• Title/Summary/Keyword: loss modulus (E")

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Measurement of Dynamic Compressive Properties of Apples using the Oscillatory Test

  • Lee, Jong-Whan;Tan, Jinglu;Waluyo, Sri
    • Journal of Biosystems Engineering
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    • v.37 no.1
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    • pp.28-35
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    • 2012
  • Purpose: This study performed the oscillatory test using the texture analyzer to characterize the viscoelastic behavior of apples such as the storage modulus (E'), the loss modulus (E"), the complex modulus (${\mid}E^*{\mid}$) and the energy dissipated per cycle ($W_{diss}$). Methods: The sinusoidal deformation with the frequency of 1-10 Hz and the maximum displacement of 0.1 mm were applied to the flesh tissues of Fuji, Golden Delicious and Red Delicious apples. The Lissajous figure was used to measure the phase angle(${\delta}$) between stress and strain curve. Results: Trigger force was critical to the measurement of the phase angle. E', E", ${\mid}E^*{\mid}$ and Wdiss were measured using the Lissajous figure and the phase angle. The complex modulus of Golden Delicious apple was significantly lower than those of Fuji apple and Red Delicious apple. Conclusions: Apple flesh was exhibiting more elasticity at low frequency, and more viscosity at high frequency. Dynamic compressive properties of Fuji apple were similar to those of Red Delicious apple but significantly different from those of Golden Delicious apple.

A Study of Dynamic Viscoelastic Properties on Temperatures of Natural Rubber (천연고무의 온도에 따른 동적 점탄성 연구)

  • Lee, Bum-Chul;Yoo, Kil-Sang
    • Elastomers and Composites
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    • v.32 no.1
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    • pp.29-36
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    • 1997
  • The change of elastic modulus(E'), loss modulus(E"), and loss $tangent(tan{\delta})$ were investigated on condition of double strain amplitude (DSA) at temperature of $-40{\sim}80^{\circ}C$ for carbon black filled natural rubber. E', E", and $tan{\delta}$ were increased as it closed to the glass transition temperature due to decrease of rubber network flexibility and carbon black agglomerate interaction. In the micro strain range, energy loss showed maximum value because of the chain slippage in rubber matrix, but the regeneration of carbon black agglomerate and rubber matrix affected decrease of energy loss over the mid-range strain. As a results of regression analysis, $E'\;_{max}$ correlation with ${\Delta}E'$ $(E'\;_{0.4%DSA}-E'\;_{2.0%DSA})$ showed linear relationship.

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Damping Properties of Plastic with Temperature Variation (온도변화에 따른 플라스틱의 진동감쇠특성)

  • Shin, Su-Hyun;Jung, Sung-Soo;Lee, Yong-Bong;Lee, Doo-Hee;Nam, Hyo-Duk
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.15 no.2 s.95
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    • pp.213-218
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    • 2005
  • It is well known that the loss factor and Young's modulus are fundamental mechanical properties of materials. Recently, the use of complex plastics is increasing for vibration proof. In this study, we evaluated two mechanical values of polycarbonate and acrylonitrile butadiene styrene by using two different standard test methods of ASTM E 756 and ISO 6721. Because damping properties of material generally depend on temperature, test specimen‘s temperature were controlled in the temperature range between - $10^{\circ}C\;and\;60^{\circ}C$. The results shown that the loss factor of polycarbonate gradually increased as increasing temperature, while the Young's modulus decreased. However, the loss factor and the Young's modulus of acrylonitrile butadiene styrene are varied somewhat at $60^{\circ}C$.

Viscoelastic Properties of MF/PVAc Hybrid Resins as Adhesive for Engineered Flooring by Dynamic Mechanical Thermal Analysis

  • Kim, Sumin;Kim, Hyun-Joong;Yang, Han-Seung
    • Journal of the Korean Wood Science and Technology
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    • v.34 no.2
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    • pp.37-45
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    • 2006
  • The viscoelastic properties of blends of melamine-formaldehyde (MF) resin and poly(vinyl acetate) (PVAc) for engineered flooring used on the Korean traditional ONDOL house floor heating system were investigated by dynamic mechanical thermal analysis (DMTA). Because MF resin is a thermosetting adhesive, the effect of MF rein was shown across all thermal behaviors. The addition of PVAc reduced the curing temperature. The DMTA thermogram of MF resin showed that the storage modulus (E') increased as the temperature was further increased as a result of the cross-linking induced by the curing reaction of the resin. The storage modulus (E') of MF resin increased both as a function of increasing temperature and with increasing heating rate. From isothermal DMTA results, peak $T_{tan{\delta}}$ values, maximum value of loss modulus (E") and the rigidities (${\Delta}E$) of MF/PVAc blends at room temperature as a function of open time, peak $T_{tan{\delta}}$ and maximum loss modulus (E") values were found to increase with blend MF content. Moreover, the rigidities of the 70:30 and 50:50 MF/PVAc blends were higher than those of the other blends, especially of 100% PVAc or MF. We concluded that blends the MF/PVAc blend ratios correlate during the adhesion process.

Study of the Measurement of Young's Modulus and Loss Factor for a Viscoelastic Damping Material Using a Multi Degree of Freedom Curve Fitting Method and RKU Equation (다자유도 곡선 맞춤법과 RKU 기법을 이용한 점탄성 감쇠재의 탄성 및 손실계수 추정방법 연구)

  • Min, Cheon-Hong;Park, Han-Il;Bae, Soo-Ryong;Jeon, Jae-Jin
    • Journal of Ocean Engineering and Technology
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    • v.25 no.1
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    • pp.67-72
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    • 2011
  • Offshore structures, such as a platform, a buoy, or a floating vessel, are exposed to several dynamic loads, and viscoelastic damping material is used to reduce the vibration of offshore structures. It is important to know the properties of viscoelastic materials because loss factor and Young's modulus of the viscoelastic damping material are dependent on frequency and temperature. In this study, an advanced technique for obtaining accurate loss factor and Young's modulus of the viscoelastic damping material is introduced based on a multi degree of freedom curve-fitting method and the RKU (Ross-Kerwin-Ungar) equations. The technique is based on a modified experimental procedure from ASTM E 756-04. Loss factor and Young's modulus of the viscoelastic damping material are measured for different temperatures by performing the test in a temperature-controlled vibration measurement room where temperature varies from 5 to 45 degrees Celsius.

Measuring of Loss factor and Young's modulus of Plastics with Temperature Variation (온도변화에 따른 플라스틱의 손실계수와 Young 률의 측정)

  • Shin Su Hyun;Jung Sung Soo;Lee Yong Bong;Lee Doo Hee
    • Proceedings of the Acoustical Society of Korea Conference
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    • autumn
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    • pp.321-322
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    • 2004
  • It is well known that the loss factor and Young's modulus are fundamental mechanical properties of materials. In this study. the dynamic characteristics of plastics are evaluated by using two different standard test methods which are ASTM E 756 and ISO 6721. Polycarbonate and acrylonitrile butadiene styrene were used as test specimens. In order to evaluate vibration of damping properties with temperature, we measured loss factor and Young's modulus of the specimens the temperature range between $-10^{\circ}C$ and $60^{\circ}C$. The Young's modulus for polycarbonate decreased significantly as increasing temperature, while the loss factor increased. However, the Young's modulus and loss factor of acrylonitrile butadiene styrene are varied somewhat with temperature.

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Comparison of Test Methods for Vibration Damping Properties (진동감쇠특성 시험법 비교)

  • Shin Su Hyun;Lee Yong Bong;Jung Sung Soo;Lee Doo Hee
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.14 no.9 s.90
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    • pp.852-860
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    • 2004
  • There are many standard methods for measuring vibration damping properties of the beam type material. Among them, three standards ASTM E 756, ISO 6721 and JIS G 0602, are compared. Loss factor and Young's modulus of the steel beam are evaluated by using five different methods and their results are compared. Logarithmic decay method and half-power bandwidth method are used to calculate the loss factor. It was observed that Young’s modulus is agree well, but loss factors are different from test to test. So the same test method must be applied to measure damping properties.

Effect of Chromium Chloride on the Mechanical and Dielectric Properties of EPDM Rubber

  • Salem, M.A.;Khaled, M.A.;Hussein, A.M.;Elway, E.
    • Macromolecular Research
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    • v.11 no.4
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    • pp.256-259
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    • 2003
  • Measurements of Young's modulus, dielectric loss and a.c. conductivity have been carried out on EPDM rubber samples loaded with different concentrations of $CrCl_3$ (0,2,4 and 6 phr). The values of Young's modulus was found to be linearly dependent on the $CrCl_3$ content. Variation of the dielectric loss with temperature showed that $CrCl_3$ may act as plasticizer. However, at higher frequencies the dielectric loss was found to be independent of frequency and the rubber samples may behave as non-polar dielectric. Investigations of the a.c conductivity suggested that the conduction in these rubber samples can be described by small polaron tunneling. In addition, conductivity was found to increase with $CrCl_3$ content.

Understanding the Viscoelastic Properties and Surface Characterization of woodflour-Polypropylene Composites (목분-폴리프로필렌 복합재의 점탄성적 성질과 표면특성)

  • Son, Jungil;Gardner, Douglas J.
    • Journal of Adhesion and Interface
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    • v.3 no.4
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    • pp.1-9
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    • 2002
  • The main goal of this study was to analyze the effect of process additives, i.e. maleated polypropylene (MAPP), and nucleating agent on the viscoelastic properties of different types of extruded polypropylene-wood plastic composites manufactured from either PP homopolymer, high crystallinity PP or PP impact copolymer using dynamic mechanical thermal analysis. And also, the esterification reaction between wood flour and maleated polypropylene, and its role in determining the mechanical properties of wood flour-polypropylene composites was investigated. The wood plastic composites were manufactured using 60% pine wood flour and 40% polypropylene on a Davis-Standard $Woodtruder^{TM}$. Dynamic mechanical thermal properties, polymer damping peaks(than ${\delta}$), storage modulus (E') and loss modulus (E") were measured using a dynamic mechanical thermal analyzer. XPS (X-ray Photoelectron Spectroscopy), also known as ESCA (Electron Spectroscopy for Chemical Analysis) study of wood flour treated with MAPP was performed to obtain information on the chemical nature of wood fiber before and after treatment. To analyze the effect of frequency on the dynamic mechanical properties of the various composites, DMA tests were performed over a temperature range of -20 to $100^{\circ}C$, at four different frequencies (1, 5, 10 and 25 Hz), and at a heating rate of $5^{\circ}C/min$. From these results, the activation energy of the various composite was measured using an Arrhenius relationship to investigate the effect of maleated PP and nucleating agent on the measurement of the interphase between the wood and plastic of the extruded polypropylene wood plastic composites.

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Thermal Properties of Corn-Starch Filled Biodegradable Polymer Bio-Composites (옥수수 전분을 충전제로 첨가한 생분해성 고분자 복합재료의 열적성질)

  • Kim, Hee-Soo;Yang, Han-Seung;Kim, Hyun-Joong;Lee, Young-Kyu;Park, Hee-Jun
    • Journal of the Korean Wood Science and Technology
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    • v.32 no.5
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    • pp.29-38
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    • 2004
  • In this study, we investigated the thermal properties of corn-starch filled polybutylene succinate-adipate (PBS-AD) bio-composites. Thermal analysis (TA) is used to describe the analytical method for measuring the chemical property and weight loss of composite materials as a function of temperature. The thermal stability of corn-starch was lower than that of pure PBS-AD. As corn-starch loading increased, the thermal stability and degradation temperature of the bio-composites decreased and the ash content increased. It can be seen that the degree of compatibility and interfacial adhesion of the bio-composites decreased because of the increasing mixing ratio of the corn-starch. As the content of corn-starch increased, there was no significant change in the glass transition temperature (Tg) and the melting temperature (Tm) for the bio-composites. The storage modulus (E') and loss modulus (E") of the corn-starch flour filled PBS-AD bio-composites were higher than those of PBS-AD, because of the incorporation of corn-starch increased the stiffness of the bio-composites. At higher temperatures, the decreased storage modulus (E') of bio-composites was due to the increased polymer chain mobility of the matrix polymer. From these results, we can expect that corn-starch has potential as a reinforcing filler for bio-composites. Furthermore, we recommend using a coupling agent to improve the interfacial adhesion between corn-starch and biodegradable polymer.