• Title/Summary/Keyword: melt mixing.

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Wood Fiber-Thermoplastic Fiber Composites by Turbulent Air Mixing Process(II) - Effect of Process Variables on The Mechanical Properties of Composites - (난기류 혼합법을 이용한 목섬유-열가소성 섬유 복합재에 관한 연구(II) - 공정변수가 복합재의 기계적 성질에 미치는 영향 -)

  • Yoon, Hyoung-Un;Lee, Phil-Woo
    • Journal of the Korean Wood Science and Technology
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    • v.25 no.3
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    • pp.58-65
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    • 1997
  • This research was carried out to evaluate the effect of process variables on mechanical properties of the wood fiber-thermoplastic fiber composites by turbulent air mixing method. The turbulent air mixer used in this experiment was specially designed in order to mix wood fiber and thermoplastic polypropylene or nylon 6 fiber, and was highly efficient in the mixing of relatively short plastic fiber and wood fiber in a short time without any trouble. The adequate hot - pressing temperature and time in our experimental condition were $190^{\circ}C$ and 9 minutes in 90% wood fiber - 10% polypropylene fiber composite and $220^{\circ}C$ and 9 minutes in 90% wood fiber 10% nylon 6 fiber composite. Both in the wood fiber - polypropylene fiber composite and wood fiber- nylon 6 fiber composite, the mechanical properties improved with the increase of density. Statistically, the density of composite appeared to function as the most significant factor in mechanical properties. Within the 5~15% composition ratios of polypropylene or nylon 6 fiber to wood fiber, the composition ratio showed no significant effect on the mechanical properties. Bending and tensile strength of composite, however, slightly increased with the increase of synthetic fiber content. The increase of mat moisture content showed no significant improvement of mechanical properties both in wood fiber - polypropylene fiber composite and wood fiber nylon 6 fiber composite. Wood fiber - nylon 6 fiber composite was superior in th mechanical strength to wood fiber-polypropylene fiber composite, which may be related to higher melt flow index of nylon 6 fiber(22g/10min) than of polypropylene fiber(4.3g/10min).

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Experimental Study for Keeping a Melting Pool in a Waste Pyrolysis Melting Incinerator (폐기물 열분해 용융소각로의 용탕 유지를 위한 실험적 연구)

  • Kim, Bong-Keun;Park, Ju-Won;Yu, Tae-U;Yang, Won;Jeun, Keum-Ha
    • 한국연소학회:학술대회논문집
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    • 2006.10a
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    • pp.151-155
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    • 2006
  • The large amount of energy is consumed in a process for keeping the high temperature melting pool. For this reason, in addition to the wastes input to keep the high temperature melting pool, it is necessary for an auxiliary fuel and LOx to throw into the melting pool. So in this study, using a new melting furnace system, the experiments to keep the melting pool with minimal energy without throwing an auxiliary fuel and LOx was carried out. Also it is hoped that the results of the experiment will be available to analyze keeping a melting pool and behavior in a melting furnace.

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Preparation and Mechanical Properties of SBS/Clay Nanocomposites (SBS/Clay나노복합체의 제조 및 기계적 특성)

  • Choi, Hyun-Kuk;Park, Se-Hyeong
    • Journal of the Korean Society of Industry Convergence
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    • v.17 no.1
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    • pp.1-6
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    • 2014
  • Styrene-butadiene-styrene copolymer(SBS)/Clay nanocomposites were prepared by melt mixing method with organic clay modified with dimethyl dihydrogenated-tallow amine(Cloisite 15A) and methyl tallow bis (2-hydroxy-ethyl) amine(Cloisite 30A), respectively. From the results of XRD, we found that mono layered silicates were dispersed in SBS matrix and they were exfoliated nanocomposites. Mechanical properties of exfoliated SBS nanocomposites were more improvedl than those of SBS. Especially, it was found that the addition of small amount of organoclay was enough to improve mechanical properties without increasing hardness.

Transesterification and Compatibilization in the Blends of Bisphenol-A Polycarbonate and Poly(trimethylene terephthalate)

  • Na Sang-Kuwon;Kong Byeong-Gi;Choi Changyong;Jang Mi-Kyeong;Nah Jae-Woon;Kim Jung-Gyu;Jo Byung-Wook
    • Macromolecular Research
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    • v.13 no.2
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    • pp.88-95
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    • 2005
  • Melt blending of Bisphenol A polycarbonate (PC) and poly(trimethylene terephthalate) (PTT) was carried out over the entire composition range. The mixing time was varied up to 90 min. The resulting samples were analyzed by FT-IR, DSC, XRD, DMTA, $^{1}H NMR$, and SEM. The process of transesterification between the two polymers and their resulting compatibilization were observed. The behaviors of the PTT-rich and PC-rich blends were different and an equilibrium was found to exist. Peculiar behavior, which was different from that of the PTT-rich and PC-rich blends, was exhibited by the 50/50 (PTT/PC) blend.

Rheological characterization of nanoparticle filled polymeric systems

  • Kim, Byoung-Chul;Chae, Dong-Wook
    • Proceedings of the Polymer Society of Korea Conference
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    • 2006.10a
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    • pp.219-219
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    • 2006
  • This study focuses on the effects of dispersion method of a nanoparticle in a polymer matrix such as melt mixing, solution blending, and in-situ polymerization on the physical properties of the nanocomposites. Introduction of a nanoparticle to a polymer resulted in some unusual physical properties. In some cases the nanoparticle played a role of a nucleating agent, leading to decreasing induction time to crystallization. In addition, the dispersion state of the nanoparticle in the polymer matrix also had a significant influence on the physical properties of the nanocomposites. Hence the method of introducing the nanoparticle to the polymer made contribution to the rheological properties of the nanocomposite systems.

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Characteristics of BSCCO Superconductor Tube Using Partial Melting Process (부분용융법을 이용한 BSCCO 초전도 튜브 특성)

  • 박용민;장건익
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2001.02a
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    • pp.25-28
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    • 2001
  • Bi-2212 HTS tube was fabricated by centrifugal forming process(CFP). As a variation of melt casting process(MCP) or centrifugal casting technique, the centrifugal forming process is a flexible method for manufacturing Bi-2212 bulk tubes and has been optimized to achieve smooth surface and uniform thickness. At this process, the slurry was prepared in the mixing ratio of 10:1 between Bi-2212 powder and binder and initially charged into the rotating mold under the speed of 300~450 rpm Heat-treatment was performed at the temperature ranges of 860 ~ $890^{\circ}C$ in air for partial melting. The HTS tube fabricated by centrifugal forming process at $890^{\circ}C$ under the rotating speed of 450 rpm was highly densified and the plate-like grains with more than 20$\mu$m were well oriented along the rotating axis. The measured Tc and Jc at 10K were around 85K and 3,000A/cm2 respectively.

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Fabrication of Bi2212 superconductor by Centrifugal Forming Process (원심 성형법에 의한 고온초전도체 제조)

  • 정승호;장건익
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07a
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    • pp.503-506
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    • 2002
  • BSCCO 2212 HTS was fabricated by CFP(centrifugal forming process). The powder was initially ground in the mixing ratio of 2:2::1:2 with 10% of SrSO$_4$. The temperature increased up to 1035$^{\circ}C$ and 1200$^{\circ}C$ for melting. The melt was poured into the preheated and rotating copper mould from 200 to 600$^{\circ}C$. The specimen was not broken by thermal impact when the melting temperature was over 1050$^{\circ}C$ and copper mould was preheated over 400$^{\circ}C$ for 30min. A tube type of specimen was annealed at 840$^{\circ}C$ or 860$^{\circ}C$ in oxygen atmosphere for 24hours. Typical microstructure was analyzed in terms of CFP parameters by XRD, SEM, and EDS and also superconducting characteristics were compared.

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Effect of CNT Diameter on Physical Properties of Styrene-Butadiene Rubber Nanocomposites

  • Park, Young-Soo;Huh, Mong-Young;Kang, Sin-Jae;Yun, Seok-Il;Ahn, Kay-Hyeok
    • Carbon letters
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    • v.10 no.4
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    • pp.320-324
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    • 2009
  • We investigated the effect of diameter and content of carbon nanotubes (CNTs) on the physical properties of styrenebutadiene rubber (SBR)/CNTs nanocomposites. CNTs-reinforced SBR nanocomposites were prepared by the melt mixing process. CNTs with different diameters were synthesized by the chemical vapor deposition method (CVD). In this work, the mechanical property and other physical properties of SBR/CNTS nanocomposites were discussed as a function of the content and diameter of CNTs.

A Study on the Dispersion of Multi-walled Nanotube of MWNT/PMMA Nanocomposites (MWNT/PMMA 나노복합재료 제작시 MWNT의 분산에 관한 연구)

  • 김현철;이상의;김천곤;이정주
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2003.10a
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    • pp.29-32
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    • 2003
  • Multi -walled carbon nanotube(MWNT)/poly(methyl methacrylate) composites were fabricate d through film casting. Manufacturing process was established using a ultrasonic cleaner and a homogenizer. Acetone was used as a solvent to melt PMMA and mix with MWNT. The ultrasonic cleaner performed an important role in producing MWNT/MMA nanocomposites. Ultrasonic energy was utilized to disperse MWNT in acetone. Also, melting PMMA in acetone and mixing MWNT and PMMA were achieved using the homogenizer. It was confirmed that the nanohlbes were well dispersed in PMMA according to SEM images.

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Effects of the Interaction between Intercalant and Matrix Polymer in Preparation of Clay-dispersed Nanocomposite

  • Ko, Moon-Bae;Kim, Jyunkyung;Choe, Chul-Rim
    • Macromolecular Research
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    • v.8 no.3
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    • pp.120-124
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    • 2000
  • Clay-dispersed nanocomposites have been prepared by simple melt-mixing of two components, styrenic polymers with different content of functional groups and two different organophilic clays (Cloisite(R) 25A and Cloisite(R)30A) with a twin screw extruder. Dispersibility of 10-$\AA$-thick silicate layers of clay in the hybrid was investigated by using an X-ray diffraction method and a transmission electron microscope. It was found that if the interaction force between intercalant and matrix polymer is attractive, the matrix polymer intercalates more rapidly into the gallery of silicate layers. The faster intercalation of matrix polymer leads to the better dispersibility of silicate layers in the matrix polymer.

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