• Title/Summary/Keyword: liquid-liquid-solid

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Microstructures and Deformation Behavior of AA 2014 Aluminum Alloys in the Semi-Solid State (AA 2014 알루미늄 합금의 고상율에 따른 미세조직 및 반응고 변형 거동)

  • Han, Do-Suck
    • Journal of Korea Foundry Society
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    • v.37 no.5
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    • pp.157-163
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    • 2017
  • In the present study, the microstructural evolution and deformation behavior of AA 2014 aluminum alloys with different microstructures in a semi-solid state were investigated. For a given alloy, applied load and deformation time, the measured strain was higher at a higher temperature, indicative of a lower solid fraction. When a large proportion of the liquid was present as intragranular droplets, the alloy would not as easily deform because the effective liquid fraction between the solid grains had decreased. Greater deformation was achieved with higher grain boundary misorientations due to the enhanced wetting of the grain boundaries with liquid. A semi-empirical constitutive model is proposed for semi-solid deformation under the conditions in the present study. The mechanism of semi-solid deformation incorporates the initial flow of the liquid in the early stages of deformation, followed by a more gradual increase in the strain due to deformation by grain sliding accompanied by self-diffusion in the solid grains.

Design and Development of Fluidized Bed Cleaning System for on Heat Treatment Parts (I) - Design and Development the Experimental Fluidized Bed Cleaner and Experiments on its Cleaning Efficiency - (유동층을 이용한 열처리부품의 세정 시스템 설계 및 개발 (I) -유동층 이용 세정 실험장치 설계, 개발 및 실험 -)

  • Kim C.S.;Kim K.D.
    • Journal of Biosystems Engineering
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    • v.31 no.4 s.117
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    • pp.376-384
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    • 2006
  • This study was conducted to perform for comparative analysis of the cleaning efficiency on 3 kinds of cleaning liquid state, 3 steps of cleaning temperature $(45^{\circ}C,\;60^{\circ}C,\;70^{\circ}C,\;)$ and 6 steps of cleaning time (2.5, 5, 7.5, 10, 12.5, 15 minute). 3 kinds of cleaning liquid state are the non fluidized bed, liquid fluidized bed and liquid/solid fluidized bed. UV spectrophotometer was used in estimation of cleaning efficiency, which it is experimental equipment using the absorptiometric analysis method. Cleaning efficiency by cleaning time was increase from 2.5 minutes to 15 minutes, liquid/siolid fluidized bed was indicated the highest cleaning efficiency among the 3 kinds of cleaning liquid state and $70^{\circ}C$ of cleaning temperature at liquid/solid fluidized bed was indicated the highest cleaning efficiency as 98% among the 3 steps of cleaning temperature.

Deformation Analysis of Solid-Liquid Coupled Structure using Explicit Finite Element Program (외연 유한요소 프로그램을 이용한 고체-액체 조합 구조물의 변형해석)

  • 최형연
    • Proceedings of the Computational Structural Engineering Institute Conference
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    • 2000.04b
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    • pp.150-155
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    • 2000
  • In this study, deformation analysis for solid-liquid coupled structure has been performed using explicit finite element program In order to model the behavior of liquid, SPH (Smooth Particle Hydrodynamics) algorithm was adopted. Crash test and simulation for the hydro-type impact energy absorber were given as an example of industrial application. The obtained good correlation between the test results and simulation reveals that the proposed method could be used effectively for the structural analysis of solid-liquid coupled problems

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In-situ HRTEM Studies of Alumina-Aluminum Solid-Liquid Interfaces

  • Oh, Sang-Ho;Scheu, Christina;Ruhle, Manfred
    • Applied Microscopy
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    • v.36 no.spc1
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    • pp.19-24
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    • 2006
  • The alumina-aluminum solid-liquid interfaces were directly observed at atomic scale by heating the alumina single crystal in high-voltage electron microscope (HVEM) owing to the electron beam damage processes, Atomic ordering in the first several layers of the liquid was clearly resolved adjacent to the alumina surface and its relevance to the single crystal growth was examined with the real-time observations.

Growth Characteristics of Amorphous Silicon Oxide Nanowires Synthesized via Annealing of Ni/SiO2/Si Substrates

  • Cho, Kwon-Koo;Ha, Jong-Keun;Kim, Ki-Won;Ryu, Kwang-Sun;Kim, Hye-Sung
    • Bulletin of the Korean Chemical Society
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    • v.32 no.12
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    • pp.4371-4376
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    • 2011
  • In this work, we investigate the growth behavior of silicon oxide nanowires via a solid-liquid-solid process. Silicon oxide nanowires were synthesized at $1000^{\circ}C$ in an Ar and $H_2$ mixed gas. A pre-oxidized silicon wafer and a nickel film are used as the substrate and catalyst, respectively. We propose two distinctive growth modes for the silicon oxide nanowires that both act as a unique solid-liquid-solid growth process. We named the two growth mechanisms "grounded-growth" and "branched-growth" modes to characterize their unique solid-liquid-solid growth behavior. The two growth modes were classified by the generation site of the nanowires. The grounded-growth mode in which the grown nanowires are generated from the substrate and the branchedgrowth mode where the nanowires are grown from the side of the previously grown nanowires or at the metal catalyst drop attached at the tip of the nanowire stem.

The Effects of Fabrication Conditions on Forging Limitation and Mechanical Property in Semi-Solid Forming Process (반용융 단조공정에 있어서 제조 조건이 성형성과 기계적 성질에 미치는 영향)

  • 정경득;강충길
    • Transactions of Materials Processing
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    • v.10 no.3
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    • pp.214-222
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    • 2001
  • The homogeneous distribution of solid region without liquid segregation is important in terms of high quality component during thixoforming process. In closed die semi-solid forging process, liquid segregation is strongly affected by injection velocity than solid fraction because the material has to travel relatively long distance to fill the cavity through a narrow gate. The designed die by computer simulation data was used to thixoforging process. The thixoforming velocity to prediction the liquid segregation had been determined with strain rate associated with multistage velocity control during compression test of semi-solid material. The optimal forging velocity and die temperature were investigated to produce the near-net-shape compressor component. The mechanical properties of thixoformed component were tested with various die and material temperatures before and after heat treatment.

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Holdup and Flow Behavior of Fluidized Solid Particles in a Liquid-Solid Circulating Fluidized Bed

  • Lim, Dae Ho;Lim, Ho;Jin, Hae Ryong;Kang, Yong
    • Korean Chemical Engineering Research
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    • v.52 no.3
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    • pp.371-377
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    • 2014
  • Characteristics of holdup and flow behavior of fluidized solid particles were investigated in a liquid-solid circulating fluidized bed ($0.102m{\times}3.5m$). Effects of liquid velocity ($U_L$), particle size ($d_P$) and solid circulation rate ($G_S$) on the solid holdup, overall particle rising velocity, slip velocity between liquid and particles and hydrodynamic energy dissipation rate in the riser were examined. The particle holdup increased with increasing $d_P$ or $G_S$ but decreased with increasing $U_L$. The overall particle rising velocity increased with increasing $U_L$ or $G_S$ but decreased with increasing $d_P$. The slip velocity increased with increasing $U_L$ or $d_P$ but did not change considerably with $G_S$. The energy dissipation rate, which was found to be closely related to the contacting frequency of micro eddies, increased with increasing $d_P$, $G_S$ or $U_L$. The solid particle holdup was well correlated with operating variables such as $U_L$, $d_P$ and $G_S$.

Behavior of an Impinging Droplet on a Solid Surface with a Variation of Liquid Temperature (액체 온도 변화에 따른 평판 충돌 액적의 거동에 관한 연구)

  • Lee Dong Jo;Park Byung Sung;Chung Jin Taek;Kim Ho Young
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.29 no.3 s.234
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    • pp.330-339
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    • 2005
  • An experimental study on the behavior of droplets impinging on a solid flat surface was carried out in the present study. Breakup of a liquid droplet impinging on a solid surface has been investigated experimentally for various liquids with different properties. The liquid droplet temperature and incident angle were chosen as major parameters. Liquid droplet temperature and incident angle varied in the range from $-20{\circ}C\;to\;30{\circ}C\;and\;from\;30{\circ}\;to\;60{\circ},$ respectively. It was found that the variation of droplet temperature influences upon the mean diameter and uniformity of droplets which were bounced out from the solid surface. With increase of incident angle the dispersion mass fraction increases, causing the decrease of liquid film flow rate. As the liquid temperature increases, dispersion mass fraction increases since the surface tension decreases.

The Effect of Test Peace Size on Liquid Segregation in deformation Behavior in Mushy state Material (고액공존재료의 변형거동에서 재료의 크기가 액상편석에 미치는 영향)

  • 윤성원;서판기;강충길
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1997.10a
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    • pp.167-170
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    • 1997
  • For the optimal net shape forging of semi-solid materials (SSM), it is important to predict the deformation for variation of strain rate. It should be necessruy to conduct a formation of stress-strain curve in semi-solid alloys for analysis of the thixoforming process. Particularly, important problem to application of computer aided engineering in SSM processing is to prevent a segregation of liquid component during compression process. The liquid segregation is studied as multistage change of the strain rate and test piece size to prevent the liquid segregation during the compression process. The compression test for semi-solid aluminium alloy with a controlled solid fraction is performed by dynamic material test system with a furnace. Moreover morphology of structure and fraction of pore are investigated through compression test.

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The Effect of Specimen Size on Liquid Segregation in Deformation Behavior of Mushy State Material (고액공존재료의 변형거동에서 재료의 크기가 액상편석에 미치는 영향)

  • 윤성원;서판기;강충길
    • Transactions of Materials Processing
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    • v.12 no.2
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    • pp.94-101
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    • 2003
  • For the optimal net shape forging of S semi-solid materials (SSM), it is important to predict the deformation behavior and defects of materials. Among these defects, liquid segregation is detrimental to produce products with good mechanical properties. Moreover, to apply a numerical method to thixoforging, it is very important to prevent a liquid segregation during forming process. The liquid segregation phenomena in deformation behavior of semi-solid material with variation of test specimen size were studied. The SSM compression tests were performed by dynamic material test system with a furnace. Stress-strain curves and microstructures of SSM were investigated, and Porosities were analyzed to evaluate the effects of experiment parameters on liquid segregation.