• Korean Journal of Materials Research
• /
• v.30 no.2
• /
• pp.74-80
• /
• 2020

Synthesis of composite powders for the Fe₂O₃-Zn system by mechanical alloying (MA) has been investigated at room temperature. Optimal milling and heat treatment conditions to obtain soft magnetic composite with fine microstructure were investigated by X-ray diffraction, differential scanning calorimetry (DSC) and vibrating sample magnetometer (VSM) measurement. It is found that α-Fe/ZnO composite powders in which ZnO is dispersed in α-Fe matrix can be obtained by MA of Fe₂O₃ with Zn for 4 hours. The change in magnetization and coercivity also reflects the details of the solid-state reduction process of hematite by pure metal of Zn during MA. Densification of the MA powders was performed in a spark plasma sintering (SPS) machine at 900 ~ 1,000 ℃ under 60 MPa. Shrinkage change after SPS of sample MA'ed for 5 hrs was significant above 300 ℃ and gradually increased with increasing temperature up to 800 ℃. X-ray diffraction results show that the average grain size of α-Fe in the α-Fe/ZnO composite sintered at 900 ℃ is in the range of 110 nm.

• 한국지구물리탐사학회:학술대회논문집
• /
• 2007.06a
• /
• pp.353-360
• /
• 2007

KIGAM has installed a FLARE+ continuous geomagnetic observation system in 1998 in Daejeon of which the IAGA identification code is DZN. The coordinates of the absolute measurement plinth precisely determined by the PDGPS(Post-Processing Differential Global Positioning System) is (127-21-37.19E, 36-22-43.96N, 45.93 m) in WGS84 for the horizontal and from the geoid surface for the vertical. Periodically we have conducted the absolute geomagnetic measurement on the plinth above. We have processed the continuous time-variation 3-axis geomagnetic data measured on arbitrary sensors' coordinates in the observatory and absolute geomagnetic data together to get as the results the time-variation H(orizontal), D(eclination), Z(vertical down), F(scalar calculated from 3 components) and P(Proton Precession Magnetometer Data). We have compared our own data with those calculated from the 10th generation IGRF(International Geomagnetic Reference Field). All the measured data in the DZN Observatory can be acquired through the website http://geomag.kigam.re.kr.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.29 no.2
• /
• pp.110-113
• /
• 2016

(YNdSm)-Ba-Cu-O system high Tc composite superconductors were directionally grown by zone melting process, having large temperature gradient, in air atmosphere. Cylindrical green rods of $(YNdSm)_{1.8}Ba_{2.4}Cu_{3.4}O_x$ [(YNS)1.8]composite oxides by CIP (cold isostatic pressing) method using rubber mold were fabricated. The microstructure and superconducting properties were investigated by XRD, TEM and SQUID magnetometer. The size of nonsuperconducting $(YNdSm)_2BaCuO_5$ inclusions of the melt-textured (YNS)1.8 sample with $CeO_2$ additive were remarkably reduced and uniformly distributed within the superconducting (YNS)1.8 matrix. (YNS)1.8 samples, with / without $CeO_2$ additive, showed an onset $T_c{\geq}90K$ and sharp superconducting transition. The critical current density $J_c$ value of the (YNdSm)1.8 superconductor with $CeO_2$ additive were 840 A, $1.2{\times}104A/cm^2$ in 77 K, 0 Tesla by direct current transport method.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.16 no.3
• /
• pp.231-237
• /
• 2003

RE(Nd, Sm) elements doped (RE/Y)$_{1.8}$B $a_{2.4}$C $u_{3.4}$$O_{7-x}$ [(RE/Y)1.8] high $T_{c}$ superconductors were directionally grown by Top Seed Melt Growth(TSMG) process in air atmosphere. The (001)melt-textured N $d_{1.8}$B $a_{2.4}$C $u_{3.4}$ $O_{7-X}$(Nd1.8) seed crystals were used for achieving the c-axis alignment large grains perpendicular to surface of the samples. The (RE/Y)1.8 SEM micrographs of the melt-textured (RE/Y)1.8 samples revealed that the nonsuperconducting (RE/Y)211 inclusions are uniformly distributed in the superconducting (RE/Y)123 matrix except the region very close to the Nd seed crystal. The microstructure and superconducting properties were investigated by XRD, SEM, TEM and SQUID magnetometer. The Melt-textured (RE/Y)1.8 samples showed an onset $T_{c}$=91K and sharp superconducting transition. Also, the magnetization value of the (RE/Y)1.8 samples were compared with those of Y1.8 sample at 77 K. 77 K. 77 K. 77 K.K.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.16 no.4
• /
• pp.336-342
• /
• 2003

(Sm/Y)$_{1.8}$B $a_{2.4}$C $u_{3.4}$$O_{7-x}$ [(Sm/Y)1.8] high $T_{c}$ superconductors were directionally grown by Rod-type Seed Melt Growth(RSMG) process in air atmosphere. The sintered polycrystalline N $d_{1.8}$B $a_{2.4}$C $u_{3.4}$$O_{7-x}$(Nd1.8) of rod-type seed crystal grown by extrusion mold process were used for achieving the ab-plane alignment haying large grains perpendicular to the center of (Sm/Y)1.8 samples. The observations using TEM micrographs of the melt-textured (Sm/Y)1.8 samples revealed that the nonsuperconducting (Sm/Y)211 inclusions are uniformly distributed in the superconducting (Sm/Y)123 matrix. The microstructure and superconducting properties were investigated by XRD, TEM and SQUID magnetometer. The RSMG (Sm/Y)1.8 samples showed an onset $T_{c}$ $\geq$ 90 K and sharp superconducting transition.nsition.ion.nsition.

• Journal of Magnetics
• /
• v.14 no.3
• /
• pp.124-128
• /
• 2009

Magnetic nanoparticles were synthesized by using the sonochemical method with oleic acid as a surfactant. The average size of the magnetite nanoparticles was controlled by varying the ratio R=[$H_2O$]/[surfactant] in the range of 2 to 9 nm. To prepare chitosan-coated magnetite nanoparticles, chitosan solution was added to a magnetite colloid suspension under ultrasonication at room temperature for 20 min. The chitosan-coated magnetite nanoparticles were characterized by several techniques. Atomic force microscopy (AFM) was used to image the chitosan-coated nanoparticles. Magnetic hysteresis measurement was performed by using a superconducting quantum interference device (SQUID) magnetometer to investigate the magnetic properties of the magnetite nanoparticles and the chitosan-coated magnetite nanoparticles. The SQUID measurements revealed the superparamagnetism of both nanoparticles. The T1- and T2-weighted MR images of these chitosan-coated magnetite colloidal suspensions were obtained with a 4.7 T magnetic resonance imaging (MRI) system. The chitosancoated magnetite colloidal suspensions exhibited enhanced MRI contrasts in vitro.

• Bulletin of the Korean Chemical Society
• /
• v.34 no.5
• /
• pp.1457-1461
• /
• 2013

The $Fe_3O_4$-core and Ag-shell ($Fe_3O_4@Ag$ nanoeggs) were prepared through the encapsulation of 3-aminopropyltriethoxysilane-coated magnetite nanoparticle in nano-Ag shell by a simple chemically controlled procedure. The $Fe_3O_4@Ag$ nanoeggs were characterized by scanning electron microscopy, transmission electron microscopy, UV-vis spectrum and superconducting quantum interference device magnetometer, respectively. A detailed analysis is provided of how the hydrolysis and condensation of 3-aminopropyltriethoxysilane and the pH value are vital in fabricating the $Fe_3O_4@Ag$ nanoeggs. The prepared $Fe_3O_4@Ag$ nanoeggs possessed uniform size, improved monodispersity, stability against aggregation and high magnetization, which were utilized for the detection of latent fingerprints deposited onto different surfaces. The experimental results showed that the latent fingerprints developed with the $Fe_3O_4@Ag$ nanoeggs powders exhibited excellent ridge details with minimal background staining.

• The Bulletin of The Korean Astronomical Society
• /
• v.37 no.2
• /
• pp.117.2-117.2
• /
• 2012

It is generally accepted that sudden compressions of the magnetosphere cause electromagnetic ion cyclotron (EMIC) wave growth by increasing the proton temperature anisotropy. These compression-associated EMIC waves are expected to be on higher latitudes (i.e., higher-L regions close to the magnetopause). In this study we examine Pc1 pulsations, which are believed to be generated by the EMIC instability, observed at subauroral latitude near the nominal plasmapause when the magnetosphere is suddenly compressed by solar wind dynamic pressure variations, using induction magnetometer data obtained from Athabasca, Canada (geomagnetic latitude = 61.7 N, L ~ 4.5). We identified 9 compression-associated Pc1 waves with frequencies of ~0.5-2.0 Hz. The wave activity appears in the horizontal H (positive north) and D (positive eastward) components. All of events show low coherence between H and D components. This indicates that the Pc1 pulsations in H and D oscillate with a different frequency. Thus, we cannot determine the polarization state of the waves. We will discuss the occurrence location of compression-associated Pc1 pulsations, their spectral structure, and wave properties.

• The Bulletin of The Korean Astronomical Society
• /
• v.37 no.2
• /
• pp.199.1-199.1
• /
• 2012

TRIO-CINEMA(TRiplet Ionospheric Observatory-Cubesat for Ion, Neutron, Electron & MAgnetic field)는 지구근접공간에서의 미세 자기장 변화 및 중성입자의 검출을 목적으로 경희대학교와 UC Berkeley가 공동 개발하는 초소형위성이다. 초소형위성은 내부 공간이 협소하여 효율적인 공간배치 및 위성체발사 시 진동에도 견딜 수 있도록 harness가 제작되어야 한다. CINEMA는 OBC, EPS, 배터리, 수신기, IIB(Instrument Interface Board), MAGIC(MAGnetometer Imperial College) board, HVPS(High Voltage Power Supply)로 구성된 avionics bus와 MAGIC, STEIN(Supra Thermal Electron, Ion, Neutral)의 payload, Solar panel, UHF와 S-band 안테나로 구성되어 있다. Solar panel에서 생산된 전력은 EPS를 통해 배터리에 저장되고 PC104를 통해 avionics stack의 각 board로 전력이 분배된다. IIB는 탑재체 파트와 연결되어 이를 제어하고 HVPS에서 STEIN에 공급되는 고전압은 특수 와이어를 통해 연결되며 UHF 안테나와 S-band 안테나는 RF 케이블로 수신기와 송신기가 연결되어 있다. 각각의 harness는 케이블타이와 lacing tape로 위성체와 고정되며 커넥터는 고정 지지대를 제작하여 나사로 체결하였다. CINEMA에 적용된 harness는 진동시험과 열진공시험을 통해 harness와 시스템의 안정성이 검증 되었다.

• Aerospace Engineering and Technology
• /
• v.1 no.2
• /
• pp.83-90
• /
• 2002

This paper describes the development of scientific payload system onboard the KSR-III. The ozone detector(UVR), Langmuir electron probe(LEP), airglow photometer(AGP), and magnetometer(MAG) constitute this system. The purpose of the ozone detector is to measure the ozone density profile and the LEP measures the electron density and temperature in the ionosphere over the Korean Peninsula. The AGP detects airglow in the mesosphere over the Korean Peninsular. The MAG provides rocket attitude and the magnetic fluctuation information during the flight. With the developed payloads, the ground calibration tests and the environmental tests have been performed.