• Journal of the Korean Society for Heat Treatment
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• v.5 no.3
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• pp.179-185
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• 1992

The shape memory effect results from the martensite transfomation of each individual grain. Thus it is necessary to study the texture and its variation. In this study the change of texture during thermal cycling and it's effect on shape memory ability are investigated. The major component of the rolling texture in the parent phase is identified (001) [110], and minor components are (112) [110], (111) [112], {hkl}<100> fiber texture is developed at $45^{\circ}$ from rolling direction. In the case of martensite phase, it is estimated that the major component is (011) [100] and the minor components are (105) [501], (010) [101] and (100) [001]. According to thermal cycling. severity of texture, especially (001) [110] component in parent phase and (011) [100] component in martensite phase are increased. The shape memory ability is increased with increase of thermal cycles and also increased as the direction of specimen approach to $45^{\circ}$ from rolling direction. After first thermal cycling the temperature of transformation can be define clearly and Ms and As are raised by thermal cycling.

• Journal of the Korean Society for Heat Treatment
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• v.3 no.2
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• pp.20-31
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• 1990

This investigation has been carried out to make clear the effect of deformation temperature, strain rate and grain size on the tensile properties of 304L stainless steel. Tensile properties of the metastable austenitic 304L steel remarkably influenced by deformation temperature. Tensile strength increased with decreasing deformation temperature and the elongation showed maximum value near $40^{\circ}C$. In order to obtain the high elongation, a large amount of deformation is available in austenite before martensitic transformation and the martensite has to be induced gradually. Tensile strength and elongation increased with decreasing grain size. The temperature representing the maximum elongation shifted to low temperature and the peak width of elongation became broaden with decreasing austenite grain size. The volume fraction of strain induced martensite decreased with decreasing austenite grain size. As the strain rate increase, the temperature representing the maximum elongation value shifted to high temperature and volume fraction of strain induced martensite decreased.

• Journal of Powder Materials
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• v.29 no.6
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• pp.517-522
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• 2022

We investigate the austenite stability in nanocrystalline Fe-7%Mn-X%Mo (X = 0, 1, and 2) alloys fabricated by spark plasma sintering. Mo is known as a ferrite stabilizing element, whereas Mn is an austenite stabilizing element, and many studies have focused on the effect of Mn addition on austenite stability. Herein, the volume fraction of austenite in nanocrystalline Fe-7%Mn alloys with different Mo contents is measured using X-ray diffraction. Using a disk compressive test, austenite in Fe-Mn-Mo alloys is confirmed to transform into strain-induced martensite during plastic deformation by a disk d. The variation in austenite stability in response to the addition of Mo is quantitatively evaluated by comparing the k-parameters of the kinetic equation for the strain-induced martensite transformation.

• Journal of Powder Materials
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• v.6 no.4
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• pp.270-276
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• 1999

Ti-Ni-Cu alloy powders were fabricated by ball milling, and the properties of these powders were characterized. Mixed 50Ti-(50-x)Ni-xCu powders of 5 to 10at.%Cu composition were milled for 100 hours using SUS 1/4" balls in argon atmosphere. Ball to powder ratio was 20:1 and rotating speed was 100 rpm. Tensile strength, microstructure and phase transformation of ball milled Ti-(50-x)Ni-xCu powders were studied. After 100 hours milling, Ti, Ni and Cu elements were alloyed completely and an amorphous phase was formed. Amorphous phase was crystallized to martensite(B 19') and austenite(B2) after heat treatment for 1 hour at $850^{\circ}C$. As the Cu contents were increased, tensile strength of extruded 6061Al/TiNiCu was decreased, and B19'martensite phases In the TiNi particles were the causes of high tensile stress of extruded 6061Al/TiNiCu.NiCu.

• Archives of Metallurgy and Materials
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• v.67 no.4
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• pp.1491-1495
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• 2022

The present research deals with the effect of pre-strain on the hydrogen embrittlement behavior of intercritically annealed medium-Mn steels. A slow strain-rate tensile test was conducted after hydrogen charging by an electrochemical permeation method. Based on EBSD and XRD analysis results, the microstructure was composed of martensite and retained austenite of which fraction increased with an increase in the intercritical annealing temperature. The tensile test results showed that the steel with a higher fraction of retained austenite had relatively high hydrogen embrittlement resistance because the retained austenite acts as an irreversible hydrogen trap site. As the amount of pre-strain was increased, the hydrogen embrittlement resistance decreased notably due to an increase in the dislocation density and strain-induced martensite transformation.

• Korean Journal of Materials Research
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• v.23 no.9
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• pp.525-530
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• 2013

This study investigated the continuous cooling transformation, microstructure, and mechanical properties of highstrength low-alloy steels containing B and Cu. Continuous cooling transformation diagrams under non-deformed and deformed conditions were constructed by means of dilatometry, metallographic methods, and hardness data. Based on the continuous cooling transformation behaviors, six kinds of steel specimens with different B and Cu contents were fabricated by a thermomechanical control process comprising controlled rolling and accelerated cooling. Then, tensile and Charpy impact tests were conducted to examine the correlation of the microstructure with mechanical properties. Deformation in the austenite region promoted the formation of quasi-polygonal ferrite and granular bainite with a significant increase in transformation start temperatures. The mechanical test results indicate that the B-added steel specimens had higher strength and lower upper-shelf energy than the B-free steel specimens without deterioration in low-temperature toughness because their microstructures were mostly composed of lower bainite and lath martensite with a small amount of degenerate upper bainite. On the other hand, the increase of Cu content from 0.5 wt.% to 1.5 wt.% noticeably increased yield and tensile strengths by 100 MPa without loss of ductility, which may be attributed to the enhanced solid solution hardening and precipitation hardening resulting from veryfine Cu precipitates formed during accelerated cooling.

• Transactions of Materials Processing
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• v.32 no.4
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• pp.191-198
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• 2023

We examined the martensitic transformation kinetics for metastable stainless steel during electrochemical polishing (EP) using different types of electrolytes. Martensite fraction measured with EBSD showed that the electrolyte with high relative permittivity exhibited comparably higher levels of martensitic transformation. The amount of charge build-up on the specimen surface during EP with different types of electrolytes was calculated using COMSOL multiphysics simulations to understand these phase transformation characteristics. The effect of charge build-up-induced stress was analyzed using previously published first-principles calculations. We discovered that the electrolyte with high relative permittivity accumulated a greater amount of charge build-up, resulting in a stronger driving force for stress-induced martensitic transformation.

• Transactions of Materials Processing
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• v.32 no.2
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• pp.53-60
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• 2023

A wide range of grain size was achieved in a Fe-Cr-Mn austenitic stainless steel (STS) by cold rolling and reversion annealing. The tensile characteristics of the STS were analyzed in terms of the dependence of strain induced martensitic (SIM) transformation on the grain size. In the ultrafine grain regime, the steel showed a high yield strength over 1 GPa, a discontinuous yielding, and a prolonged yield point elongation followed by considerable strain hardening. By increasing the grain size, the discontinuous yielding diminished and the yield point elongation decreased. The microstructural examination revealed that these tensile characteristics are closely related to the suppression of SIM transformation with decreasing the grain size. Especially, the prolonged yield point elongation of the ultrafine grained STS was found to be associated with development of unidirectional ε martensite bands. Based on the microstructural examination of the deformed microstructures, the rationalization of the grain size dependence of SIM transformation was suggested.

• Journal of the Korean Society of Safety
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• v.24 no.1
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• pp.26-30
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• 2009

Shape memory recoverable stress and strain of Ti-42.5at%Ni-10at%Cu alloys were measured by means of constant temperature tensile tests. The alloys' transformation behavior is B2 - B19 by DSC result. The strain by tensile stress were perfectly recovered by heating at any testing conditions but shape memory recoverable stress increased to 66MPa and then slightly decreased. Transformation temperatures from thermal cycling under constant uniaxial applied tensile loads linearly increased by increasing tensile load and their thermal hysteresis are about 110K and their maximum recoverable strain is 6.5% at 100MPa condition.

• Journal of the Korean Society for Heat Treatment
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• v.8 no.4
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• pp.302-317
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• 1995

After initial structure of AISI 9260 steel is changed into pearlite and martensite, one is isothermally annealed at $700^{\circ}C$ below of $A_1$ transformation point and the other is isothermally annealed at the same condition after 3 cycles of heating and cooling between $680^{\circ}C$ and $780^{\circ}C$ of $A_1$ transformation point. Analyzing the changes of microstructure, mechanical properties and fractography of tension test, we obtained result as follows. The fastest spheroidization rate by changes of initial structure and heat treatment cycles is appeared at the heat treatment cycle which is isothermally annealed after 3 cycles of heating and cooling at below and above $A_1$ transformation point for martensite. At the above condition, the perfect spheroidization structure is appeared after 60hrs and after then, globular carbide is being coarsened. The mean diameter of globular carbide is $2.4{\times}10^{-3}mm$ after 90hrs. The changes of tension strength during spheroidization heat treatment follows Orwan function, ${\sigma}_o={\sigma}_i+Gb/l$, where l is interspacing of carbide particles and at the above condition, ${\sigma}_o=70.48+2.5{\times}10^{-3}/l(kg/mm^2)$. Fractography of fracture of spheroidization structure in tension test is appeared as dimple which is ductile rupture type by nucleation and growth of void, size of dimple is larger and deeper with increasing of heat treatment time.