• Title/Summary/Keyword: liquid water content

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Experimental determination of liquid entry pressure (LEP) in vacuum membrane distillation for oily wastewaters

  • Racz, Gabor;Kerker, Steffen;Schmitz, Oliver;Schnabel, Benjamin;Kovacs, Zoltan;Vatai, Gyula;Ebrahimi, Mehrdad;Czermak, Peter
    • Membrane and Water Treatment
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    • v.6 no.3
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    • pp.237-249
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    • 2015
  • In this study we investigate a laboratory scale vacuum membrane distillation system to produce pure water from model oil in water emulsion. Experimental determination of liquid entry pressure (LEP) of a commercial Durapore$^{TM}$ GVPH flat sheet membrane using model emulsions in various oil concentrations has been carried out. Two different methods of liquid entry pressure determination - a frequently used, so-called static and a novel dynamic method - have been investigated. In case of static method, LEP value was found to be 2.3 bar. No significant effect of oil content on LEP was detected up to 3200 ppm. In contrast, LEP values determined with dynamic method showed strong dependence on the oil concentration of the feed and decreased from 2.0 bar to a spontaneous wetting at 0.2 bar in the range 0-250 ppm, respectively. Vacuum membrane distillation tests were also performed. The separation performance is evaluated in terms of flux behavior, total organic carbon removal and droplet size distribution of the feed and final retentate. No significant effect of oil content on the flux was found ($5.05{\pm}0.31kgm^{-2}h^{-1}$) up to 250 ppm, where a spontaneous wetting occurred. High separation performance was achieved along with the increasing oil concentration between 93.4-97.0%.

The Effects of Liquid Pig Manure Application on the Production of Japanese Millet (Echinochloa crusgalli) Soil Properties, and the Chemical Characteristics of Leaching Water (돈분 액비 시용이 피의 생산성, 토양 특성 및 용탈수의 화학적 조성에 미치는 영향)

  • Kim, Moon-Chul;Song, Sang-Taek;Hwang, Kyung-Jun;Lim, Han-Cheol
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.26 no.4
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    • pp.257-266
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    • 2006
  • Studies were carried out to evaluate the effect of liquid pig manure on the production of Japanese millet, the chemical characteristics of pasture soil and leaching water. The study was undertaken from June to September 2005. Randomized complete block design was used to allot four treatments: T1 (no fertilizer), T2 (N : 200 kg/ha, p : 150 kg/ha, K : 150 kg/ha), T3 (liquid pig manure containing 1.7% DM 200 kg N/ha) and T4 (liquid pig manure containing 7.0% DM 200 kg N/ha). Leaching water was sampled at 21 August (1st time), 9 September (2nd time) and 26 September (3rd time), 2005, respectively. No significant differences in the dry matter yield of Japanese millet was found among the four treatments, whereas the plant lengths of Japanese millet were higher in the T2, T3 and T4 than in T1 (p<0.05). Nitrogen, P and K uptake of J. millet tended to be influenced by application of chemical fertilizer or 7.0% DM liquid pig manure compared with T1 or 1.8% DM liquid pig manure. The organic matter (OM) content of soil was higher in T2, T3 and T4 than in T1. Na content was highest in T3 among the four treatments. $NO_{3^-}N\;or\;NH_{4^-}N$ content in leaching was not different among the four treatments. $SO_4$ content in leaching water sampled in 1st time was high in T4, but in T3 from 3rd time (p<0.05). Cl, Mg and Na contents were high in leaching water sampled in the 1st time from T4, whereas high in those from T3 in 2nd or 3rd time. Results show that the application of a high DM liquid pig manure is not better for producing Japanese millet and improving the properties of pasture soil than a low DM liquid pig manure. However, the contents of $SO_4$, Cl, Mg and Na in leaching water sampled in 1st time were high in a high DM liquid pig manure.

Determination of Hyperin in the Fruits of Acanthopanax Species by High Performance Liquid Chromatography

  • Lee, Jeong-Min;Kim, Hye-Min;Lee, Su-Llim;Han, Saem;Cho, Seon-Haeng;Lee, Sang-Hyun
    • Natural Product Sciences
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    • v.16 no.1
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    • pp.39-42
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    • 2010
  • The content of hyperin in Acanthopanax species was determined by high performance liquid chromatography (HPLC). Hyperin was quantified by a reverse-phase column with elution program [initially gradient solvent (acetonitrile : water = 85 : 15 to 80 : 20 for 20 min), then isocratic solvent (acetonitrile : water = 80 : 20 for 20 min), and finally gradient solvent (acetonitrile : water = 80 : 20 to 65 : 35 for 20 min)]. UV detection was conducted at 210 nm. The content of hyperin in the fruits of Acanthopanax was measured in the species A. chiisanensis (2.04 mg/g), A. sessiliflorus (1.13 mg/g), A. divaricatus (0.98 mg/g), A. koreanum (0.75 mg/g) and A. senticosus (0.05 mg/g). The content of hyperin in A. chiisanensis was higher than that of other Acanthopanax species.

Freezing Behaviors of Frozen Foods Determined by $^1H$ NMR and DSC

  • Lee, Su-Yong;Moon, Se-Hun;Shim, Jae-Yong;Kim, Yong-Ro
    • Food Science and Biotechnology
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    • v.17 no.1
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    • pp.102-105
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    • 2008
  • The freezing patterns of commercial frozen foods were characterized by using proton nuclear magnetic resonance ($^1H$ NMR) relaxometry and differential scanning calorimetry (DSC). The liquid-like components like unfrozen water were investigated as a function of temperature (10 to $-40^{\circ}C$) and then compared with the unfrozen water content measured by DSC. The formation of ice crystals and the reduction of water in the foods during freezing were readily observed as a loss of the NMR signal intensity. The proton NMR relaxation measurement showed that the decreasing pattern of the liquid-like components varied depending on the samples even though they exhibited the same onset temperature of ice formation at around $0^{\circ}C$. When compared with the unfrozen water content obtained by the DSC, the NMR and DSC results could be closely correlated at the temperature above $-20^{\circ}C$. However, the distinct divergence in the values between 2 methods was observed with further decreasing temperatures probably due to the solid glass formation which was not detected by DSC.

The Preparation and Application of Lamella Liquid Crystal to Skin Care Product (Skin care 화장료로서 단상형 액정조성물의 제조 및 응용)

  • 박병덕;이명진;이종기;이승헌
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.26 no.1
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    • pp.93-106
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    • 2000
  • One phase liquid crystal formula was developed by using of nonionic surfactants, polyols, water and oils and its physical property was investigated. At the system oft to 1 ratio of POE octyldodecyl ether series, which have Y type (branch type) hydrophobic group, and POE glyceryl monostearate series, Y type hydrophilic group, it was examined that the formula at 7:3, 6:4, and 5:5 ratio of nonionic surfactant : polyols, shows L$\alpha$ , a pattern which is a typical characteristic of liquid crystal structure under the cross microscope polarized film. As results of L$\alpha$ phase diagram study, the formula which had high hydrophilic nonionic surfactant and the 7:3 ratio of nonionic surfactant : polyol appeared to increase the amount of oil containment and to be capable of the lamella formation. Besides it was examined that lamellar liquid crystal formula could contain about 25-40% water between lamella layers and it was transformed into w/o emulsion following as water content increased. When the lamella gel was applied into a human skin, it was investigated that it had effectiveness in increasing transepidermal water content of the skin.

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Analysis of Anti-adipogenic Constituents of Cordyceps militaris Using High Performance Liquid Chromatography-Diode Array Detection in Different Samples: Comparison with Anti-adipogenic Activity

  • Liu, Qing;Hong, In-Pyo;Han, Sang-Bae;Hwang, Bang-Yeon;Lee, Mi-Kyeong
    • Natural Product Sciences
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    • v.18 no.3
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    • pp.171-176
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    • 2012
  • We previously isolated cordycepin, guanosine and tryptophan from Cordyceps militaris as antiadipogenic constituents. For the quality control of C. militaris for anti-adipogenic activity, simultaneous analytical method using high-performance liquid chromatography (HPLC)-diode array detection (DAD) was developed and validated. Quantitation of these compounds in various Cordyceps samples from different sources and various extraction methods were conducted using developed method. Our study shows that natural Cordyceps and host insect possess higher content than cultured ones and fruiting bodies, respectively. The content of cordycepin showed great difference in different C. militaris samples whereas trytophan content was similar in tested samples. Addition of water to extraction solvent greatly increased the yield of guanosine and tryptophan. High temperature and longer extraction time increased yield of guanosine, whereas the content of trytophan was decreased in high temperature during extraction with water. Extraction using ultrasonic apparatus slightly increased extraction efficiency. Cordycepin, however, has little variation in different extraction method tested. Strong anti-adipogenic activity was observed in the samples that contain all the three constituents. Taken together, quantitation of these compounds using developed analytical method might provide basic requirement for the anti-adipogenic activity of C. militaris.

Flame-resistant treatment schedule of Microwave drying wood (마이크로웨이브 건조목재의 방염처리 스케줄)

  • Park, Cheul-Woo;Her, Jae-Won;Lim, Nam-Gi
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2011.11a
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    • pp.27-28
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    • 2011
  • This research aims to secure fundamental data for the development offire-retardant wood by soaking dried wood in fire-retardant liquid. To dry wood, optimal drying conditions for softwood usually used as structural material and hardwood usually used as finishing or furniture material were derived by varying the microwave outputs and heating times of microwave wood drying equipment. The research foundthat each specimen needs 8 to 15 minutes of heating time depending on water content and output. For softwood, fire-retardant liquid equivalent to about 10 percent of the total mass of the specimen infiltrated into the dried wood, of which the water content was reduced to 5~6 percent.

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Changes in the Constituents and Antioxidant Activity in Accordance with the Processing Conditions of Citrus unshiu Markovich (진피의 수치 조건에 따른 성분 및 항산화 활성 변화)

  • Cha, Bae Cheon
    • Korean Journal of Pharmacognosy
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    • v.46 no.1
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    • pp.23-30
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    • 2015
  • Processing of medicinal plants is one of the processing methods for reducing of toxicity or improving of effect on medicinal plants. In this study, we studied the changes in the constituents and antioxidant activity in accordance with the processing conditions by the salt water of Citrus unshiu Markovich. Changes in antioxidant activity was measured by the DPPH method and changes in the components were analyzed by high performance liquid chromatography. As a result, the content of the main constituents (narirutin, hesperidin) and total polyphenol were increased by increasing the concentration of salt water. Moreover, antioxidant activity was increased gradually in proportion to the increase of the total polyphenol content.

Material Properties Evaluation of Cement Mortar Mixed with Organic/Inorganic Combined Water-repellent (유/무기 복합 발수제를 혼입한 모르타르의 재료특성 평가)

  • Kim, Wan-Su;Yoon, Chang-Bok;Cho, In-Sung;Lee, Han-Seung
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.24 no.6
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    • pp.50-58
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    • 2020
  • When the concrete surface layer is damaged, The method of impregnating the concrete surface with a water repellent cannot secure the expected durability. Recently, various waterproofing and water-repellent materials were mixed into concrete or mortar to secure water repellency even inside cracks, but compressive strength was greatly reduced. In order to overcome the decrease in compressive strength, there has not yet been a study using the merits of organic and inorganic materials at the same time, so in this study, the physical properties and water repellency performance were evaluated by mixing an organic/inorganic composite water repellent appropriately mixed with an organic and inorganic material into the mortar. When mixed with organic/inorganic water repellent, the flow and air content were reduced by about 10% and 50% compared to the Liquid specimen. In the case of the P6L1 specimen, it was confirmed that the compressive strength decreased by about 3.5% compared to the non-mixed mortar at 39.5 MPa, the same as the existing water repellent, Powder. Water-repellent performance The organic-inorganic composite water repellent mixture specimen confirmed higher water repellency than the existing water repellent mixture powder, and the chloride penetration resistance evaluation result showed that the organic-inorganic composite water repellent mixture specimen reduced the passing charge by about 45% compared to the non-mixed mortar. In summary, it is judged that the P5L1 organic/inorganic composite water repellent mixed with a powder water repellent and a liquid water repellent in a ratio of 5:1 is the most reasonable to prevent the decrease in compressive strength and secure water repellency.

Shear Behavioral Characteristics of Weathered Residual Soil for the Change Water Content (풍화잔적토의 함수비 변화에 따른 전단거동특성)

  • Yoo, Nam-Jae;Kim, Young-Gil;Lee, Jong-Ho
    • Journal of Industrial Technology
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    • v.17
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    • pp.119-124
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    • 1997
  • This thesis is an experimental research of shear behavioral characteristics and shear behavioral coefficient of weathered residual soil which is mostly contained in soil of Korea. Using the weathered residual soil from mountain near Kangwon National University, this experimental research were contained the physical properties of sample in term of the basic test method such as specific gravity, plastic and liquid limit, grain-size distribution, density and water content. Experimental results obtained from direct shear test sand triaxial compression tests show that according to step loading, linear strain and linear stress increase continually and angle of internal friction decreases just little according to incresing of water content in case of ignoring the cohesion, and angle of internal friction appears the maximum angle near a optimum moisture content in case of considering the cohesion.

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