• Title/Summary/Keyword: liquid water content

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Self Assembly and Formation of Bi-continuous Cubic Liquid Crystalline Phase (바이컨티니어스 큐빅상 액정의 생성과 자기조직화)

  • Kim, In-Young;Choi, Hwa-Sook;Lee, So-Ra;Choi, Seong-Ho
    • Journal of the Korean Applied Science and Technology
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    • v.31 no.3
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    • pp.478-485
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    • 2014
  • This study is to form the self assembly of cubic crystalline phase to penetrate into the skin epidermis. The various performance synthesized diglyceryl phytylacetate (DGPA) having hydroxyl group (-OH) and 4 methyl chains with phytyl group was carried out as an amphoteric lipid such as emulsifying power, self assembly. Emulsifying activity of DGPA was very stabilized on only 1% of small content, it could make a W/O emulsion containing high internal phase incorporated with water. Cubic liquid crystal structure with DGPA on three-phase diagram was formed, when mixed DGPA, dimethicone (2CS), and water. Through three-phase diagram forming the cubic liquid crystal area, hexagonal structure zone, and mixing water phase and hexagonal structure area, reversed micelle area were respectively certified. Its structure was proved by the SAXS (small angled x-ray scattering) analysis. As an application, formation of cubosome containing 10% of magnesium ascorbylphosphate and 5% of pyridoxine tris-hexyldecanoate was encapsulated. Occlusive effect of cubosome had above 1.7 times better than reversed micelle. From using poloxamer of dispersing agent, phase structure recovered from W/O emulsion to cubic liquid crystal phase when storage in $33^{\circ}C$ incubator. Therefore, our this study is expected to be as epidermal-dermal skin absorbers in skin care cosmetics and pharmaceuticals industries as raw materials to form a cubic crystal phase through a more in-depth research to DGPA having amphoteric lipid property.

Comparison of Ingredients and Activities of Danggwisoo-san and Jakyakgamcho-tang by Extraction Method (추출법에 따른 당귀수산과 작약감초탕의 성분과 활성의 비교)

  • Lee, Dae-Yeon;Lee, Ho-Sung;Jo, Ju-Hwi;Yi, Young-Woo;Kim, Sung-Jin;Kang, Kyungrae;Kwon, Tae-Wook;Yang, Seung Gu;Lee, In-Hee
    • Journal of Korean Medicine Rehabilitation
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    • v.30 no.4
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    • pp.31-39
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    • 2020
  • Objectives Danggwisoo-san and Jakyakgamcho-tang are frequently prescribed for traffic accident patients in Korea. The aim of this study was to examine index compound analysis, antioxidant activity and amount of starch measurement by extraction method. Methods Danggwisoo-san and Jakyakgamcho-tang were extracted with water and 70% ethanol. Antioxidant activity was measured by 2,2-Diphenyl-1-picrylhydrazyl, 2,2-azino-bis(3-ethylbenzothiazoline-6-sulfonic acid) and ferric reducing antioxidant power according to the standard protocol. The contents of the indicator components nodakenin, paeoniflorin, and glycyrrhizin were measured by high-performance liquid chromatography, respectively. All starches were hydrolyzed and then total D-glucose was measured and compared. Results Antioxidant activity was excellent in 70% ethanol in all assays. The index component was jagged because its solubility was different depending on the extraction solvent. Starch content was significantly lower in 70% alcohol extract than water extract. Conclusions The results of this study showed that physiological activities and components are different according to extraction conditions. Each herbal medicine has a suitable extraction solvent. Also, the difference in starch content is an object to be considered as it may affect digestion and absorption.

Indirect Verification of the Icing Test Condition Using Ice Thickness (얼음두께를 이용한 결빙시험조건의 간접 확인기법)

  • Kim, Yoo Kyung;Park, Nameun;Choi, Gio
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.46 no.11
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    • pp.944-951
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    • 2018
  • Artificial icing test and wind tunnel test can be performed to reduce the development period when a rotorcraft is required operation under icing situations. Artificial icing test of the KUH(Korean Utility Helicopter) was performed in advance to verify anti-icing and de-icing performance before natural icing test. Although high-precision sensor, the CCP(Cloud Combination Probe) is used to measure icing test condition parameters such as LWC(Liquid Water Content) and MVD(Median Volume Diameter), the measured values need to be verified in various methods due to the possibility of uncertainties which are the test atmosphere environment, sensor errors, and etc. The calculated LWC from the ice thickness cumulated on the fuselage of the KUH is compared to the measured value by CCP, and the results show the effective indirect method to check the test conditions.

Meteorological Conditions for the Cloud Seeding Experiment by Aircraft in Korea (인공강우 항공실험을 위한 한반도 기상조건의 예비결과)

  • Jung, Woonseon;Chang, Ki-Ho;Ko, A-Reum;Ku, Jung Mo;Ro, Yonghun;Chae, Sanghee;Cha, Joo Wan;Lee, Chulkyu
    • Journal of Environmental Science International
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    • v.30 no.12
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    • pp.1027-1039
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    • 2021
  • In this study, we investigated the optimal meteorological conditions for cloud seeding using aircraft over the Korean Peninsula. The weather conditions were analyzed using various data sources such as a weather chart, upper air observation, aircraft observation, and a numerical model for cloud seeding experiments conducted from 2018 to 2019 by the National Institute of Meteorological Sciences, Korea Meteorological Administration. Cloud seeding experiments were performed in the seasons of autumn (37.0%) and winter (40.7%) in the West Sea and Gangwon-do. Silver iodide (70.4%) and calcium chloride (29.6%) were used as cloud seeding materials for the experiments. The cloud seeding experiments used silver iodide in cold clouds. Aircraft observation revealed relatively low temperatures, low liquid water content, and strong wind speeds in clouds with a weak updraft. In warm clouds, the cloud seeding experiments used calcium chloride. Observations included relatively high temperatures, high liquid water content, and weak wind speeds in clouds with a weak updraft. Based upon these results, we determined the comprehensive meteorological conditions for cloud seeding experiments using aircraft over the Korean Peninsula. The understanding of optimal weather conditions for cloud seeding gained from this study provide information critical for performing successful cloud seeding and rain enhancement.

Optimization of Extraction Conditions for Total Phenolics from Sapium japonicum Using a Pressurized Liquid Extractor

  • Kim, Mi-Bo;Park, Jae-Sung;Lim, Sang-Bin
    • Food Science and Biotechnology
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    • v.18 no.4
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    • pp.996-1000
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    • 2009
  • Sapium japonicum was extracted by a pressurized liquid. Operating parameters such as the type and the ratio of solvent to water, temperature, pressure, and number of extractions were investigated as the main variables that influence the extraction efficiencies of total phenolics (TP). MeOH extracted the highest level of TP as 50.4 mg GAE/g compared to 48.8 and 27.2 mg GAE/g with $H_2O$ and EtOH, respectively. $EtOH:H_2O$ (40:60, v/v) was found to be the best solvent for TP extraction as 90.3 mg GAE/g compared to 85.0 and 84.3 mg GAE/g in 40:60 and 60:40 of $MeOH:H_2O$, respectively. TP were increased with the increase of the number of extraction steps. TP content was increased by 11% as the extraction temperature was increased from 40 (97.4) to $50{\circ}C$ (108.3 mg GAE/g). The optimum extraction conditions of TP were; extraction solvent, $EtOH:H_2O$ (40:60, v/v); temperature, $50{\circ}C$; pressure, 10.2 MPa; 2 extraction steps.

Determination of 11 Ginsenosides in Black Ginseng Developed from Panax ginseng by High Performance Liquid Chromatography

  • Sun, Bai-Shen;Gu, Li-Juan;Fang, Zhe-Ming;Wang, Chun-Yan;Wang, Zhen;Sung, Chang-Keun
    • Food Science and Biotechnology
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    • v.18 no.2
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    • pp.561-564
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    • 2009
  • A high performance liquid chromatography (HPLC) method has been developed for determination of 11 ginsenosides in black ginseng (BG, white ginseng that is subjected to 9 cycles of $95^{\circ}C$ for 3 hr). After eluted by gradient elution of water-acetonitrile without buffer in 70 min, 11 ginsenosides in BG were identified. The proposed method provided good linearity ($R^2$>0.9995), accuracy (92.2-106.6%), and intra- and interday precision (RSD<2.6%). In addition, ginsenosides compositions in white, red, and black ginsengs were investigated using this method, respectively. Interestingly, in BG, the content of ginsenoside $Rg_3$ which does not existed in white ginseng was 7.51 mg/g, approximately 20 times than that in red ginseng.

Pre-cooking and liquid smoke affect the physicochemical and microbiological quality and polyhydroxy aromatic hydrocarbon (PAH) content in smoked skipjack tuna (Katsuwonus pelamis L.)

  • Silvana Dinaintang Harikedua;Ella Dertina Saragih;Eunike Louisje Mongi;Lena Jeane Damongilala;Netty Salindeho;Henny Adeleida Dien;Nurmeilita Taher;Helen Jenny Lohoo;Mayse Sofien Siby
    • Food Science and Preservation
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    • v.31 no.2
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    • pp.210-217
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    • 2024
  • This study aimed to compare the quality of smoked fish products processed with liquid smoke with and without pre-cooking when stored at room temperature (25℃) for 0, 2, 4, and 6 days. The observations included moisture content, water holding capacity, color, and total plate and mold counts. The treated samples were also analyzed for polyhydroxyaromatic hydrocarbons (PAHs) at day 0. The study found that the pre-cooked products had a lower moisture content (55.1%) than the control (59.9%) during storage. Additionally, the pre-cooked product had a higher water holding capacity than the control. The TPC value indicates that the pre-cooked product meets the Indonesian standard for smoked fish up to the 2nd day of storage, whereas the control product only meets the standard on day 0. However, the total mold of the control products meets the Indonesian standard until the 2nd day of storage, while the pre-cooked products only meet the standard on day 0. The pre-cooked product had a higher lightness value (L*) than the control. The analysis of polyhydroxy aromatic hydrocarbon (PAH) showed that the pre-cooking process did not affect the concentration of PAH.

Effect of acid whey and freeze-dried cranberries on lipid oxidation and fatty acid composition of nitrite-/nitrate-free fermented sausage made from deer meat

  • Karwowska, Malgorzata;Dolatowski, Zbigniew J.
    • Asian-Australasian Journal of Animal Sciences
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    • v.30 no.1
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    • pp.85-93
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    • 2017
  • Objective: This study evaluated the effect of acid whey and freeze-dried cranberries on the physicochemical characteristics, lipid oxidation and fatty acid composition of nitrite-free fermented sausage made from deer meat and pork fat. Antioxidant interactions between acid whey and cranberry compounds were also explored. Methods: Four formulations of fermented venison sausage were prepared: F1 (control), F2 (with 5% liquid acid whey), F3 (with 0.06% of freeze-dried cranberries), and F4 (with 5% liquid acid whey and 0.06% of freeze-dried cranberries). Each sample was analyzed for pH, water activity ($a_w$), heme iron content, 2-thiobarbituric acid reactive substances (TBARS) value and conjugated dienes at the end of the manufacturing process and at 30 and 90 days of refrigerated storage. Fatty acid composition was measured once at the end of the manufacturing process. Results: At the end of ripening, all samples presented statistically different values for a pH range of 4.47 to pH 4.59. The sum of the unsaturated fatty acids was higher, while the conjugated diene and the TBARS values were lower in sausages with freeze-dried cranberries as compared to the control sausage. The highest content of heme iron (21.52 mg/kg) at day 90 was found in the sausage formulation with the addition of freeze-dried cranberries, which suggests that the addition of cranberries stabilized the porphyrin ring of the heme molecule during storage and thereby reduced the release of iron. The use of liquid acid whey in combination with cranberries appears to not be justified in view of the oxidative stability of the obtained products. Conclusion: The results suggest that the application of freeze-dried cranberries can lower the intensity of oxidative changes during the storage of nitrite-free fermented sausage made

Aerobic Liquid Fermentation of Food Wastes by Using Yeast (효모에 의한 남은 음식물의 호기성 액상발효)

  • Lee, Ki-Young;Yu, Sung Jin;Yu, Seung Yeung
    • Journal of the Korea Organic Resources Recycling Association
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    • v.8 no.4
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    • pp.147-152
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    • 2000
  • For the probiotic feed production from residual food waste by using the yeast Kluyveromyces marxianus, aerobic liquid fermentation was attempted at $35^{\circ}C$. After grinding finely, optimal fermentation conditions of the substrate was investigated in shaking incubator. By controlling water content yeast growth was studied at each different solid content of 5, 10 and 15% respectively. The most active growth of the yeast was shown at 10%. For the stimulation of the cell growth, mixed culture with Aspersillus oryzae was conducted in a 2 litre-jar fermenter. As the results, the yeast growth rate was increased, but the maximum viable cell count amounted was slightly higher as $3.5{\times}10^9/ml$ than single culture.

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Comparison of Anthocyanin Content in Seed Coats of Black Soybean [Glycine max(L.) Merr.] Cultivars Using Liquid Chromatography Coupled to Tandem Mass Spectrometry

  • Shin, Sung-Chul;Lee, Soo-Jung;Lee, Sung-Joong;Chung, Jong-Il;Bae, Dong-Won;Kim, Soo-Taek;Sung, Nak-Ju
    • Food Science and Biotechnology
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    • v.18 no.6
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    • pp.1470-1475
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    • 2009
  • The seed coat of the black soybean contains 3 main anthocyanins such as delphinidin-3-O-$\beta$-glucoside, cyanidin-3-O-$\beta$-glucoside, and petunidin-3-O-$\beta$-glucoside. As a part of our effort on discovering and breeding new black soybean cultivars which possesses specific anthocyanin component rich, we determined the anthocyanin profiles of the 2 cultivars recently developed soybean cv. Gaechuck #1 and cv. Gyeongsang #1, using liquid chromatography-tandem mass spectrometry (LC-MS/MS) and compared their content and identity with those of previously known 10 cultivar controls. The Cosmosil-$5C_{18}$-AR-II column were selected for the analysis because of the best peak separation. The column temperature was set up at $35^{\circ}C$. The mobile phase consisting of water containing 0.5%(v/v) formic acid and methanol gave good separation between the 3 anthocyanin analytes and internal standard (quercetin 3-O-$\beta$-rutinoside) and peaks with suppressed tail. The MS/MS spectra of each individual anthocyanin standard were detected in positive electron spray ionization (ESI) modes. It was disclosed that the anthocyanin contents of the soybean cv. Gaechuck#1 and cv. Gyeongsang#1 are roughly higher than those of the 10 controls.