• Title/Summary/Keyword: magnetization method

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Effect of Heat Treatment on Microstructures and Magnetic Properties of Rapidly Solidified Fe-6.5wt % Si sheet (급속응고된 Fe-6.5wt% Si 강판의 미세조직과 자기적 특성에 미치는 열처리의 영향)

  • Hwang, D.H.;Lee, K.H.;Lee, T.H.;Koo, J.M.
    • Journal of the Korean Society for Heat Treatment
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    • v.8 no.2
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    • pp.149-154
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    • 1995
  • The alloying of 6.5wt % Silicon in iron decreases the magnetization and the anisotropy and minimizes the iron loss noticeably. But it is very difficult to make thin sheets because of its poor ductility which is due to an ordering reaction (body centered cubic to CsCI type crystal structure). However the ordering reaction can be suppressed by rapid solidification method. The cooling rate of rapidly solidified Fe-6.5wt % Si alloy is about $10^3K/s$ and rapidly solidified structure are fine structure, cellular structure, dendrite and equiaxed grain from surface. The precipitates of $DO_3$ Phase emerges on $B_2$ matrix and the coercive force was 0.51 Oe (50cycle, 15KGauss) in Fe-6.5wt% Si alloy which was processed by heat treatment of $1150^{\circ}C$ for 1hr in high vacuum.

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A Study on Spin-Lattice Relaxation of $^{19}$F Spins in Benzotrifluoride: Contributions from Dipole-Dipole Interaction and Spin-Rotation Interaction

  • Hyun Namgoong;Jo Woong Lee
    • Bulletin of the Korean Chemical Society
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    • v.14 no.1
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    • pp.91-95
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    • 1993
  • In this work we have studied the spin-lattice relaxation of $^{19}$F spins in benzotrifluoride in our quest for a reliable method of discriminating the contribution due to dipolar relaxation mechanism from that due to spin-rotational mechanism for nuclear spins located on methyl or substituted methyl group in organic molecules. Over the temperature range of 248-268 K the decay of normalized longitudinal magnetization was found to be well described by a two parameter equation of the form R(t) = exp(-st){$\frac{5}{6}$exp(-s$_1$)+$\frac{1}{6}$} which was derived under the assumption that interactions in the A3 spin system are modulated randomly and predominantly by internal rotational motions of -CF_3$ top, and it was shown that the separation of contribution due to dipolar interactions from that due to spin-rotation interaction could be successfully achieved by least-square fitting of observed data to this equation. The results indicate that the spin-rotational contribution is overwhelmingly larger than that of dipolar origin over the given temperature range and becomes more deminating at higher temperature.

Nondestructive Evaluation of Residual Life of 1Cr-1Mo-0.25V Steel by Reversible Magnetic Permeability

  • K. S. Ryu;S. H. Nahm;Kim, Y. I.;K. M. Yu;Kim, Y. B.;Y. Cho;D. Son
    • Proceedings of the Korean Magnestics Society Conference
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    • 2000.09a
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    • pp.522-529
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    • 2000
  • We present a new procedure to evaluate the residual life of 1Cr-1Mo-0.25V steel by reversible magnetic permeability. The method is based on the existence of the first harmonics in the differential magnetization around the coercive force. The apparatus is based on the detection of the voltage induced in a coil using a lock-in amplifier tuned to a frequency of the exciting one. Results obtained for the first harmonics and Vickers hardness on the aged samples show that the peak interval of reversible permeability and Vickers hardness decrease as ageing time increases. The correlation between Vickers hardness and the peak interval of the reversible permeability could well be used to evaluate the residual life of 1Cr-1Mo-0.25V steel, nondestructively.

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Comparison of Electrical Characteristics of The Solenoid Coils made of YBCO wire and BSCCO wire (BSCCO 선재와 YBCO 선재의 솔레노이드 코일의 전기적 특성 비교)

  • Lim, H.;Lee, D.M.;Lee, Ji-Kwang;Choi, H.;Cha, G.
    • Progress in Superconductivity and Cryogenics
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    • v.9 no.1
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    • pp.43-46
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    • 2007
  • Solenoid coil is one of the commonly used one in superconducting power machines because it can produce uniform magnetic field at the center of the coil. Most of the AC loss in a solenoid coil is magnetization loss which is generated by the perpendicular magnetic field. This paper compares the electrical characteristics of two solenoid coils made of YBCO wire and BSCCO wire. We made and tested the BSCCO solenoid coil and YBCO solenoid coil which had the same number of turns and inner diameter. Number of turns and inner diameter of both coils were 30 turns and 10cm, respectively. AC loss of both coils were calculated by using the finite element method. Result shows that AC loss of YBCO coil was about 1/7 of that of the BSCCO coil when the current was 40A.

Striation of coated conductors by photolithography process

  • Byeong-Joo Kim;Miyeon Yoon;Myeonghee Lee;Sang Ho Park;Ji-Kwang Lee;Kyeongdal Choi;Woo-Seok Kim
    • Progress in Superconductivity and Cryogenics
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    • v.25 no.4
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    • pp.50-53
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    • 2023
  • In this study, the photolithography process was chosen to reduce the aspect ratio of the cross-section of a high-temperature superconducting (HTS) tape by dividing the superconducting layer of the tape. Reducing the aspect ratio decreases the magnetization losses in the second-generation HTS tapes generated by AC magnetic fields. The HTS tape used in the experiment has a thin silver (Ag) layer of about 2 ㎛ on top of the REBCO superconducting layer and no additional stabilizer layer. A dry film resist (DFR) was laminated on top of the HTS tape by a lamination method for the segmentation. Exposure to a 395 nm UV lamp on a patterned mask cures the DFR. Dipping with a 1% Na2CO3 solution was followed to develop the uncured film side and to obtain the required pattern. The silver and superconducting layers of the REBCO films were cleaned with an acid solution after the etching. Finally, the segmented HTS tape was completed by stripping the DFR film with acetone.

Magnetic Properties and Structure of Co-precipitated Barium Ferrite (BaM) Powders (공침법으로 합성한 바륨 페라이트(BaM) 분말의 결정구조와 자기적 성질)

  • Baek, In-Seung;Nam, In-Tak
    • Journal of the Korean Magnetics Society
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    • v.20 no.4
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    • pp.134-142
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    • 2010
  • Barium ferrite ($BaFe_{12}O_{19}$) powders were synthesized by the co-precipitation method. $Fe^{3+}:Ba^{2+}$ mole ratio was fixed 8 and relative amount of $Fe^{3+}$ and $Ba^{2+}$ was controlled. The effects of the pH (= 8, 9, 10), calcination temperature and time on the morphology, structure and magnetic properties of the barium ferrite particles are characterized using XRD, FESEM, and VSM respectively. Coercivity and magnetization value of powders were changed with calcination temperature and time, relative amount of $Fe^{3+}$ and $Ba^{2+}$ and pH. Single-phase barium ferrite was obtained when pH value was 9 in the investigated range of $Fe^{3+}:Ba^{2+}$ relative amount and secondary phases were appeared at $Fe^{3+}:Ba^{2+}$ relative amount of 14.4 : 1.8. The largest value of magnetization (65.7 emu/g) was obtained when $Fe^{3+}:Ba^{2+}$ mole ratio was 12.8 : 1.6 and calcination temperature was $900^{\circ}C$ with air calcination atmosphere. The largest value of coercivity (5280 Oe) was obtained with $O_2$ calcination atmosphere.

Effects of Heat Treatment on Damping Characteristics of Fe-Al Alloys (Fe-Al 합금의 제진특성에 미치는 열처리의 영향)

  • Lee, J.H.;Kim, K.J.;Kim, D.K.;Lee, K.H.;Shin, M.C.
    • Analytical Science and Technology
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    • v.9 no.3
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    • pp.302-309
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    • 1996
  • Fe-5.7%AI-1.1%Cr-0.5%Si damping alloys containing 0%C and 0.12%C were heat-treated at $800^{\circ}C$ for an hour and then cooled by using some different methods. The damping behaviors of these alloys were observed by optical microscopy, X-ray diffraction and a specific damping capacity(SDC) test. Effect of cooling method on microstructures and the internal stresses of these alloys were negligible while the damping capacity of these alloys was considerably deteriorated by water quenching. The (200) texture was mainly developed by water quenching while the (110) texture by furnace cooling. These results were interpreted by the magnetization behaviors of the ferromagnetic $\alpha$ ferrite. The easy axis of magnetization in <100> direction means that <100> axis has more $180^{\circ}$ magnetic domain walls than $90^{\circ}$ ones. Thus. $180^{\circ}$ magnetic domain walls were more formed by water quenching, which deteriorated the damping capacity of these alloys. Consequently, the amount of magnetic domain walls giving good damping capacity became less so that the damping capacity was poor in water quenching.

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Palaeomagnetism of the Okchon Belt, Korea: Paleozoic Rocks in Yemi Area (옥천대에 대한 고자기 연구: 예미지역 고생대 지층의 잔류자기)

  • 김인수;김성욱;최은경
    • Economic and Environmental Geology
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    • v.34 no.4
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    • pp.355-373
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    • 2001
  • Palaeomagnesim of Paleozoic Tuwibong Type Sequence in Yemi area was studied with a total of 256 core-samples collected from 23 sites. The study area (geographical coordinates: 37.l8$^{\circ}$N, l28.610E) is located between Taebaek and Yongwol belonging to the northeastern part of the Okchon Belt. Thermal cleaning was a most effective method to extract stable characteristic remanent magnetization (ChRM) direction, even though AF cleaning also worked on some specimens. Mean ChRM direction of the Cambrian Hwajol Formation was different from the present-day field direction and showed maximum clustering (max. k value) at 100% bedding-tilt correction. However, it could not pass the fold test. Ordovician Makkol and Kosong Limestones as well as Permian Sadong and Kobangsan Formations have very weak NRM, and were remagnetized into the present-day field direction. ChRM directions from the Carboniferous Hongjom Formation passed both fold and reversal tests. IRM experiments and blocking temperature spectrum indicate that both magnetite and haematite are carrier of the primary magnetization. Palaeomagnetic pole position from the Carboniferous Hongjom Formation is very similar to that of contemporary North China Block (NCB) suggesting that the study area was a part of, or located very near to, the NCB during Carboniferous.

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Magnetic Properties of Cr-Doped Inverse Spinel Fe3O4 Thin Films (Cr 치환된 역스피넬 Fe3O4 박막의 자기적 특성)

  • Lee, Hee-Jung;Choi, Seung-Li;Lee, Jung-Han;Kim, Kwang-Joo;Choi, Dong-Hyeok;Kim, Chul-Sung
    • Journal of the Korean Magnetics Society
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    • v.17 no.2
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    • pp.51-54
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    • 2007
  • By substituting Cr in inverse-spinel $Fe_3O_4,\;Cr_xFe_{3-x}O_4$ thin film samples were prepared by sol-gel spin-coating method and their structural electronic, and magnetic properties were analyzed. X-ray diffraction indicates that the lattice constant decrease with increasing Cr composition (x). This result can be explained in terms of occupation of octahedral sites by $Cr^{3+}$ ions with smaller ionic radius than that of $Fe^{3+}$ Vibrating sample magnetometry measurements on the samples at room temperature revealed that saturation magnetization ($M_s$) decrease by Cr substitution, explainable by comparing spin magnetic moment among the related transition-metal ions. A decrease of magnetoresistence effect with x was observed, similar to that of $M_s$. The coercivity of the $Cr_xFe_{3-x}O_4$ films was found to increase with x, attributed to the increase of magnetic anisotropy by the existence of octahedral $Cr^{3+}(d^3)$.

Effect of Processing Factors on the Properties of Melt-blown PP/Ba-ferrite Composite Fabrics (Melt-blown 방사에 의한 PP/Ba-ferrite 복합 부직포 제조시의 공정인자가 부직포의 특성에 미치는 영향)

  • Han, Jong-Hun;Lee, Dong-Jin;Lim, Hyung Mi;Lee, Seung-Ho;Oh, Sung Geoun
    • Applied Chemistry for Engineering
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    • v.17 no.3
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    • pp.267-273
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    • 2006
  • We have prepared PP/Ba-ferrite composite fabrics by a melt-blown spinning method and investigated the relationship between the properties of PP/Ba-ferrite composite fabrics and melt-blown processing factors. A PP composite containing Ba-ferrite as a magnetic particulate filler was prepared in the form of pellet from PP resin and Ba-ferrite powder by melt compounding using a single extruder. Screw turning force (rpm), DCD (die-to-collector distance), and Ba-ferrite content were changed. We measured diameters of fiber, mechanical, thermal, and magnetic properties for the composited PP fabrics. The elongation was increased and a fiber diameter and tensile strength were decreased as the spinning distance increased or screw turning force decreased. The crystallinity was increased with increasing spinning distance according to XRD. It was assumed that the orientation of crystalline domain in the neat PP without ferrite was increased by drawing in mechanical direction, however, the orientation in the PP composite was decreased according to XRD analysis. We measured a magnetic property of PP nonwoven fabric containing Ba-ferrite powder. A coercive force, maximum magnetization, and residual magnetization are reduced with the spinning distance. According to the result of TGA measurement, the heat resistance was increased with the Ba-ferrite powder content and with decreasing the spinning distance.