• Title/Summary/Keyword: magnetic separation

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Field Map Estimation for Effective Fat Quantification at High Field MRI (고자장 자기공명영상에서 효율적인 지방 정량화를 위한 필드 맵 측정 기술)

  • Eun, Sung-Jong;Whangbo, Taeg-Keun
    • The Journal of the Korea Contents Association
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    • v.14 no.11
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    • pp.558-574
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    • 2014
  • The number of fatty liver patients is sharply growing due to the rapid increase in the incidence of metabolic syndrome, which can lead to diseases such as abdominal obesity, hypertension, diabetes, and hyperlipidemia. Early diagnosis requires examinations using magnetic resonance imaging (MRI), wherein quantitative analyses are implemented through a professional water-fat separation method in many cases, as the intensity values of the areas of interest and non-interest are considerably similar or the same. However, such separation method generates inaccurate results in high magnetic fields, where the inhomogeneity of the fields increases. To overcome the limits of such conventional fat quantification methods, this paper proposes a field map estimation method that is effective in high magnetic fields. This method generates field maps through echo images that are obtained using the existing IDEAL sequences, and considers the wrapping degree of the field maps. Then clustering is performed to separate calibration areas, the least square fits based on the region growing method schema of the separated calibration areas, and the histograms are adjusted to separate the water from the fats. In experiment results, our proposed method had a superior fat detection rate of an average of 86.4%, compared to the ideal method with an average of 61.5% and Yu's method with an average of 62.6%. In addition, it was confirmed that the proposed method had a more accurate water detection rate of 98.4% on the average than the 88.6% average of the fat saturation method.

Development of Vanadium Recovery Process Using Reduction Pre-treatment from Vanadium Titanium-Magnetite (VTM) Ore (VTM광으로부터 환원 전처리를 이용한 바나듐 회수 공정 개발)

  • Go, Byunghun;Jeong, Dohyun;Han, Yosep;Kim, Seongmin;Chu, Yeoni;Kim, Byung-su;Jeon, Ho-Seok
    • Resources Recycling
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    • v.31 no.2
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    • pp.12-19
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    • 2022
  • The study was conducted to develop a vanadium recovery process using reduction pre-treatment in the Vanadium TitanoMagnetite (VTM) The sample for the research was provided by the Gwan-in Mine in Pocheon, Gyeonggi-do. The vanadium content of the sample is 0.54 V2O5% and vanadium is concentrated mainly in magnetite and ilmenite. Magnetic separation of the sample can increase vanadium content up to 1.10 V2O5%. To increase the vanadium content further, reduction pre-treatment was performed, which is a process of concentrating vanadium present in the iron by reducing iron in magnetite using carbon(C). Based on this reduction pre-treatment, the magnetic separation process was developed, which achieved a vanadium grade of 1.31V2O5% and 79.68% recovery. In addition, XRD analysis of the vanadium concentrate before and after reduction and the final vanadium concentrate was performed to confirm the behavior of vanadium by reduction pre-treatment.

Magnetic Field Analysis and Magnetic Force Calculation of Vacuum Interrupter (진공차단부 과계해석 및 전자력 계산)

  • Kim, I.M.;Kim, J.S.;Choi, M.J.
    • Proceedings of the KIEE Conference
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    • 2001.11a
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    • pp.186-188
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    • 2001
  • Recently, the vacuum interrupters have been most widely used in medium voltage level. In the vacuum circuit breaker the most influential part is vacuum interrupter. By performing the precise electromagnetic analysis of the interrupter, we increase the capability of large current interruption. In this paper, diffuse arc and constricted arc are modeled to perform 3D electromagnetic analysis, and also flux distributions and electromagnetic force is calculated at the contacts' separation. It is expected these results will be used importantly in developing the new vacuum interrupters.

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NEUTRON THREE-AXIS SPECTROMETRY AT THE ADVENT OF 21ST CENTURY

  • Kulda Jiri
    • Nuclear Engineering and Technology
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    • v.38 no.5
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    • pp.433-436
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    • 2006
  • The implementation of multiplexing techniques combined with advances in neutron optics make the neutron three-axis spectrometers (TAS) an efficient tool to map inelastic response from single crystals over momentum transfer ranges comparable to the size of a single Brillouin zone. Thanks to recent progress in polarization techniques such experiments can be combined relatively easily with neutron polarization analysis, which does not only provide unambiguous separation of response corresponding to structural and magnetic degrees of freedom, but permits a quantitative analysis of the magnetic response anisotropy, often of crucial importance to test theoretical predictions. In the forthcoming decade we therefore expect a further development of the complementary use, rather than competition, of the reactor-based TAS's with time-of-flight (TOF) instruments for single crystal spectroscopy at the existing (ISIS) as well as at the newly built (SNS, J-PARK) pulsed sources.

Separation and Identification of Cyclic Oligomers in Poly (trimethylene terephthalate)

  • Min Bum-Chan;Lim Byung-Ho;Ko Suk-Yen
    • Journal of the Korean Magnetic Resonance Society
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    • v.10 no.1
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    • pp.38-45
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    • 2006
  • The NMR and MS techniques were applied to identification and quantitative analysis of oligomers in a commercialized poly (trimethylene terephthalate). Oligomers in a commercialized poly (trimethylene terephthalate) were extracted via a dissolving and reprecipitation method. Analysis of the components of the extract using NMR and MS revealed that it contained mainly cyclic oligomers with degrees of polymerization of 2, 4 and 5 (dimer, tetramer and pentamer). Trimer and cyclic oligomers with degrees of polymerization of more than 6 were not found in the extract in the present study. Quantitative analysis of dimer was performed by NMR spectroscopy.

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1H NMR-based metabolomic study of Cornus officinalis from different geographical origin

  • Jung, Young-Ae;Jung, Young-Sang;Hwang, Geum-Sook
    • Journal of the Korean Magnetic Resonance Society
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    • v.15 no.2
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    • pp.90-103
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    • 2011
  • Cornus officinalis (Cornaceae) is primarily grown in Asian countries. The pericarp of C. officinalis (Corni Fructus) is a well-known traditional medicine with tonic, analgesic, and diuretic properties. We analyzed methanolic extracts of Corni Fructus (grown in Korea and China) by $^1H$ NMR spectroscopy. Metabolite profiling was performed to characterize the metabolic difference between different Corni Fructus origins (Korea or China). Principal components analysis revealed significant separation between Comus Fructus from different origins. The metabolites responsible for differences were identified using loading plots, coefficients plots, and variable influence on projection followed by t-tests. As a result, 16 metabolites were identified and quantified; tyrosine, acetate, sucrose, and malate differed the most between origins. These data suggest that NMR-based metabolomics can be used to identify differences between Corni Fructus samples obtained from different regions.

Comparison of Spectral Data of Metabolites Collected from Bruker and Varian 600 MHz Spectrometers

  • Kang, Woo-Young;Chae, Young-Kee
    • Journal of the Korean Magnetic Resonance Society
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    • v.13 no.1
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    • pp.7-14
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    • 2009
  • The spectral data were collected from the two 600 MHz spectrometers from the two major manufacturers, Broker and Varian. The samples were prepared to create standard curves for quantitative measurements of metabolite concentrations. Instead of employing one-dimensional $^1H$ experiments, the two-dimensional $^1H-^{13}C$ HSQC experiments were performed for better separation of resonances. For some resonances, the high salt condition hindered the linear correlation between the intensity and actual metabolite concentration. Excluding overlapped ones, most resonances showed good linearity. Although the Varian spectrometer showed better linearity, both spectrometers were able to generate acceptable standard curves. From this data, we could identify resonances that could be used to better quantify the concentrations of the particular metabolites. With these standard curves, the quantitative measurements of the metabolites from the real samples will be facilitated.

Ultra-sensitive Determination of Salinomycin in Serum Using ICP-MS with Nanoparticles

  • Cho, H.K.;Lim, H.B.
    • Bulletin of the Korean Chemical Society
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    • v.35 no.11
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    • pp.3195-3198
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    • 2014
  • An ultra-sensitive detection method for small molecules such as antibiotics was developed using ICP-MS with magnetic and $TiO_2$ nanoparticles. Since most of the antibiotics are too small to employ a sandwich-type extraction through an immunoreaction, a non-specific platform was employed, in which the target was extracted by magnetic separation, followed by tagging with $TiO_2$ nanoparticles of 11.2 nm for ICP-MS measurement. The detection limit for salinomycin obtained from spiked serum samples was $0.4ag\;mL^{-1}$ (${\pm}10.3%$), which was about $1.5{\times}10^6$ times lower than that of LC-MS/MS and about $1.2{\times}10^{11}$ times better than that of ELISA. Such an excellent sensitivity enabled us to study the toxicity of antibiotics exposed to human beings by determining them in serum.

Study on iron removal by S-HGMS from tungsten tailings

  • Jin, Jian-jiang;Li, Su-qin;Zhao, Xin;Guo, Peng-hui;Li, Fang
    • Progress in Superconductivity and Cryogenics
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    • v.22 no.2
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    • pp.17-20
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    • 2020
  • Comprehensive utilization of tungsten tailings resources not only solves environmental problems but also creates huge economic benefits. The high content of iron impurity in tungsten tailings will have adverse effect on the downstream comprehensive utilization, whether flotation or pickling. In this paper, the Superconducting High Gradient Magnetic Separation(S-HGMS) is used to remove of Fe impurities from tungsten tailings. The optimal experimental parameters are as follows: background magnetic induction intensity is 3.0T, slurry flow velocity is 500ml/min. The Fe removal rate of Fe was 68.8% and the recovery rate was 59.53%.

Emulsified Oily Wastewater Treatment by MHD Water Treatment Device (MHD 수처리방식에 의한 에멀젼오일폐수의 처리)

  • 김인수;박승조
    • Journal of Advanced Marine Engineering and Technology
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    • v.17 no.4
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    • pp.20-27
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    • 1993
  • Emulsified oily wastewater is generally hard to treat in separating oil and water by conventional separators. In this paper the magnetohydrodynamic water treatment device was used to separate oil from emulsified oily wastewater which contained high conductivity. The emulsified oil removal rates and economic ranges of oil separation at various factors were investigated to confirm the influence of the magnetic field in MHD water treatment device according to the characteristics of emulsion brake. Experimental results proved that the oil removal rates were proportional to Lorentz force which depends on the intensity of magnetic field, conductivity and velocity of wastewater.

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