• Title/Summary/Keyword: melting centrifugal process

검색결과 28건 처리시간 0.018초

CMP 방법으로 제조한 BSCCO 2212 튜브의 임계전류특성에 미치는 열처리 온도의 영향 (Effects of Heat-treatment Temperature on the Critical Current of BSCCO 2212 Tube Prepared by CMP Method)

  • 최정숙;오성룡;전병혁;김형섭;김혜림;현옥배;김찬중
    • Progress in Superconductivity
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    • 제8권1호
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    • pp.98-103
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    • 2006
  • [$Bi_2Sr_2Ca_1Cu_2O_x$](BSCCO 2212) tubes were fabricated by centrifugal melting process(CMP). BSCCO 2212 powder was melted in a Pt crucible and solidified in a rotating steel mold. The BSCCO 2212 tube samples separated from steel mold were heat-treated at $800^{\circ}C\;and\;810^{\circ}C$ in oxygen flow. The critical current($I_c$) of the samples was measured by transport measurement at 77K, and the microstructure was investigated by scanning electron microscope. The $J_c$ at 77K of the tubes heated treated at $800^{\circ}C\;and\;810^{\circ}C$ were 197 and 240 $A/cm^2$, respectively. It was observed that the plate like grains in BSCCO 2212 tube was more developed in the sample heat treated at $810^{\circ}C\;and\;800^{\circ}C$ heated tube. It is found that the critical current($I_c$) of the BSCCO 2212 sample was dependent on the heating schedule regarding the growth of the BSCCO 2212 grains.

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한류기용 Bi2212 튜브의 특성 (Bi2212 Tube Characteristics for SCFCL)

  • 이남일;장건익;오일성;박권배
    • Progress in Superconductivity
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    • 제7권2호
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    • pp.174-178
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    • 2006
  • For the practical application on SCFCL, Bi2212 tubes were fabricated by Centrifugal Forming Process (CFP) in terms of many different processing parameters. Typical sizes of tubes were 60, 150 mm in length and 2.5, 3.5, 4.8 mm in thickness. Initially powder was melted by induction heating. The optimum range of melting temperatures and preheating temperature were $1100^{\circ}C$ and $500^{\circ}C$ for 30min respectively. The nominal mold rotating speed was around 1000 RPM. A tube was annealed at $840^{\circ}C$ for 80 hours in oxygen atmosphere. The tube of 50mm x 70mm x 2.5mm, rotated with 1000 RPM showed $I_c=890\;A\;and\;T_c=80$. It was found that the tube processed with faster rate of mold rotation speed, thinner tube thickness and shorter tube length shows better electric characteristics as compared with the tube normally processed. In order to study the uniformity heat and fluid flow analysis tool was adopted along tube.

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주조용 TiAl 합금의 조직 미세화를 위한 반복열처리 공정 조건에 관한 연구 (The Effects of Cyclic Heat Treatment Process for Fine Microstructure of TiAl Cast Alloy)

  • 공만식;양현석
    • 열처리공학회지
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    • 제32권5호
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    • pp.195-200
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    • 2019
  • For expanding the applications and workability of TiAl alloy, elongation is very important property. Fine microstructure is needed for elongation and physical properties of TiAl alloys. In this study, The effects of cyclic heat treatment process for fine microstructure of Ti-46Al-Nb-W-Cr-Si-C alloy, which was made by VAR (vacuum arc remelting) and VIM(vacuum induction melting) centrifugal casting process, was investigated. Cycle heat treatment process was very effective for recrystallization of this TiAl system, which has microstructure size of $50{\sim}100{\mu}m$ through pre-heat treatment, cyclic heat treatment in ${\alpha}+{\gamma}$ phase region and solution heat treatment respectively. Refined grain size was finally confirmed by photos of optical microscope and scanning electron microscope.

다이캐스팅형 원심주조기에 대한 충진율·전도율 해석 (Conductivity·Filling Rate Analysis for Die-Casting Centrifugal Casting Machine)

  • 이양창;이준성
    • 한국산학기술학회논문지
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    • 제16권4호
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    • pp.2364-2369
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    • 2015
  • 본 논문에서는 고정밀 로터용 원심주조기 방식을 연구 및 개발함으로써 관련 업종의 생산성 향상을 위하여 로터의 충진율 해석을 통해 RPM에 따른 로터의 충진율을 비교해 최적의 RPM을 제시하였다. 회전속도가 600 rpm일 때 충진율 99.47%를 보여줌으로써 실제 작업현장에서의 결과와 비슷하므로 이를 토대로 추가적으로 수행하여 그 결과를 이용한다면 보다 정확한 공정설계를 할 수 있을 것으로 사료된다. 또한 소형 레이들의 전도율해석을 통하여 고품질의 주조제품이 생산될 수 있도록 적합한 소형 레이들의 온도를 분석하였다. 니크롬선을 이용한 가열장치가 없는 경우는 $427^{\circ}C$까지 급격히 떨어진 상태로 알루미늄용액이 급격히 굳어지기 시작했다. 그러나 니크롬선의 가열장치가 있는 경우에는 알루미늄 용액의 용융온도인 $660^{\circ}C$이상을 유지한 상태에서 작업을 할 수 있었으며 온도변화가 거의 없음을 알 수 있었다.

Transfer characteristics of a lithium chloride-potassium chloride molten salt

  • Mullen, Eve;Harris, Ross;Graham, Dave;Rhodes, Chris;Hodgson, Zara
    • Nuclear Engineering and Technology
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    • 제49권8호
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    • pp.1727-1732
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    • 2017
  • Pyroprocessing is an alternative method of reprocessing spent fuel, usually involving the dissolving spent fuel in a molten salt media. The National Nuclear Laboratory designed, built, and commissioned a molten salt dynamics rig to investigate the transfer characteristics of molten lithium chloride-potassium chloride eutectic salt. The efficacy and flow characteristics of a high-temperature centrifugal pump and argon gas lift were obtained for pumping the molten salt at temperatures up to $500^{\circ}C$. The rig design proved suitable on an industrial scale and transfer methods appropriate for use in future molten salt systems. Corrosion within the rig was managed, and melting techniques were optimized to reduce stresses on the rig. The results obtained improve the understanding of molten salt transport dynamics, materials, and engineering design issues and support the industrialization of molten salts pyroprocessing.

원심 용융 성형공정으로 제조된 BSCCO 튜브의 전기적 특성 (Electronical Property of BSCCO Tube Fabricated by Centrifugal Melting Process)

  • 최정숙;오성룡;전병혁;김혜림;현옥배;김형섭;김찬중
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2006년도 하계학술대회 논문집 Vol.7
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    • pp.267-267
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    • 2006
  • 전력에 큰 손실을 초래하는 고장전류를 차단하기 위한 한류기(FCL) 소재로서 고온 초전도체인 BSCCO 2212가 사용된다. 고온에서 용융된 BSCCO 2212 분말은 원심성형법에 의해 한류기용 튜브로 제조되었다. BSCCO 튜브의 기계적 특성을 높이고 용융온도를 낮추기 위해 $SrSO_4$(10wt-%)를 첨가하였다. 용탕은 $1200^{\circ}C$에서 완전히 용융되어 금속 몰드로 주입되었고 원심성형에 사용되는 금속 몰드는 $550^{\circ}C$ 온도로 2시간 예열 후 1020 ~ 2520 RPM으로 회전시켰다. 원심력에 의해 성형된 BSCCO 튜브는 약 48시간 동안 로에서 서냉 후 금속 몰드로부터 분리하였다. 튜브의 용이한 분리를 위해 이형제로서 BSCCO 2212 powder를 사용하였고 임계전류측정을 고려하여 Ag tape 단자를 튜브 끝단에 부착하였다. BSCCO 제조 공정에 있어서 몰드의 예열온도, 용융온도, 몰드 회전속도 등의 변수를 조절하여 최적의 조건을 확립하였다. 제조한 BSCCO 튜브의 임계전류($I_c$)와 임계전류밀도($J_c$)는 77K에서 536A와 $205A/cm^2$ 이었다. 본 연구에서는 BSCCO 2212 튜브를 제조하는 공정조건 변화와 각 조건에서 제조된 BSCCO 2212 튜브의 전기적 특성 및 그에 따른 분석에 대해 기술하였다.

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치과용 주조 합금의 방전가공에 따른 표면 성분 변화 (Elemental alteration of the surface of dental casting alloys induced by electro discharge machining)

  • 장용철;이명곤
    • 대한치과기공학회지
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    • 제31권1호
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    • pp.55-61
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    • 2009
  • Passive fitting of meso-structure and super-structures is a predominant requirement for the longevity and clinical success of osseointegrated dental implants. However, precision and passive fitting has been unpredictable with conventional methods of casting as well as for corrective techniques. Alternative to conventional techniques, electro discharge machining(EDM) is an advanced method introduced to dental technology to improve the passive fitting of implant prosthesis. In this technique material is removed by melting and vaporization in electric sparks. Regarding the efficacy of EDM, the application of this technique induces severe surface morphological and elemental alterations due to the high temperatures developed during machining, which vary between $10,000{\sim}20,000^{\circ}C$. The aim of this study was to investigate the morphological and elemental alterations induced by EDM process of casting dental gold alloy and non-precious alloy used for the production of implant-supported prosthesis. A conventional clinical dental casting alloys were used for experimental specimens patterns, which were divided in three groups, high fineness gold alloy(Au 75%, HG group), low fineness gold alloy(Au 55%, LG group) and nonprecious metal alloy(Ni-Cr, NP group). The UCLA type plastic abutment patterns were invested with conventional investment material and were cast in a centrifugal casting machine. Castings were sandblasted with $50{\mu}m\;Al_2O_3$. One casting specimen of each group was polished by conventional finishing(HGCON, LGCON, NPCON) and one specimen of each group was subjected to EDM in a system using Cu electrodes, kerosene as dielectric fluid in 10 min for gold alloy and 20 min for Ni-Cr alloy(HGEDM. LGEDM, NOEDM). The surface morphology of all specimens was studied under an energy dispersive X-ray spectrometer (EDS). The quantitative results from EDS analysis are presented on the HGEDM and LGEDM specimens a significant increase in C and Cu concentrations was found after EDM finishing. The different result was documented for C on the NPEDM with a significant uptake of O after EDM finishing, whereas Al, Si showed a significant decrease in their concentrations. EDS analysis showed a serious uptake of C and Cu after the EDM procedure in the alloys studied. The C uptake after the EDM process is a common finding and it is attributed to the decomposition of the dielectric fluid in the plasma column, probably due to the development of extremely high temperatures. The Cu uptake is readily explained from the decomposition of Cu electrodes, something which is also a common finding after the EDM procedure. However, all the aforementioned mechanisms require further research. The clinical implication of these findings is related with the biological and corrosion resistance of surfaces prepared by the EDM process.

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