• Textile Coloration and Finishing
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• v.15 no.6
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• pp.39-46
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• 2003

The experiments about dyeing concentration, temperature and time were done using yellow, red and purple loess as natural inorganic dyes in order to verify a degree of dyeing, characteristics of color and fastness. The results were as following; 1. As a result of analyzing components of loess, purple loess was much than other loess in quartz component and coarse particles contained. This affected to the degree of dyeing. 2. The stronger dyeing concentration was, the more the degree of dyeing was improved, and yellow loess containing fine particles was the best in the degree of dyeing. 3. When it was dyed with raising up to $100^\circ{C}$ for 10 minutes after stirring for 20 minutes at $60^\circ{C}$, was better than on starting at $40^\circ{C}$ or $80^\circ{C}$ in the degree of dyeing. Also yellow loess was the best in these experiments. 4. Washing fastness of loess was low such as other natural dyes, but dyeing wasn't transferred to other textiles. On the other hand, light fastness of it was very excellent and rubbing fastness was relatively good as 3~3.5.

• Journal of the Korean Society of Clothing and Textiles
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• v.24 no.5
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• pp.619-627
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• 2000

Historically, dyed textiles were symbols of status and, because of their expense, reserved only for people of wealth and specalist, Early dye sources probably included plant, animal and mineral extracts. As synthetic dyes have been developed, beginning with synthetic indigo in 1897, reliance on natural dye sources diminished. But renewed interest in natural dyes is fueled by a pro-environment consumer aware of the ecological liabilities of the dye industry. Han Jee was imported from China where it was influenced to period of the three kingdoms(Silla, Baekje, Kokuryo). After that, Han Jee was used for paper in old Korea for long thime before paper was came with civilization. In this paper, dyeing of Han Jee with loess were investigated according to dyeing temperature, dyeing time, loess concentration, and effects of additives. As a reuslts, λmax of Han Jee dyed by loess was 710nm. ΔE values of Han Jee increased by loess concentration, dyeing time, dyeing temperature. Dyeing with additives treatment increased dyeability. Especially, Han Jee treated with aluminium acetate shows the largest dyeability of the Han Jee. The Han Jee dyed loess had very good lightfastness.

• International Journal of Human Ecology
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• v.8 no.2
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• pp.99-106
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• 2007

In this study, the mechanical properties related to the fabric appearance of well being functional bamboo knitted fabric before and after loess dyeing were evaluated. The mechanical properties of fabrics were measured by KES-F system, that is, shape retention, draping, wrinkle recovery, compression property, and surface properties, and total hand value of three types of knitted fabric, 100% bamboo, 100% cotton, and bamboo / cotton blend (60 / 40) were evaluated before and after loess dyeing. As a result, it was found that appearance density, shape retention, and drape coefficient of cotton knitted fabric were greater than those of bamboo knitted fabric. After loess dyeing, shape retention and drape coefficient, wrinkle recovery of bamboo knitted fabric improved and WC/C and MMD/SMD decreased. According to THV, the hand of bamboo/cotton blend knit is the best among three samples by compensation the weak properties of the two fiber. Therefore, loess dyeing seemed to be a good method for improving shape retention and hand value of 100% bamboo and bamboo blended fabric.

• Fashion & Textile Research Journal
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• v.17 no.6
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• pp.1004-1012
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• 2015

The purpose of this study is to investigate the loess dyeability of soybean fabric using loess as colorants. Recent days, various textile products such as inner wears, sheets and interior goods are manufactured using materials dyed with loess emphasizing its improved metabolism, anti-bacterial, deodorizing properties, and far infrared ray emissions. Soybean fabric was dyed with loess solution according to concentration of loess, dyeing temperature and dyeing time. To improve washing fastness, soybean fabric and dyed soybean fabric with loess were mordanted by mordanting agents such as sodium chloride(NaCl), Acetic acid(CH₃COOH) and Aluminium Potassium Sulfate(AlK(SO₄)₂·12H₂O). Dyeability and color characteristics of dyed soybean fabric were obtained by CCM observation. Particle size distribution of loess, the dyeability(K/S) of soybean fabric, morphology and washing durability of loess dyed soybean fabric were investigated. The results obtained were as follows; Mean average diameter of loess was 1.08µm. The main components of loess used in this study were silicon dioxide(SiO₂), aluminium oxide(Al₂O₃), and iron oxide(Fe₂O₃). The content of these three component was above 75 weight %. The dyeability of soybean fabric was increased gradually with increasing concentration of loess. The optimum dyeing temperature and dyeing time were 90℃ and 60minutes expectively. The fastness to washing according to concentration of loess and mordanting method indicated good grade result as more than 4 degree in all conditions.

• Fashion & Textile Research Journal
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• v.2 no.2
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• pp.118-122
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• 2000

Dyeing properties of silk fabric with loess were studied by investigating the effect of dyeing conditions, such as concentration of loess, dyeing temperature and time, on dye uptakes. And also the effects of mordant and mordanting methods on color change and dye uptakes were inverstigated. For the practical use, the various color fastness of dyed fabric were evaluated. The dye uptakes of dyed fabric were increased gradually with increasing concentration of loess, dyeing time and temperature. The K/S value of dyed fabric most efficient for the premordanting method. The color fastness was improved when mordants were added.

• Textile Coloration and Finishing
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• v.17 no.2 s.81
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• pp.1-9
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• 2005

Mixed dyeing were carried out ll"ing yellow, red and purple loess as mineral dyes verify their dyeability, color shade and fastness. The proper density of Chinese ink were 0.5, 1.0, 2.0, 2.5, $5\%$(o.w.b). The grinded chinese ink had better stainability compared with the general Chinese ink. The mixed dyeing improvement of stainability in the density of loess of $40\%$(o.w.b) among the yellow, red, and purple loess. The colors in the mixed dyeing with Chinese ink were $3.801\~8.13Y,\;0.128\~7.038Y\;and\;4.222\~9.304Y$. The colorfastness were 1-2 in the homogeneous dyeing with Chinese ink. It was improved 1-3 in the mixed dyeing. Light colorfastness of the homogeneous and mixed dyeing were excellent as a value of 5. The dry rubbing fastness in the homogeneous dyeing was 3-3.5, and 3 in the wet rubbing. As for the mixed dyeing, the dyes of Chinese ink showed poor diffusion into the fiber, resulting in low fastness due to the existence of the dyes on the surface.

• Journal of the Korean Society of Clothing and Textiles
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• v.21 no.3
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• pp.600-606
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• 1997

The dyeing with loess has been studied. Two kinds of cotton fabrics having different thickness and density were dyed in loess paste bath. The color differences of the fabrics which were dyed repeatedly.five times were not significant. The dyeing of cotton fabrics with loess was not exactly reproducible, but dyeability of the cotton fabrics of high density was better than that of low density. Loess on the dye6 fabrics was physically jammed between the fibers in the form of the fine particles. The cotton fabrics dyed with loess have good light fastness, but their laundering fastness and abrasion fastness were not good. An aftertreatment was carried out by using the extracted solution from acorn or persimon, and FeSO4 lot improving fastness. When the dyed fabrics was after-treated with FeSO4, the laundering fastness and wet abrasion fastness were improved extremely.

• Current Research on Agriculture and Life Sciences
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• v.31 no.3
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• pp.193-199
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• 2013

This study dyed rayon fabric using loess as a natural colorant. To obtain the optimal dyeing conditions, various dyeing conditions were examined (temperature, pH, time, and concentration). The color fastness was evaluated using standard washing and rubbing fastness tests. The results were as follows: The loess powder particle size ranged from 0.4 to $1.7{\mu}m$ with a distribution range of 1.1 to $1.4{\mu}m$, representing a fine and uniform manufactured loess powder. The loess component analysis showed a large amount of silicon dioxide and aluminum oxide. TheFT-IR spectra showed that the ammonium group in the rayon fabric produced N-H banding at $1,540cm^{-1}$. The highest K/S value for the rayon fabric was obtained when the pH was 8.0, and this value increased rapidly with a longer dyeing time and when increasing the loess concentration to 30% (w/v). Pre-treatment with a soybean solution produced the highest K/S value for the rayon fabric with a loess concentration of 30% (w/v). The SEM analysis showed a higher amount of loess adhered to the rayon fabric surface when increasing the loess concentration. However, pre-treatment with a cationic agent and soybean solution resulted in a much higher attachment of loess to the fabric surface. Thus, the experimental results showed that using a cationized fabric and pre-treatment with a soybean solution are more effective when dyeing rayon fabric with loess than when using only loess.

• Textile Coloration and Finishing
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• v.18 no.4
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• pp.1-10
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• 2006

Tannin treatment has been used for improving the color fastness of dyed materials. In natural dyeing, the tannin treatment is highly effective in improving the fastness. The chitosan treatment also improves the fastness and depth of shade in natural dyeing. In this study, the effects of tannin and chitosan pre-treatment on the color and fastness in loess dyeing were investigated. Cotton woven fabric specimens and cotton knit fabric specimens were pre-treated with chitosan solution in acetic acid, and the specimens were then treated with or without tannin. The specimens were finally dyed with loess. The tannin treatment decreased the K/S values, while the chitosan treatment increased the K/S. Both the tannin treatment and the chitosan treatment increased the wash fastness and light fastness. In tannin treatment, tannin component and Fe component of loess may react together to decrease the lightness and develop dark color. For maintaining inherent color of the loess, it is much preferable to employ chitosan treatment rather than tannin treatment.

• Fashion & Textile Research Journal
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• v.7 no.3
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• pp.327-332
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• 2005

The purpose of this study is to investigate the effect of chitosan treatment on the dyeing of cotton fabric specimens using loess as colorants. The wet pick up ratio of the chitosan acid solution, as well as the drying condition after the padding of the fabric specimens, was changed in order to study the loess uptake on the fabric. The average particle diameter of the loess was measured. Main components of the loess were $SiO_2$, $Al_2O_3$, and $Fe_2O_3$. By the chitosan treatment, the loess amount on the cotton fabric increased. 80% wet pick up ratio of the chitosan acid solution on the cotton fabric specimen allowed more stable and even adhesion of the loess on the fabric surface, compared to the cases of 100% and 120% wet pick up ratio.