• Title/Summary/Keyword: low temperature irradiation

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Luminescence Identification Characteristics for Irradiated Dried Fishery Products (조사처리한 건조수산품의 전처리 방법에 따른 Luminescence 판별 특성)

  • Kim, Moon-Young;Ahn, Jae-Jun;Kim, Gui-Ran;Kwak, Ji-Young;Park, Kun-Sang;Lee, Kyung-Jin;Kwon, Joong-Ho
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.42 no.11
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    • pp.1837-1842
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    • 2013
  • Photostimulated luminescence (PSL) and thermoluminescence (TL) analyses were conducted for the detection of different gamma-irradiated dried fishes (mussel, squid, beka squid, mitra squid, plaice, and saury) at 0, 1, 5 and 10 kGy. For TL analysis, the contaminating silicate minerals were obtained by density separation or acid hydrolysis treatment. PSL determinations indicated that all the non-irradiated samples showed PSL photon counts/60 s (PCs) lower than 700 PCs (negative), but the irradiated mussel sample at 5 and 10 kGy were only possibility identified showing higher than 5000 PCs (positive). Irrespective of sample kinds and methods of mineral separation, all the non-irradiated samples showed TL glow curves in low-intensity with a maximum peak only after $250^{\circ}C$. However, all the irradiated samples produced TL glow curves in high intensity with a maximum peak particularly in the temperature range of 1$150{\sim}250^{\circ}C$. In conclusion, more distinguishable TL results [glow curve, TL ratio ($TL_1/TL_2$)] were obtained from the marker minerals separated by acid hydrolysis rather than density method.

Synthesis of TiO2/active carbon composites via hydrothermal process and their photocatalytic performance (수열합성법에 의한 TiO2/active carbon 복합체의 제조 및 광촉매특성)

  • Kim, Dong Jin;Lee, Jin Hee;Lee, Byeong Woo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.23 no.5
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    • pp.241-245
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    • 2013
  • Granular bamboo-derived active carbons (AC) were impregnated (or coated) with $TiO_2$ nano crystalline powders. The photocatalytic activity of the $TiO_2$-impregnated active carbons ($TiO_2$/AC) were determined on the basis of the degradation rate of methylene-blue aqueous solution under UV irradiation. The active compounds of $TiO_2$ were impregnated onto the AC under moderate hydrothermal conditions (${\leq}200^{\circ}C$, pH 11). The mean size of $TiO_2$ particles calculated from BET surface area were found to be as 50 nm. The $TiO_2$ precipitates were coated on the cavities or pores on the surfaces of highly activated carbons. Since the hydrothermal process led to a lowering of the on-set temperature of the anatase-to-rutile transition of $TiO_2$ as low as $200^{\circ}C$, $TiO_2$ crystallites of a pure anatase or a mixed form with rutile were successfully coated on the AC depending on the synthesis temperatures.

365 nm LED laser treatment on beagle for gingival whitening without gum dermabrasion (잇몸 박피술 없는 치은 미백을 위한 비글에서 365 nm LED 레이저 치료)

  • Lee, Sung-Ho;Kim, Ryun Kyung;Seo, Na-Ri;Lim, Ho-Kyung;Byun, Soo-Hwan;Lim, Young-Joon;Kim, Soung-Min;Lee, Jong-Ho
    • Journal of Dental Rehabilitation and Applied Science
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    • v.32 no.2
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    • pp.117-122
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    • 2016
  • Purpose: Gingival whitening is one of dental treatment purposes which is close to treating aesthetic disorders. Initial gingival whitening treatment was done by dermabrasion using a high power Diode Laser. However, this treatment method cannot be free from any infection or pain after the treatment. Therefore, we have decided to progress gingival whitening treatment using a low power LED laser. Materials and Methods: The laser was irradiated on pork meat then the safety of output power, temperature change and skin denaturalization was measured. Bison 365 nm LED laser was irradiated on oral mucosal pigment of a 15 - 20 kg beagle for 15 min for 1 - 2 weeks, one or two times each. Any pigment loss was checked through Hematoxyline-Eosin staining. Results: The melanin pigments at the area of 365 nm LED Laser irradiation were decreased. Conclusion: The 365 nm LED Laser proposed in this study is considered to compensate the bleaching effect achieved by either using Diode laser or surgical methods.

Determination of Optimal Storage Condition for Pre-packed Hanwoo Loin

  • Seol, Kuk-Hwan;Park, Tu San;Oh, Mi-Hwa;Park, Beom-Young;Cho, Seong In;Lee, Mooha
    • Food Science of Animal Resources
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    • v.33 no.3
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    • pp.390-394
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    • 2013
  • The aim of this study was to determine the optimal storage condition of pre-packed Hanwoo beef without freezing. Hanwoo loin was purchased from a local distributor at 48 h after slaughter, then sliced in $1.5{\pm}0.5$ cm thickness, and packed in a polyethylene (PE) tray covered with linear low-density polyethylene (LLDPE) film. The studied factors to set the optimal storage condition were chamber temperature (5, 2.5 and $-1^{\circ}C$ for 14 d), cooling method (direct and indirect cooling system), and ultraviolet (UV) light irradiation for beef surface sterilization (0, 30, 60, and 120 min). The changes of pH, thiobarbituric acid reactive substances (TBARS) and number of aerobic bacteria were measured during storage. Beef samples stored in $-1^{\circ}C$ showed the minimal increasing rate in TBARS and microbial growth. After 15 d of storage, there was no significant difference in pH and TBARS values. However, the microbial population of beef stored in direct type cooling chamber ($4.25{\pm}0.66$ Log CFU/g) was significantly lower than that of beef stored in indirect type chamber ($6.47{\pm}0.08$ Log CFU/g) (p<0.05). After 4 d of storage, 60 or 120 min UV light irradiated beef samples showed significantly lower microbial population, and at 14 d of storage, 60 min UV irradiated beef sample showed significantly lower microbial population ($3.14{\pm}0.43$ Log CFU/g) than control ($4.46{\pm}0.13$ Log CFU/g) (p<0.05). However, TBARS values of 60 or 120 min UV light irradiated beef samples were significantly higher than non-irradiated beef sample after 4 d of storage (p<0.05).

Batch Scale Storage of Sprouting Foods by Irradiation Combined with Natural Low Temperature -V. Cooking Qualities of Irradiated Chestnut after Long-term Storage- (방사선조사(放射線照射)와 자연저온(自然低溫)에 의한 발아식품(發芽食品)의 Batch Scale저장(貯藏)에 관(關)한 연구(硏究) -제5보(第五報) : 장기저장(長期貯藏)된 조사(照射)밤의 조리적성(調理適性)에 대하여-)

  • Yang, Ho-Sook;Kim, Jong-Gun;Cho, Han-Ok;Byun, Myung-Woo;Kwon, Joong-Ho
    • Korean Journal of Food Science and Technology
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    • v.15 no.3
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    • pp.238-244
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    • 1983
  • The cooking quality of irradiated chestnut after longterm storage were evaluated. 1. Color degree and tannin content of irradiated chestnut were slightly increased with the storage, but there was a little difference according to the radiation dose after nine months storage. 2. The main component of free sugars in the irradiated chestnut were identified as sucrose, glucose, fructose and the amino acids of chestnut were identified in the decreasing order of glutamic acid, aspartic acid, leucine, arginine, glycine, alanine, serine, pheylalanine, threonine, valine, isoleucine, tyrosine, methionine and cystein. Free sugars and amino acids of 25 Krad irradiated group showed a little difference compared with those of control group after nine months storage. 3. The calorie of candied chestnut prepared from nine months stored was marked 199 Kcal/100g of edible parts compared with 159 Kcal of raw chestnut. 4. Texture and sensory evaluation of candied chestnut prepared from nine months stored were better in 20-25 Krad irradiated group than in control group.

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Recycling Properties of Visible-Light Driven CdZnS/ZnO Photocatalyst Prepared by a Simple Precipitation Method (단순 침전법으로 제조한 가시광선용 CdZnS/ZnO 광촉매의 재활용 특성)

  • Lee, Gun Dae;Park, Seong Soo;Jin, Youngeup;Hong, Seong Soo
    • Clean Technology
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    • v.23 no.2
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    • pp.196-204
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    • 2017
  • CdZnS/ZnO composite was prepared through low-temperature precipitation and drying method. The property of CdZnS/ZnO as a recyclable photocatalyst for the degradation of rhodamine B (RhB) under visible light irradiation was examined. The sample was characterized by XRD, FE-SEM, XPS, UV-vis DRS and photoluminescence techniques before and after repeated reaction to investigate the change of properties during the photocatalytic reaction. During repeated reaction, the CdZnS/ZnO showed an improved photocatalytic activity and recycle stability. Among two feasible reaction pathways for photocatalytic degradation of RhB, the cleavage of conjugated chromophore was found to predominate over N-dealkylation of chromophore skeleton in the present work. The results indicate that the CdZnS/ZnO, prepared by a simple precipitation method, can be used as a visible-light driven photocatalyst with enhanced cycle stability and activity.

Luminescence Detection Characteristics for Irradiated Dried Fishes Using PSL-TL System (Photostimulated luminescence-thermoluminescence 분석체계를 이용한 조사 처리된 건어류의 luminescence 판별 특성)

  • Kim, Moon-Young;Kim, Gui-Ran;Ahn, Jae-Jun;Park, Kun-Sang;Kim, Eun-Jeong;Lee, Kyung-Jin;Kwon, Joong-Ho
    • Korean Journal of Food Science and Technology
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    • v.45 no.1
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    • pp.8-12
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    • 2013
  • Photostimulated luminescence (PSL) and thermoluminescence (TL) analyses were conducted for the detection of different irradiated dried fishes. All the non-irradiated samples provided PSL counts of lower than 700 (negative: $T_1$). Clear identification of irradiated sample was only possible for irradiated anchovy with PSL counts >5000; however, the results were unsatisfactory (not positive) for irradiated cod, dried filefish, hairtail, and herring samples. The contaminating silicate minerals were obtained by density separation or acid hydrolysis to perform TL analysis, which resulted in a low intensity of TL glow curve with a maximum peak after $250^{\circ}C$ for the non-irradiated samples that are irrespective of their kinds and methods for the mineral separation. The TL glow curves of high intensity with maximum peak in the temperature range of $150-250^{\circ}C$ were observed for all the irradiated samples. However, better results of TL glow curves and particularly of the TL ratio ($TL_1/TL_2$) were obtained when the minerals were separated by a acid hydrolysis method.

The Study on Filling Factor of Radiation Shielding Lead-free Sheet Via Screen Printing Method (스크린 프린팅 공법을 통한 방사선 무연 차폐 시트에 관한 연구)

  • Kang, Sang-Sik;Jeong, Ah-Rim;Lee, Su-Min;Yang, Seung-Woo;Kim, Kyo-Tae;Heo, Ye-Ji;Park, Ji-Koon
    • Journal of the Korean Society of Radiology
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    • v.12 no.6
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    • pp.713-718
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    • 2018
  • In many previous studies, monte carlo simulation is used to produce lead-free shielding sheet, and the possibility of radiation shielding capability and weight reduction is presented. But it is difficult to simulation for binder and micro-pores because of In fact it does not provide sufficient information necessary for the commercialization process. Therefore, in this paper, the results of radiation shielding capability corresponding to filling factor was presented by using the screen printing method to provide information on gel-paste required for the commercialization process. In this study, the geometric setup for evaluate of radiation shielding ability was designed to comply with IEC 61331-1:2014 and KS A 4025. In addition, radiation irradiation conditions were 100 kVp filtered with 2.0 mmAl total filtration was applied according to KS A 4021 standard. In this study, Pb $1270{\mu}m$, $BaSO_4$ $3035{\mu}m$, $Bi_2O_3$ $1849{\mu}m$ and $WO_3$ $2631{\mu}m$ were analyzed based on ten value layer. Additionally, the filling factor was analyzed as $BaSO_4$ 38.6%, $Bi_2O_3$ 27.1%, $WO_3$ 30.15%. However, in the case of applying low-temperature high-pressure molding in the future, it is expected that the radiation shielding capability can be sufficiently improved by reducing the porosity while increasing the filling factor.

Photocatalytic Decomposition of Rhodamine B over BiVO4 Doped with Samarium Ion (Sm 이온이 도핑된 BiVO4에서 로다민 B의 광촉매 분해 반응)

  • Hong, Seong-Soo
    • Clean Technology
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    • v.27 no.2
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    • pp.146-151
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    • 2021
  • Pure and Sm ion doped BiVO4 catalysts were synthesized using a conventional hydrothermal method and characterized by XRD, DRS, SEM, and PL. We also examined the activity of these materials on the photocatalytic decomposition of rhodamine B under visible light irradiation. The doping of Sm ion into BiVO4 catalyst changed the ms-BiVO4 crystal structure into the tz-BiVO4 crystal structure in the low synthesis temperature. Light absorption analysis using DRS showed that all the catalysts displayed strong absorption in the visible range of the electromagnetic spectrum regardless of Sm ion doping. In addition, an amorphous morphology was shown in the pure BiVO4 catalyst, but the morphology of the BiVO4 catalyst doped with Sm ion was changed into an ellipse shape and also the particle size decreased. In the photocatalytic decomposition of rhodamine B, Sm ion doped BiVO4 catalyst showed higher photocatalytic activity than the pure BiVO4 catalyst. In addition, the Sm3-BVO catalyst doped with 3% Sm ion showed the highest photocatalytic activity, as well as the highest formation rate of OH radicals (•OH) and the highest PL peak. This result suggests that the formation rate of OH radicals produced in the interface between the photocatalyst and water is well correlated with the photocatalytic activity.

Adsorption and Regeneration Characteristics of Ammonia on NiCl2 Impregnated Adsorbents (NiCl2 첨착된 흡착제 상에서 암모니아의 흡착 및 재생 특성)

  • Lim, Jeong-Hyeon;Song, Kang;Park, Chu-Sik;Kim, Young-Ho
    • Applied Chemistry for Engineering
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    • v.33 no.2
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    • pp.202-209
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    • 2022
  • Effects of the support and amount of NiCl2 on ammonia adsorption capacity were investigated to improve the ammonia adsorption performance. NiCl2 was impregnated onto the surface of various supports under ultrasonic irradiation. The physicochemical properties and ammonia adsorption performance of NiCl2-impregnated adsorbents were investigated. Among the various supports, it was found that the adsorption capacity of ammonia was the best when NiCl2 was impregnated on activated carbon (AC) with the highest specific surface area. As a result of changing the amount of NiCl2 impregnated on AC, the NiCl2(2.0)/AC adsorbent impregnated with 2 mmol·g-1 of NiCl2 showed the highest ammonia adsorption capacity of 5.977 mmol·g-1. In addition, the adsorption capacity was found to be maintained at an almost constant level in five repeated cycle tests under the condition that low-temperature heat could be utilized. This indicates that the adsorbent has excellent regeneration ability.