• Title/Summary/Keyword: mechanical characterization

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A study on the Synthesis and Characterization of Polyimide/TiO2 Nanocomposite (폴리이미드/TiO2 나노복합재의 합성과 물성 연구)

  • Lee, Bong-Shin;Lee, Joong-Hee;Kim, In-Taek;Lee, Myong-Hoon;Nah, Chang-Woon
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.12
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    • pp.2624-2630
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    • 2002
  • Organic/inorganic hybrid materials have rapidly become a fascinating research field. In this study, $polyimide/TiO_2$ composites were synthesized from nano-sized anatase $TiO_2$ and two types of polyimide, that is, BPDA-PPD and PMDA-ODA. Nano-sized $TiO_2$ particles were prepared from $TiOEt_4$ solution by the sol-gel method. The synthesized PI/$TiO_2$ composites were characterized by using XRD, TGA, FT-IR, TEM, and Atomic Force Microscope(AFM). $TiO_2$ particles were dispersed well in polyimides and the mechanical and thermal stability of polyimide was improved with $TiO_2$ nano particles.

Characterization of Polyolefin Bumper Recycled by Chemical Removal Method using Electronic Speckle Pattern Interferometry (화학적 박리방법과 ESPI에 의한 재생된 폴리올레핀 범퍼수지의 물성평가)

  • 김현경;강기수;김경석;홍진후
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1997.10a
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    • pp.295-298
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    • 1997
  • Recycl ing of PP/EPR based bumper coated with polyester urethane paint has been per formed by chemical decoating method. Electronic Speckle Pattern Interferometry (ESP11 has been applied to characterize the deformation of polyolef in based bumper. In additon, physical properties and processability of recycled materials have been investigated by dynamic mechanical thermal analysis, impact test and melt flower index measurement. The results show that the deformation ratio of recycled material is higher than that of virgin one. The morphological change of EPR, degree of distribution and dispersion during the recycling process seem to be the most important factor for the deformation and the mechanical properties of recycled materials. The experimental results obtained show that ESPI is very powerful technique to study the thermal mechanical property of polyolefin bumper system.

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Fabrication and Strength Properties of LPS-SiC based materials

  • Lee, Sang-Pill;Kohyama, Akira
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2006.11a
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    • pp.25-28
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    • 2006
  • This paper dealt with the LPS process for the development of high performance SiC materials, based on the detailed analysis of their microstructure and mechanical properties. The submicron SiC powder was used for the fabrication of LPS-SiC materials. A mixture of $Al_2O_3$ and $Y_2O_3$ particles was also used as a sintering additive in the LPS process. LPS-SiC materials were fabricated at different temperatures, using various additive composition ratio ($Al_2O_3/Y_2O_3$). The total amount of additive materials ($Al_2O_3+Y_2O_3$) was fixed as 10 wt%. The characterization Of LPS-SiC materials was investigated by means of SEM, XRD and three point bending test. The LPS-SiC material represented a relative density of about 98 % and a flexural strength of about 800MPa, when it was fabricated at the temperature of $1820^{\circ}C$ and the additive compositional ratio of 1.5.

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A study on the prediction of the mechanical properties of nanoparticulate composites using homogenization method with effect interface concept (유효계면 모델과 균질화 기법을 이용한 나노입자 복합재의 역학적 물성 예측에 관한 연구)

  • Jang, Seong-Min;Yang, Seung-Hwa;Yu, Su-Young;Cho, Maeng-Hyo
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.684-689
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    • 2008
  • In this study, homogenization method combined with the effective interface model for the characterization of properties of the nanoparticulate composites is developed. In order to characterize particle size effect of nanocomposites, effective interface model has been developed. The application range of analytical micromechanics approach is limited because a simple analytical approach is valid only for simple and uniform geometry of fiber particles. Therefore this study focuses on the analysis of mechanical properties of the effect interface through the continuum homogenization method instead of using analytical micromechanics approach. Using the homogenization method, elastic stiffness properties of the effective interface are numerically evaluated and compared with the analytically obtained micromechanics solutions. The suggested homogenization method is expected to be applied to optimization problems for nanocomposite design.

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Evaluation of Mechanical Characteristic of Laser-Welded Blank of a Boron Steel by Using Laser Ablation of Al-Si Coating Layer (Al-Si 코팅층 Laser Ablation 변수에 의한 LWB 보론강판의 기계적 특성 평가)

  • Moon, J.H.;Lee, M.S.;Kang, C.G.
    • Transactions of Materials Processing
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    • v.20 no.8
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    • pp.540-547
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    • 2011
  • Recent years have seen advent of hot stamped parts made from laser-welded blanks of boron steels for structures requiring high crash energy absorption. However, the presence of Al-Si coating interfered with satisfactory mechanical characterizations after laser butt welding. In this study, laser ablation technology was considered in order to facilitate adequate mechanical characterization of the final hot-stamped panels.

Nondestructive Characterization of Materials Using Laser-Generated Ultrasound

  • Park, Sang-Woo;Lee, Joon-Hyun
    • International Journal of Reliability and Applications
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    • v.5 no.1
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    • pp.1-13
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    • 2004
  • It is recently well recognized that the technique for the one-sided stress wave velocity measurement in structural materials provides measurement in structural materials provides valuable information on the state of the material such as quality, uniformity, location of cracked or damaged area. This technique is especially effective to measure velocities of longitudinal and Rayleigh waves when access to only one surface of structure is possible. However, one of problems for one-sided stress wave velocity measurement is to get consistent and reliable source for the generation of elastic wave. In this study, the laser based surface elastic wave was used to provide consistent and reliable source for the generation of elastic wave into the materials. The velocities of creeping wave and Rayleigh wave in materials were measured by the one-sided technique using laser based surface elastic wave. These wave velocities were compared with bulk wave velocities such as longitudinal wave and shear wave velocities to certify accuracy of measurement. In addition, the mechanical properties such as poisson's ratio and specific modulus(E/p) were calculated with the velocities of surface elastic waves.

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Mechanical Stability of Pixel-Isolated Liquid Crystal Mode in Flexible Display

  • Jung, Jong-Wook;Jin, Min-Young;Kim, Hak-Rin;Kim, Jae-Hoon
    • 한국정보디스플레이학회:학술대회논문집
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    • 2005.07a
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    • pp.353-356
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    • 2005
  • We have characterized the mechanical stability of the Pixel-Isolated Liquid Crystal (PILC) mode for plastic LC display applications. In our device, the LC molecules are fully isolated in the pixels by the phase-separated polymer walls. The experimental results of microscopic observation and electro-optic characterization show that our flexible PILC device has good mechanical stability against external point pressure or bending distortion due to the polymer walls in our structure.

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A finite element-experimental study of the impact of spheres on aluminium thin plates

  • Micheli, Giancarlo B.;Driemeier, Larissa;Alves, Marcilio
    • Structural Engineering and Mechanics
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    • v.55 no.2
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    • pp.263-280
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    • 2015
  • This paper describes a study of the collision of hard steel spheres against aluminium thin circular plates at speeds up to 140 m/s. The tests were monitored by a high speed camera and a chronoscope, which allowed the determination of the ballistic limit and the plate deformation pattern. Quasi-static material parameters were obtained from tests on a universal testing machine and dynamic mechanical characterization of two aluminium alloys were conducted in a split Hopkinson pressure bar. Using a damage model, the perforation of the plates was simulated by finite element analysis. Axisymmetric, shell and solid elements were employed with various parameters of the numerical analysis being thoroughly discussed, in special, the dynamic model parameters. A good agreement between experiments and the numerical analysis was obtained.

Synthesis and Characterization of a Novel Silicon-Containing Epoxy Resin

  • Park Soo-Jin;Jin Fan-Long;Lee Jae-Rock
    • Macromolecular Research
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    • v.13 no.1
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    • pp.8-13
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    • 2005
  • A novel silicon-containing epoxy resin, the diglycidylether of bisphenol A-silicon (DGEBA-Si), was synthesized and characterized. The properties of the DGEBA-Si epoxy resin cured with 4,4-diaminodiphenyl methane (DDM), including its cure behavior, glass transition temperature, thermal stability, and mechanical strength were investigated. The char yield of the DGEBA-Si/DDM system was higher than that of a commercial DGEBA/DDM system, indicating that the DGEBA-Si epoxy resin showed good flame-retardance. The cured DGEBA-Si/DDM specimens possessed lower glass transition temperatures and higher mechanical properties than DGEBA/DDM specimens. These features were attributed to the introduction of siloxane groups into the main chain of the epoxy resin, which resulted in the improved flexibility of the cured DGEBA-Si/DDM system.

Effects of Composition and Additives on the Mechanical Characteristics of 3Y-TZP (3Y-TZP의 기계적 특성에 미치는 산화물 조성 및 첨가제의 영향)

  • Park, Mi-Jung;Yang, Seong-Koo;Kang, Jong-Bong
    • Journal of the Korean Ceramic Society
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    • v.43 no.10 s.293
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    • pp.640-645
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    • 2006
  • Monoclinic zirconia and yttria were mixed with a stoichiometric composition of 3Y-TZP (3 mol% Yttria-stabilized Tetragonal Zirconia Polycrystal). The specimen was sintered at 1350$\sim$1450$^{\circ}C$ and mechanical characterization and microstructure analysis were conducted. Microhardness and fracture toughness were shown as 1357.4 Hv and 8.56 MPa $m^{1/2}$. respectively. Without alumina, they were 1311 Hv and 10.02 MPa $m^{1/2}$ respectively. By mixing two different oxides, it was possible to obtain high values of microhardness and fracture toughness. It was possible that was turned out nano-scale particle using the co-milling of high mechanical energy.