• Elastomers and Composites
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• v.34 no.1
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• pp.11-19
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• 1999

Rebound, storage and loss modulus, and tan ${\delta}$ were investigated on cured rubbers with various ratios of sulfur to accelerator and the volume fraction of carbon black in the cured rubbers. The rebound was increased as the sulfur to accelerator ratio and the volume fraction of carbon black decreased. The storage modulus decreased as the loading of carbon black and the strain increased regardless of the cure systems. The network structure formed by filler-filler interaction was destroyed above 6% strain regardless of the loading of carbon black, because constant storage modulus was shown at the higher strain than 3% for $40{\sim}50phr$ loading of carbon black and at the higher strain than 6% for 60 phr and above loading of carbon black. Little effect on loss modulus was found at the low loading of carbon black, but the peak of loss modulus was shown at 1% strain as the loading of carbon black was increased. Tan ${\delta}$ increased as the loading of carbon black and the strain were increased regardless of the cure system, and maximum tan ${\delta}$ was shown at 2% strain regardless of the loading of carbon black.

• The Journal of the Acoustical Society of Korea
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• v.37 no.5
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• pp.338-342
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• 2018

In order to solve the floor impact sound problem in the upper and lower floors, the Ministry of Land, Transport and Maritime Affairs also notifies the physical properties of the resilient material affecting the floor impact sound level. The dynamic modulus of elasticity and the loss factor before and after heating are most related to the floor impact noise, especially for the cushioning material. Therefore, in this study, the rate of change with respect to the dynamic modulus and loss factor with temperature change was examined by increasing $10^{\circ}C$ by $10^{\circ}C$ from the temperature condition of $70^{\circ}C$ specified in the standard. The dynamic modulus of elasticity and the loss modulus were measured by using the pulse excitation method for eight kinds of samples. The calculation method was calculated by the time series analysis method using the damped vibration waveform.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2001.05a
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• pp.19-22
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• 2001

This paper proposes a double cantilever sandwich-beam method for evaluating the frequency dependence of material dynamic characteristics. The flexural vibration of a double cantilever sandwich-beam specimen with a partially inserted rubber layer was studied using a finite element simulation in combination with the sine-sweep test. Quadratic relationships of dynamic elastic modulus and material loss factor of rubbers with frequency were quantitatively suggested employing the least square error method.

• Composites Research
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• v.23 no.1
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• pp.17-22
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• 2010

The compressive and dynamic properties of magnetorheological elastomers were investigated as functions of magnetizable particle volume fraction, alignment of the embedded particle and magnetic force. The specimens consisted of pure and filled silicons with randomly dispersed, longitudinal and transverse aligned magnetizable particle chains. To align the embedded particles in the elastomer, the cross-linking of the elastomer composites took place in a magnetic field. The compression and dynamic tests in the absence and the presence of different magnetic forces were carried out. The modulus and loss factor of the elastomer composites increase with increasing volume fraction at the same magnetic force. The case of longitudinal alignment shows a high modulus and loss factor when compared to the case of transverse alignment or random dispersion.

• Korean Journal of Materials Research
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• v.21 no.7
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• pp.377-383
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• 2011

Thermoelectric power, dc conductivity, and the dielectric relaxation properties of $La_2NiO_{4.03}$ are reported in the temperature range of 77 K - 300 K and in a frequency range of 20 Hz - 1 MHz. Thermoelectric power was positive below 300K. The measured thermoelectric power of $La_2NiO_{4.03}$ decreased linearly with temperature. The dc conductivity showed a temperature variation consistent with the variable range hopping mechanism at low temperatures and the adiabatic polaron hopping mechanism at high temperatures. The low temperature dc conductivity mechanism in $La_2NiO_{4.03}$ was analyzed using Mott's approach. The temperature dependence of thermoelectric power and dc conductivity suggests that the charge carriers responsible for conduction are strongly localized. The relaxation mechanism has been discussed in the frame of the electric modulus and loss spectra. The scaling behavior of the modulus and loss tangent suggests that the relaxation describes the same mechanism at various temperatures. The logarithmic angular frequency dependence of the loss peak is found to obey the Arrhenius law with activation energy of ~ 0.106eV. At low temperature, variable range hopping and large dielectric relaxation behavior for $La_2NiO_{4.03}$ are consistent with the polaronic nature of the charge carriers.

• Journal of the Korean Wood Science and Technology
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• v.34 no.2
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• pp.37-45
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• 2006

The viscoelastic properties of blends of melamine-formaldehyde (MF) resin and poly(vinyl acetate) (PVAc) for engineered flooring used on the Korean traditional ONDOL house floor heating system were investigated by dynamic mechanical thermal analysis (DMTA). Because MF resin is a thermosetting adhesive, the effect of MF rein was shown across all thermal behaviors. The addition of PVAc reduced the curing temperature. The DMTA thermogram of MF resin showed that the storage modulus (E') increased as the temperature was further increased as a result of the cross-linking induced by the curing reaction of the resin. The storage modulus (E') of MF resin increased both as a function of increasing temperature and with increasing heating rate. From isothermal DMTA results, peak $T_{tan{\delta}}$ values, maximum value of loss modulus (E") and the rigidities (${\Delta}E$) of MF/PVAc blends at room temperature as a function of open time, peak $T_{tan{\delta}}$ and maximum loss modulus (E") values were found to increase with blend MF content. Moreover, the rigidities of the 70:30 and 50:50 MF/PVAc blends were higher than those of the other blends, especially of 100% PVAc or MF. We concluded that blends the MF/PVAc blend ratios correlate during the adhesion process.

• The Journal of the Acoustical Society of Korea
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• v.21 no.1E
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• pp.12-17
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• 2002

Two improvements are discussed in measurement of the complex Young's modulus of the acoustic materials by using the transfer function method. It is found that the accelerometer misalignment might result in the severe measurement error, particularly in high frequency range. The supporting structure is modified to attach the upper and lower accelerometers along the vertical axis. Secondly, the method fur solving the equation associated with wave model is described. The solution of the lumped mass-spring model is chosen as the starting value for low frequency range, while in the mid and high frequency, the solution to the previous frequency step is used as the initial values. Measurements are done for hard and soft rubber specimens. It is shown that the erroneous peaks in the transfer function, due to the measurement error, cause highly incorrect Young's modulus and loss factors.

• Proceedings of the KSR Conference
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• 2007.11a
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• pp.852-858
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• 2007

The durability of carbon/epoxy composites under salt water environment was investigated through salt water spray tester. Salt water environment was obtained through salt spray and salt immersion. 5% NaCl solution was used for salt water as natural salt water. Mechanical test was performed to obtain tensile properties, flexural properties, and shear properties of carbon/epoxy composite over 12 months under salt water environment. Dynamic mechanical analyzer was used to investigate thermal analysis properties such storage modulus, loss modulus, and tan ${\delta}$. Also FT/IR test was conducted to investigate a change in chemical structure. According to the results, mechanical properties were found to be slowly degraded as a function of exposure times. Regarding to thermal analysis properties, storage modulus was insensitive to exposure times, but loss modulus was shown to be slightly decreased. Although the shape and location of peak in FT/IR were not much changed, the intensity of peak in FT/IR was affected on exposure times. We also found that salt water immersion was more severe to the durability of carbon/epoxy composite rather than salt water spray.

• International Journal of Highway Engineering
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• v.16 no.3
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• pp.43-50
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• 2014

PURPOSES : The dynamic modulus can be determined by applying the various theories from the Impact Resonance Testing(IRT) Method. The objective of this paper is to determine the best theory to produce the dynamic modulus that has the lowest error as the dynamic modulus data obtained from these theories(Complex Wave equation Resonance Method related to either the transmissibility loss or not, Dynamic Stiffness Resonance Method) compared to the results for dynamic modulus determined by using the Universal Testing Machine. The ultimate object is to develop the predictive model for the dynamic modulus of a Linear Visco-Elastic specimen by using the Complex Wave equation Resonance Method(CWRM) came up for an existing study(S. O. Oyadiji; 1985) and the Optimization. METHODS : At the destructive test which uses the Universal Testing Machine, the dynamic modulus results along with the frequency can be used for determining the sigmoidal master curve function related to the reduced frequency by applying Time-Temperature Superposition Principle. RESULTS : The constant to be solved from Eq. (11) is a value of 14.13. The reduced dynamic modulus obtained from the IRT considering the loss factor related to the impact transmissibility has RMSE of 367.7MPa, MPE of 3.7%. When the predictive dynamic modulus model was applied to determine the master curve, the predictive model has RMSE of 583.5MPa, MPE of 3.5% compared to the destructive test results for the dynamic modulus. CONCLUSIONS : Because we considered that the results obtained from the destructive test had the most highest source credibility in this study, the dynamic modulus data obtained respectively from DSRM, CWRM were compared to the results obtained from the destructive test by using th IRT. At the result, the reduced dynamic modulus derived from DSRM has the most lowest error.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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• 2003.11a
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• pp.700-703
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• 2003

The test method of ASTM E 756 and KS D 0076 to estimate vibration-damping properties is compared. Comparison method depending on specimen support, exciting method and calculation method for loss factor is used. Half-power bandwidth method and vibration decay method is used in the calculation method for loss factor, and Young's modulus is decided by geometric character and density for specimen and resonance frequency. Vibration measurement sensor is compared by using non-contact displacement detector, velocity detector and accelerometer. This paper is also presented the matter which is able to cause error in the measurement