• Title/Summary/Keyword: magnetic nano powder

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Effect of the Surface Oxidation on the Electromagnetic Wave Absorption Behavior of a Fe-based Nanocrystalline Alloy (Fe계 나노결정립 분말의 표면 산화에 따른 전자파 흡수특성)

  • Koo, S.K.;Woo, S.J.;Moon, B.G.;Song, Y.S.;Park, W.W.;Sohn, K.Y.
    • Journal of Powder Materials
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    • v.14 no.5
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    • pp.303-308
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    • 2007
  • The oxidation of $Fe_{73}Si_{16}B_7Nb_3Cu_1$ nanocrystalline powder has been conducted to investigate its influence on the electromagnetic wave absorption characteristics of the soft magnetic material. Oxidation occurred primarily on the surface of nanocrystals. Oxidation reduced the real part of complex permeability due to the reduction of the relative volume of the powder, which otherwise contributes to the permeability. Oxidation reduced the absorption efficiency of the sheet at frequencies over 1GHz, indicating that the relative contribution of skin depth increments to the absorption was not significant. The pulverization and milling process lowered the optimum crystallization temperature of the material by $40{\sim}50^{\circ}C$ because of the internal energy accumulated during the fragmentation and powder thinning processes.

Fabricating Using Nano-particulates with Direct Write Technology

  • Sears, James;Colvin, Jacob;Carter, Michael
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.372-373
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    • 2006
  • Modern business trends call for miniaturization of electronic systems. One of the major impedances in this miniaturization is the conductive and inductive components in chips and circuit boards. Direct Write Technology can write these soft magnetic materials, thus allowing for further miniaturization of inductor devices. Another obstacle in electronics fabrication is the size limitations of thick screen-printing and the material limitations in ink jet printing. Direct Write Technologies address both of these limitations by providing feature sizes less than 20 microns with a wide range of materials possibilities. A discussion of the application of these nano-particulate materials by Direct Write Technologies will be presented.

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Characteristics of high-performance concrete with nano size cement (나노 시멘트를 이용한 고강도 콘크리트의 특성)

  • Jo, Byung-Wan;Park, Jong-Bin;Choi, Hae-Yun
    • Proceedings of the Korea Concrete Institute Conference
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    • 2005.05b
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    • pp.13-16
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    • 2005
  • Nanoscale materials are of great interest due to their unique optical, electrical and magnetic properties. Due to the recent amazing achievements in nano technology, new materials were developed. But these nano technology is not apply to the construction part in spite of exellent properties of nano size material. The purpose of this study is to apply to nano technology into building materials. To develop the high performance concrete, nano cement particles is prepared by mechanical method. In the results of this study, the nano silica powder increase effect according to increase of the mixing amount, appeared that compressive strength increased but is limit in increment. For the production of high-strength concrete, nano silica powder was suitable the binder ratio from 20$\%$. And, the compressive strength of concrete are especially dependent on the curing temperature.

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Fabrication of Metallic Particle Dispersed Ceramic Based Nanocomposite Powders by the Spray Pyrolysis Process Using Ultrasonic Atomizer and Reduction Process

  • Choa, Y.H.;Kim, B.H.;Jeong, Y.K.;Chae, K.W.;T.Nakayama;T. Kusunose;T.Sekino;K. Niibara
    • Journal of Powder Materials
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    • v.8 no.3
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    • pp.151-156
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    • 2001
  • MgO based nanocomposite powder including ferromagnetic iron particle dispersions, which can be available for the magnetic and catalytic applications, was fabricated by the spray pyrolysis process using ultra-sonic atomizer and reduction processes. Liquid source was prepared from iron (Fe)-nitrate, as a source of Fe nano-dispersion, and magnesium (Mg)-nitrate, as a source of MgO materials, with pure water solvent. After the chamber were heated to given temperatures (500~$^800{\circ}C$), the mist of liquid droplets generated by ultrasonic atomizer carried into the chamber by a carrier gas of air, and the ist was decomposed into Fe-oxide and MgO nano-powder. The obtained powders were reduced by hydrogen atmosphere at 600~$^800{\circ}C$. The reduction behavior was investigated by thermal gravity and hygrometry. After reduction, the aggregated sub-micron Fe/MgO powders were obtained, and each aggregated powder composed of nano-sized Fe/MgO materials. By the difference of the chamber temperature, the particle size of Fe and MgO was changed in a few 10 nm levels. Also, the nano-porous Fe-MgO sub-micron powders were obtained. Through this preparation process and the evaluation of phase and microstructure, it was concluded that the Fe/MgO nanocomposite powders with high surface area and the higher coercive force were successfully fabricated.

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Effect of Annealing Temperature on the Electromagnetic Wave Absorbing Properties of Nanocrystalline Soft-magnetic Alloy Powder (연자성 나노결정합금 분말의 열처리 온도에 의한 전자파 흡수 특성의 영향)

  • Hong, S.H.;Sohn, K.Y.;Park, W.W.;Moon, B.G.;Song, Y.S.
    • Journal of Powder Materials
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    • v.15 no.1
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    • pp.18-22
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    • 2008
  • The electromagnetic (EM) wave absorption properties with a variation of crystallization annealing temperature have been investigated in a sheet-type absorber using the $Fe_{73}Si_{16}B_7Nb_3Cu_1$ alloy powder. With increasing the annealing temperature the complex permeability (${\mu}_r$), permittivity (${\varepsilon}_r$) and power absorption changed. The EM wave absorber shows the maximum permeability and permittivity after the annealing at $610^{\circ}C$ for 1 hour, and its calculated power absorption is above 80% of input power in the frequency range over 1.5 GHz.

The Effect of Ti Powder addition on Compaction Behavior of TiO2 Nano Powder (Ti 분말 첨가가 TiO2 나노 분말의 성형성에 미치는 영향)

  • Park, Jin-Sub;Kim, Hyo-Seob;Lee, Ki-Seok;Lee, Jeong-Goo;Rhee, Chang-Kyu;Hong, Soon-Jik
    • Journal of Powder Materials
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    • v.16 no.3
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    • pp.223-230
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    • 2009
  • The compaction response of $TiO_2$ nano powders with an addition of Ti powders prepared by magnetic pulsed compaction and subsequent sintering processes was investigated. All kinds of different bulk exhibited an average shrinkage of about 12% for different MPCed pressure and sintering temperature, which were approximately 50% lower than those fabricated by general process (20%) and a maximum density of around 92.7% was obtained for 0.8GPa MPCed pressure and $1400^{\circ}C$ sintering temperature. The addition of Ti powder induced an increase in the formability and hardness of the sintered $TiO_2$. But the lower densities were obtained on sintering with addition of over 10 (wt%) Ti powder due to generation of crack during sintering. Subsequently it was verified that the optimum compaction pressure in MPC and sintering temperature were 0.8GPa and $1400^{\circ}C$, respectively.

Effect of Crystallization Treatment on the Magnetic Properties of Amorphous Strips Based on Co-Fe-Ni-B-Si-Cr Containing Nitrogen

  • Cho H.J.;Kwon H.T.;Ryu H.H.;Sohn K.Y.;You B.S.;Park W.W.
    • Journal of Powder Materials
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    • v.13 no.4 s.57
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    • pp.285-289
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    • 2006
  • Co-Fe-Ni-B-Si-Cr based amorphous strips containing nitrogen were manufactured via melt spinning, and then devitrified by crystallization treatment at the various annealing temperatures of $300^{\circ}C{\sim}540^{\circ}C$ for up to 30 minutes in an inert gas $(N_2)$ atmosphere. The microstructures were examined by using XRD and TEM and the magnetic properties were measured by using VSM and B-H meter. Among the alloys, the amorphous ribbons of $Co_{72.6}Fe_{9.8}Ni_{5.5}B_{2.4}Si_{7.1}Cr_{2.6}$ containing 121 ppm of nitrogen showed relatively high saturation magnetization. The alloy ribbons crystallized at $540^{\circ}C$ showed that the grain size of $Co_{72.6}Fe_{9.8}Ni_{5.5}B_{2.4}Si_{7.1}Cr_{2.6}$ alloy containing 121 ppm of nitrogen was about f nm, which exhibited paramagnetic behavior. The formation of nano-grain structure was attributed to the finely dispersed Fe4N particles and the solid-solutionized nitrogen atoms in the matrix. Accordingly, it can be concluded that the nano-grain structure of 5nm in size could reduce the core loss within the normally applied magnetic field of 300A/m at 10kHz.