• 한국동물위생학회지
• /
• 제28권3호
• /
• pp.285-294
• /
• 2005

This study was conducted to investigate the extraction method for the determination of organochlorine, organophosphorus and synthetic pyrethroid pesticide residues in beef fat by gas chromatography-mass selective detector(GC-MSD). Twenty one pesticide residues in fat were determined using a simple and rapid procedure based on solid- phase extraction(SPE) clean-up cartridges with octadecyl $(C_{18})-bonded$ porous silica, florisil, $10\%$ deactivated florisil. a tandem $C_{18}$ and florisil and a tandem $C_{18}$ and $10\%$ deactivated florisil. Solvent-solvent extraction using acetonitrile was not satisfied to eliminate fat interference for pesticide residue analysis by GC-MSD, and the recoveries of the method in fat ranged from 16.2 to $57.3\%$ except DDT$(83.2\%)$. The recoveries of SPE methods using a tandem $C_{18}$ and Florisil was $59.6\~123.8\%$ except fenitrothion $(135.2\%)$. the SPE method was verified the satisfactory performance of pre-treatment for pesticide residues analysis in fat by GC-MSD. The efficiency of florisil deactivated with $10\%$ water has been not proved significantly on recoveries of pesticide residues in fat.

• 수완나부미
• /
• 제14권1호
• /
• pp.161-189
• /
• 2022

Nguyễn Nhật Ánh and Yoshimoto Banana are authors from two different literary movements, cultures, and countries. Their works are all best-sellers and have received many prestigious awards. Comparing their works from the perspective of shoujo manga, we can see that there are many similarities between them. Regarding the concept of composition, they all want to create works that are accessible to the majority of the public. Therefore, they choose topics which are close and attractive to mass readers as well as simple style, characters, literary devices, artistic space and time that are famous in shoujo - a popular art form of Japan. However, the ideological content in the works of both is not explicit and simple, but expresses the eternal feelings and values of humanity such as love for people, love for the homeland, country, reflecting the depths of both the conscious and the subconscious as well as profound aesthetic and philosophical values, profound aesthetic and philosophical values. Their works present the trend of interference between popular culture and elite literature. We can draw lessons for young writers, cultural managers and a wide audience from the success of these two writers.

• 분석과학
• /
• 제37권4호
• /
• pp.230-238
• /
• 2024

This study evaluates a method for quantifying selenium (Se) concentration in soil using inductively coupled plasma mass spectrometry (ICP-MS), with oxygen as a reaction gas. This approach addresses the challenge of detecting low levels of Se in complex soil matrices and aims to effectively minimize interference problems typically associated with argon plasma in traditional ICP-MS analyses. The analytical method utilizes conditions optimized for minimizing spectral interference and were validated by linearity, accuracy, precision, limit of detection (LOD), and limit of quantification (LOQ). The method demonstrated good linearity, high accuracy (90-97 %), and remarkable sensitivity, achieving detection and quantification limits of 0.15 ㎍/kg and 0.44 ㎍/kg, respectively. Developed analysis method for Se in soil was applied to field samples in the different regions of South Korea and Se concentration ranged from 0.11 to 0.52 mg/kg. Correlation analysis between Se concentration and soil properties showed that Se concentration was significantly correlated with cation exchange capacity (CEC) and available phosphorus among other soil properties.

• 한국인터넷방송통신학회논문지
• /
• 제11권3호
• /
• pp.107-113
• /
• 2011

본 논문은 기존 CMA (Constant Modulus Algorithm) 적응 등화기의 성능인 수렴 특성과 잔류 부호간 간섭을 개선하기위하여 Coordinate Reduction을 적용한 CR(Coordinate Reduction)-CMA에대한 관한 것이다. 송신 시스템과 수신 시스템을 연결하는 무선과 유선의 대역 제한 채널에서 발생되는 부호간 간섭에의한 찌그러짐을 줄이기 위하여 등화기가 사용되며, 이의 대표적인 알고리즘으로는 CMA가 널리 알려져 있다. 이와같은 채널을 통하여 대량의 정보를 고속으로 전송하기 위해서는 등화에 필요한 오버헤드를 최소화할 수 있는 빠른 수렴 속도가 요구된다. 논문에서는 등화기 입력단에서 정상 등화 상태에서 오차를 주이는 수신 신호의 Coordinate를 reduce하는 새로운 비용 함수를 도입하였다. 컴퓨터 시뮬레이션을 통하여 제안한 알고리즘이 기존 CMA 보다 빠른 수렴 속도와 적은 잔류 부호간 간섭양을 가짐을 확인할 수 있었다.

• 한국인터넷방송통신학회논문지
• /
• 제11권6호
• /
• pp.41-47
• /
• 2011

본 논문은 기존 CMA(Constant Modulus Algorithm) 적응 등화기의 성능인 수렴 특성과 잔류 부호 간 간섭을 개선하기 위하여 가중치 벡터의 업데이트를 이중으로 적용한 DW-MCMA(Dual Weight vector Modified Constant Modulus Algorithm)에 대한 관한 것이다. 송신 시스템과 수신 시스템을 연결하는 무선과 유선의 대역 제한 채널에서 발생되는 부호간 간섭에 의한 찌그러짐을 줄이기 위하여 등화기가 사용되며, 이의 대표적인 알고리즘으로는 CMA가 널리 알려져 있다. 이와 같은 채널을 통하여 대량의 정보를 고속으로 전송하기 위해서는 등화에 필요한 오버헤드를 최소화할 수 있는 빠른 수렴 속도가 요구된다. 논문에서는 컴퓨터 시뮬레이션을 통하여 기존 CMA와 MCMA보다 등화기 입력단에서 정상 등화 상태의 오차를 줄일 수 있는 새로운 비용함수와 가중치 벡터를 이중으로 적용하는 제안 방식인 DW-MCMA가 잔류 부호간 간섭량과 빠른 속도를 가짐을 확인하였다.

• Nuclear Engineering and Technology
• /
• 제54권12호
• /
• pp.4636-4643
• /
• 2022

A time-of-flight and energy (TOF-E) detection system for the measurement of ²³⁶U accelerator mass spectrometry (AMS) has been developed to improve the ²³⁶U/²³⁸U sensitivity at Micro Analysis Laboratory, Tandem accelerator (MALT), The University of Tokyo. With observing TOF distribution of ²³⁵U, ²³⁶U and ²³⁸U, this TOF-E detection system has clearly separated ²³⁶U from the interference of ²³⁵U and ²³⁸U when measuring three kinds of uranium standards. In addition, we have developed a novel method combining kernel-based density estimation method and multi-Gaussian fitting method to estimate the ²³⁶U/²³⁸U sensitivity of the TOF-E detection system. Using this new estimation method, 3.4 × 10^-12 of ²³⁶U/²³⁸U sensitivity and 1.9 ns of time resolution are obtained. ²³⁶U/²³⁸U sensitivity of TOF-E detection system has improved two orders of magnitude better than that of previous gas ionization chamber. Moreover, unknown species other than uranium isotopes were also observed in the measurement of a surface soil sample, which has demonstrated that TOF-E detection system has a higher sensitivity in particle identification. With its high sensibility in mass determination, this TOF-E detection system could also be used in other heavy isotope AMS.

• 전자공학회논문지T
• /
• 제36T권3호
• /
• pp.64-71
• /
• 1999

본 논문에서는 DD(Direct-drive)의 기구로서 2자유도 평행링크 기구를 사용하였다. 평행링크 기구는 2개의 모터가 각각 기저부에 설치되어 있기 때문에 모터 자체의 질량이 다른 모터에 부하가 되지 않고, 링크의 수는 증가하지만 arm의 질량이 가볍게 되어, 링크 파라미터의 설정에 의하여 원심력 등의 비선형력이 없어지며 동시에 모터사이의 비간섭화를 실현할 수 있다. 그리고 평행링크 DD로븟 매니퓰레이터의 고정도 운전의 실현을 위하여 신경회로망을 이용한 학습제어계를 설계하여 학습속도의 개선과 함께 변화한 작업대상에의 적응력을 개선하기 위하여 신경회로망과 피드백제어기로 학습제어 알고리즘을 구성한다.

• 한국정밀공학회지
• /
• 제26권1호
• /
• pp.89-96
• /
• 2009

This paper describes the intelligent robot's hand with three finger sensors for a humanoid robot. In order to grasp an unknown object safely, the intelligent robot's hand should measure the mass of the object, and determine the grasping force using the mass, finally control the grasping force using the finger sensors and the controller. In this paper, the intelligent robot's hand for a humanoid robot was developed. First, the six-axis force/moment sensor was manufactured. second, three finger force sensors were designed and fabricated, third, the high-speed controller was manufactured using DSP(digital signal processor), finally, the characteristic test for determining a grasping force and for grasping an unknown object safely It is confirmed that the hand could grasp an unknown object safely.

• 한국위성정보통신학회논문지
• /
• 제12권2호
• /
• pp.71-78
• /
• 2017

망 중립성은 ISP가 이용자에게 비차별성, 상호접속성, 접근성을 보장하여 누구든지 통제나 간섭 없이 동등한 서비스를 받을 수 있도록 하는 개념이다. 그러나 현재 인터넷 망은 P2P 서비스 확산과 실시간 대용량 비디오 스트리밍 서비스와 같이 버퍼링에 민감한 서비스에서 트래픽이 급증하고 있다. 이를 관리하기 위해 ISP가 서비스를 간섭, 변경, 통제하는 등 망 중립성을 훼손하면서, 망 중립성에 대한 논쟁이 끊임없이 발생하고 있다. 따라서 본 논문에서는 망 중립성의 원칙과 개념, 이에 대한 국내외의 입법 정책현황을 비교 분석하고, 이를 기반으로 국내 망 중립성 가이드라인의 쟁점사항과 개선방안을 제시한다.

• 분석과학
• /
• 제32권3호
• /
• pp.88-95
• /
• 2019

This study was conducted to establish the analytical method for the determination of cyanide in blood, urine, lung and skin tissues in rats. In order to detect or quantify the sodium cyanide in above biological matrixes, it was derivatized to Pentafluorobenzyl cyanide (PFB-CN) using pentafluorobenzyl bromide (PFB-Br) and then reaction substance was analyzed using gas chromatography mass spectrometer (GC/MS)-SIM (selected ion monitoring) mode. The analytical method for cyanide determination was validated with respect to parameters such as selectivity, system suitability, linearity, accuracy and precision. No interference peak was observed for the determination of cyanide in blank samples, zero samples and lower limit of quantification (LLOQ) samples. The lowest limit detection (LOD) for cyanide was $10{\mu}M$. The linear dynamic range was from 10 to $200{\mu}M$ for cyanide with correlation coefficients higher than 0.99. For quality control samples at four different concentrations including LLOQ that were analyzed in quintuplicate, on six separate occasions, the accuracy and precision range from -14.1 % to 14.5% and 2.7 % to 18.3 %, respectively. The GC/MS-based method of analysis established in this study could be applied to the toxicokinetic study of cyanide on biological matrix substrates such as blood, urine, lung and skin tissues.