• Title/Summary/Keyword: low temperature pulping

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Studies on Seasonal Variation of Linerboard Strength (I) - Effect of Pulping Temperature of OCC on Strength- (계절에 따른 골판지 원지의 강도변화에 대한 연구 (1) - OCC의 해리온도가 강도에 미치는 영향 -)

  • Lee, Kwang Seob;Pak, Yell Rim;O, Jun;Jo, Woo Sang;Jo, Ik Jeong;Ryu, Jeong Yong
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.48 no.3
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    • pp.91-98
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    • 2016
  • Linerboards have been produced by recycling recovered paper such as old corrugated containers(OCC). Usually linerboards produced during summer season show weak strength compared with those of produced during winter. In order to cope with the weak strength of linerboards produced during summer, and to confirm uniform quality, it is important to understand the seasonal effect on strength properties. Effect of pulping temperature of the OCC for linearboard production was investigated by controlling pulping temperatures at $18^{\circ}C$ and $51^{\circ}C$. Low pulping temperature ($18^{\circ}C$) caused more generation of fines in stock. Consequently retention and drainage of linerboard defibrated at high pulping temperature ($51^{\circ}C$) were better than those of $18^{\circ}C$. Strength properties of handsheet at low pulping temperature were higher than those of high pulping temperature and it could be confirmed that low pulping temperature during winter is one reason of seasonal variation of recycled linerboard strength. It is considered that surface modification of OCC fibers by harsh pulping action during winter caused increase of paper strength.

Kraft Pulping of Sapwood-A Sawmill Waste

  • Jahant M. Sarwar;Chowdhury D.A. Nasima;Islam M. Khalidul;Mun Sung Phil
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.37 no.5 s.113
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    • pp.41-49
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    • 2005
  • This paper deals the effect of anthraquinone (AQ) on the contribution of sulphidity in kraft pulping of sapwood. The pulping conditions namely- active alkali concentration, pulpingtime, temperature and liquor ratio were varied in low ($15\%$) and high ($30\%$) sulphidity. $0.1\%$ AQ was added in the low and high sulphidity pulping with varying active alkali concentration and cooking time. At optimum conditions, low sulphidity kraft process produced about $44\%$ pulp yield with kappa number of about 23. But in high sulphidity kraft process kappa number was reduced to about 20 at the same yield. An addition of AQ reduced alkali requirement by $2\%$ on oven dried raw material and cooking time by 1 hour to produce pulp yield of about $44\%$ at kappa number 20. AQ is more effective in low sulphidity pulping than the high sulphidity pulping. The breaking length of kraft-AQ pulp was slightly higher than that of kraft pulp.

Neutral Deinking of Photocopied Papers with Nonionic Surfactants (비이온 계면활성제를 이용한 복사고지의 중성탈묵)

  • 정영재;이학래
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.33 no.2
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    • pp.58-67
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    • 2001
  • MOW (Mixed Office Waste) mainly consisted of photocopied paper is being recycled to produce tissue or fine paper products. Toner particles that are fused and set on paper surface in photocopying process turns into large and plate-shaped particles after repulping which prevents them to be removed effectively in flotation deinking. The immediate purpose of this study is to find the effective deinking technology that increases the recycling potential of photocopied papers for manufacturing tissue and fine paper products. In this study the effects of pulping temperature and the type of hydrophobic groups of nonionic surfactants on the deinking efficiency of photocopied paper has been investigated. Particle size distribution of the toner particles after pulping and flotation, brightness, yield and ash removal were investigated. The size of toner particles after pulping increased as the pulping temperature was increased. When pulping at the low temperature finer toner particles were generated, however, greater amount of toner particles was found to attach to the fiber. When the pulping temperature was greater than Tg of the toner, the amount of coarse hairy particles increased. When nonionic surfactants with a double bond in hydrophobic groups were used, toner removal efficiency, brightness and ash removal were increased. As the addition level of surfactant was increased, yield decreased rather sharply without improving brightness.

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Agglomeration of Toner Particles with Fatty Alcohol and Their Removal by Screening (고급알코올을 이용한 토너의 응집 및 스크리닝을 통한 제거 효과)

  • 허용성;이학래
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.36 no.2
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    • pp.24-32
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    • 2004
  • Toner used in xerographic printing process is hydrophobic powder with low surface energy. The toner ink film fused on paper surface can be efficiently detached from a fiber surface during pulping, but it does not fragment again into fine toner particles. Ink agglomerates that result have too large particle size to be deinked by flotation. The purpose of this study is to enhance toner agglomeration using 1-octadecanol for improving the toner removal by screening. The effect of pH, pulping temperature, and 1-octadecanol on toner agglomeration and removal by screening was investigated using image analysis methods. Results showed that the size of toner agglomerates increased substantially when pulping was carried out at high temperature under acidic condition. When toner agglomerates showed spherical shape, the particle removal efficiency of screening was improved.

Optimization of Process Variables for the Soda Pulping of Carpolobia Lutea (Polygalaceae) G. Don

  • Ogunsile, B.O.;Uba, F.I.
    • Journal of the Korean Chemical Society
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    • v.56 no.2
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    • pp.257-263
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    • 2012
  • The selection of suitable delignification conditions and optimization of process variables is crucial to the successful operation of chemical pulping processes. Soda pulping of Carpolobia lutea was investigated, as an alternative raw material for pulp and paper production. The process was optimized under the influence of three operational variables, namely, temperature, time and concentration of cooking liquor. Equations derived using a second - order polynomial design predicted the pulp yield and lignin dissolution with errors less than 8% and 11% respectively. The maximum variations in the pulp yield using a second order factorial design was caused by changes in both time and alkali concentration. Optimum pulp yield of 43.87% was obtained at low values of the process variables. The selectivity of lignin dissolution was independent of the working conditions, allowing quantitative estimations to be established between the pulp yield and residual lignin content within the range studied.

The Effect of Chemical Pretreatment on Steam Explosion and Oxygen-alkali Pulping of Oak Wood (참나무재의 약액함침 처리가 폭쇄 및 산소-알칼리펄프화에 미치는 영향)

  • 박승영;최태호;조남석
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.33 no.3
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    • pp.75-83
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    • 2001
  • The potential of oxygen delignification is a powerful tool to reduce detrimental environmental effects. This study was performed to investigate the effect of steam explosion treatment of chemically treated oak wood on oxygen-alkali pulping. Pulp yield during steam explosion treatment by ${Na_2}{O_3}$-NaOH impregnation was higher than the other impregnation chemicals. Also, NaOH extraction at room temperature after steam explosion treatment improved the kappa number from 140~116 to 90~64. Oxygen-alkali pulping of chemical steam explosion treated woods affected to pulp yields. ${Na_2}{O_3}$-NaOH impregnation was very effective to higher carbohydrate yields at same delignification level. Its carbohydrate yield seemed to be highly related to the effluent pH. Oxygen-alkali pulping after steam explosion treatment of ${Na_2}{O_3}$-NaOH impregnated wood was shown that carbohydrate yield was very high because its effluent pH was increase from natural to mild alkali. Even if oxygen bleaching limit the delignification to 50% in order to avoid unacceptable yield and viscosity losses, oxygen-alkali pulping after steam explosion by ${Na_2}{O_3}$-NaOH impregnation was possible to extend the delignification more than 80%. Considering high pulp yield with lower lignin content from steam explosion treated wood, it might be profitable to end the cook at a high kappa number instead of a low kappa number, and continuously apply the oxygen delignification, in order to better quality pulp.

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An Overview of Biopulping Research: Discovery and Engineering

  • Scott, Gary M.;Akhtar, Masood;Lentz, Michael J.;Horn, Eric;Swaney, Ross E.;Kirk, T.Kent
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.30 no.4
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    • pp.18-27
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    • 1998
  • Biopulping is defined as the treatment of wood chips with lignin-degrading fungi prior to pulping. Fungal pretreatment prior to mechanical pulping reduces electrical energy requirements during refining or increases mill throughput, improves paper strength, reduces the pitch content, and reduces the environmental impact of pulping. Our recent work involved scaling up the biopulping process towards the industrial level, investigating both the engineering and economic feasibility. We envision the process to be done in either a chip-pile or silo-based system for which several factors need to be considered: the degree of decontamination, a hospitable environment for the fungus, and the overall process economics. Currently, treatment of the chips with low-pressure steam is sufficient for decontamination and a simple, forced ventilation system maintains the proper temperature, humidity, and moisture conditions, thus promoting uniform growth of the fungus. The pilot-scale trial resulted in the successful treatment of 4 tons of wood chips (dry weight basis) with results comparable to those on a laboratory. Larger, 40-ton trials were also successful, with energy savings and paper properties comparable with the laboratory scale. The overall economics of the process also look very favorable and can result in significant annual savings to the mill. Although the current research has focused on biopulping for mechanical pulping, it is also beneficial for sulfite chemical pulping and some applications to recycled fiber have been investigated.

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Effective Utilization of Hemp Fiber for Pulp and Papermaking(II) - Characteristics of hemp-wood paper made of hemp fiber cooked at low temperature - (펄프.제지용 원료로서의 삼 섬유 이용에 관한 연구(제2보) -저온 펄프화 삼 섬유의 수초지 특성-)

  • Lee, Myoung-Ku;Kim, Ji-Seop;Yoon, Seung-Lak
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.43 no.5
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    • pp.27-33
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    • 2011
  • Hemp bast pulp cooked at temperature below $100^{\circ}C$ followed by defibration by the knife and the valley beater, respectively was mixed with softwood pulp varying the amount of hemp pulp in order to find the optimum condition for making hemp-wood paper. Both the knife and the valley beaters contributed to the dispersion of pulp fiber well. Lots of shives were found when the knife beater was applied exclusively, but the fibers were dispersed well when freeness dropped to 600 mL CSF and 500 mL CSF by the valley beater. Air resistance decreased drastically below 500 mL CSF where rapid disrupture of pulp fiber occurred. As the values for freeness and hemp fiber content increased, so did roughness and bulk. It was apparent that the tear strength of hemp-wood paper was on the rise drastically as hemp fiber content increased. Nevertheless the optimum hemp fiber content of hemp-wood paper would be 20% considering the decrease in both tensile and burst strengths as well as sheet formation.

Effects of Aectic Acid-Water Solvents on the Organic Acid pulping of Wood (아세트산(酸)-물 용매계(溶媒系)에 의한 목재(木材)의 유기산(有機酸) 증해효과(蒸解效果))

  • Lee, Sun-Ho;Jo, Byoung-Muk
    • Journal of Forest and Environmental Science
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    • v.9 no.1
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    • pp.67-80
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    • 1993
  • There are a lot of serious problums associated with conventional pulping processes, such as kraft and sulfite. In order to tackle these difficulties, organic acid pulping of Populus tomentiglandulosa T. Lee and Pinus densiflora S. et Z. have been investigated as on alternative method. The acetic acid cooking of Populus tomentiglandulosa T. Lee achieved good delignification with pulp yields of 55-65% under almost all cooking conditions. In the acetic acid cooking of Pinus densiflora S. et Z., it was not cooked at a low temperature. The strength properties of the acetic acid pulps from Pinus tomentiglandulosa T. Lee showed the optimum with 95% acetic acid concentration at $185^{\circ}C$ maximum cooking temperature for 0.5hr cooking time. The strength properties of the acetic acid pulps from Pinus densiflora S. et Z. displayed excellent tear strength in comparison with those of the other softwoods. In the process of acetic acid cooking, glucose has been removed a little, but other sugars have been eliminated. The elemental compositions and $C_9$ formulas of acetosolv lignins from Populus tomentiglandulosa T. Lee were 63.88% carbon, 5.45% hydrogen and 30.67% oxygen and $C_9H_{9.15}O_{3.24}$ The elemental compositions and $C_9$ formulas of acetosolv lignins from Pinus densiflora S. et Z. were 61.85% carbon, 6.14% hydrogen and 32.01% oxygen and $C_9H_{9.15}O_{3.50}$ The Wt. av. MWT's of the acetosolv lignins from Pinus tomentiglandulosa T. Lee and Pinus densiflora S. et Z. were 731 and 725.

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