성천;김광석
    • 한국대기환경학회:학술대회논문집
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    • 한국대기환경학회 2002년도 추계학술대회 논문집
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    • pp.296-297
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    • 2002
  • 입자상 오염물질은 공기역학적 직경 2.5$\mu\textrm{m}$를 기준으로 미세입자와 거대입자로 나누어지는 쌍극분포의 형태(Whitby et at., 1972)를 나타내며, 분진이 인체에 미치는 영향에 관한 많은 연구를 통해 10$\mu\textrm{m}$ 이하의 입자가 호흡성 분진으로 인체에 더 유해한 영향을 미치고 있음이 밝혀졌다(Emison, 1988). 이러한 특징은 동일 질량의 분진을 가정할 때 입자의 직결이 작아질수록 저감효율이 떨어지며, 분진의 표면적이 커져 중금속이나 가스상 오염물질의 흡착이 상대적으로 용이해지기 때문이다(Saffiotti, 1965). (중략)

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칼라 패턴인식을 이용한 마모입자 분석 (Wear Debris Analysis using the Color Pattern Recognition)

  • 장래혁;;윤의성;공호성;강기홍
    • 한국윤활학회:학술대회논문집
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    • 한국윤활학회 2000년도 제31회 춘계학술대회
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    • pp.54-61
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    • 2000
  • A method and results of classification of 4 types metallic wear debris were presented by using their color features. The color image of wear debris was used (or the initial data, and the color properties of the debris were specified by HSI color model. Particle was characterized by a set of statistical features derived from the distribution of HSI color model components. The initial feature set was optimized by a principal component analysis, and multidimensional scaling procedure was used for the definition of classification plane. It was found that five features, which include mean values of H and S, median S, skewness of distribution of S and I, allow to distinguish copper based alloys, red and dark iron oxides and steel particles. In this work, a method of probabilistic decision-making of class label assignment was proposed, which was based on the analysis of debris-coordinates distribution in the classification plane. The obtained results demonstrated a good availability for the automated wear particle analysis.

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금속환원법에 의한 바나듐 분말 추출 (Extraction of Vanadium Powder by Metallothermic Reduction)

  • 이동원;허상현;염종택;왕제필
    • 한국분말재료학회지
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    • 제20권1호
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    • pp.43-47
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    • 2013
  • The extraction of metallic pure vanadium powder from raw oxide has been tried by Mg-reduction. In first stage, $V_2O_5$ powders as initial raw material was reduced by hydrogen gas into $V_2O_3$ phase. $V_2O_3$ powder was reduced in next stage by magnesium gas at 1,073K for 24 hours. After reduction reaction, the MgO component mixed with reduced vanadium powder were dissolved and removed fully in 10% HCl solution for 5 hours at room temperature. The oxygen content and particle size of finally produced vanadium powders were 0.84 wt% and 1 ${\mu}m$, respectively

GIS 립 스페이서의 가상스트리머 진전에 따른 전계해석 및 절연특성 (Electric Field Analysis with Imaginary Streamer Process and Insulation Characteristics on the Ribbed Spacer for GIS)

  • 류성식;최영찬;이창용;곽희로
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2001년도 하계학술대회 논문집 C
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    • pp.1649-1651
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    • 2001
  • The effect of ribbed spacers having metallic particle attached to the post-type spacer on dielectric breakdown phenomena has been investigated using electric field analysis for imaginary streamer process and a breakdown experiment. It was described that the electric field analysis and the dielectric breakdown test were performed on the case that the particle was attached to the various position of the ribbed spacer having various shapes. As a result, the breakdown voltage of the spacer with two ribs was highest, and it was varied by the length and the thickness of the rib. Especially, in case of the rib with round edge, the breakdown voltage was higher than that with rectangular edge, which complied with the result through the field analysis.

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화염분무열분해 공정을 이용한 저온 연료전지 연료전극용 탄소담지 Pt-Ru 촉매의 제조 (Synthesis of Carbon-Supported Pt-Ru Catalysts using a Flame Spray Pyrolysis Method for Fuel Electrode of Low Temperature Fuel Cell)

  • 이현민;이동근
    • 한국입자에어로졸학회지
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    • 제8권2호
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    • pp.69-74
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    • 2012
  • This study describes how successfully a conventional flame aerosol synthesis was used to continuously synthesize Pt-Ru catalysts supported by carbon agglomerates. Nearly spherical catalysts produced in the flame were mainly composed of metallic Pt and Ru with the molar ratio of 1:1 and those sizes were controllable from ~1.5 nm to ~2.0 nm. Nevertheless, only Pt peaks were found from X-ray diffraction experiments, suggesting that amorphous-like Ru was well mixed in the crystalline Pt lattices. It was found from Cyclo-voltamograms and CO stripping experiments that the electrochemical properties of the catalysts are at least comparable to that of a conventional commercial sample.

밀양ㆍ창원지역의 PM10 음이온 성분 및 금속성분의 화학적 특성 (Chemical Characteristics of Anian Concentration and Metallic Element of PM10 in the Miryang and Changwon)

  • 서정민;정찬호;최금찬;강신묵
    • 한국대기환경학회:학술대회논문집
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    • 한국대기환경학회 2003년도 추계학술대회 논문집
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    • pp.330-332
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    • 2003
  • 현대 사회는 인구, 산업, 경제, 활동이 도시에 집중되어 발달되고 있으며, 도시에서의 활동증가로 인한 교통량도 급격히 증가하고 있다. 급격히 증가된 인간의 생활환경 변화로 인한 오염물질의 배출도 역시 증가하여 우리의 주변환경을 심각하게 오염시키고 있다. 대기중에 존재하는 에어로졸 입자는 자연발생원에서 직접 대기중에 배출되는 해염입자, 토양입자 등과 같은 1차 입자(Primary particle)와 주로 연소, 소각 등에 의해 인위적으로 발생된 가스상 물질의 대기중에서 다양한 물리ㆍ화학적인 반응을 통해 생성되는 2차입자(Secondary particle)로 크게 구별할 수 있다. (중략)

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액체질소 중에서의 연면방전 특성 (Characteristics of Surface flashover in LN2)

  • 정종만;백승명;김상현
    • 한국전기전자재료학회논문지
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    • 제16권1호
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    • pp.70-76
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    • 2003
  • For the development of superconducting power apparatus, it is necessary to establish the dielectric technology in coolant like L$N_2$. Therefore in this paper we conducted experiment of surface flashover that could occur in the windings of HTS transformer which will be developed in the pancake coil type. First, we distinguished two types of surface flashover by electrode alignment, such as parallel and vertical, and then compared with each characteristics of surface flashover. The flashover voltage was more affected by thickness of spacer than by surface length when the thickness of spacer is over 1 mm. And the surface flashover with metallic particle attached on the spacer was tested, it was affected by the particle position. The more close to the electrodes, the worse the characteristics. Also the experiment was conducted when the electrode was immersed in liquid nitrogen(L$N_2$) partially. The surface flashover characteristics of spacer was, when immersed partially in 50%, rapidly decreased.