• YAKHAK HOEJI
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• v.52 no.6
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• pp.446-451
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• 2008

A high-performance liquid chromatography (HPLC) with diode array detector (DAD) and electrospray ionization mass spectrometry (ESI-MS) was established for the simultaneous determination of chlorogenic acid (1), sweroside (2), luteolin-7-O-glucoside (3), (E)-aldosecologanin (4) and 3,5-dicaffeoylquinic acid (5) from Lonicera joponica flower buds. The optimal chromatographic conditions were obtained on an ODS column (5 ${\mu}m$, 4.6${\times}$150 mm) with the column temperature $25^{\circ}C$. The mobile phase was composed of (A) water with 0.1% formic acid and (B) acetonitrile with 0.1% formic acid using a gradient elution, the flow rate was 0.3 ml/min. Detection wavelength was set at 250 nm. All calibration curves showed good linear regression ($r^2$>0.994) within test ranges. The developed method provided satisfactory precision and accuracy with overall intra-day and inter-day variations of 0.05${\sim}$1.95% and 0.15${\sim}$2.26%, respectively, and the overall recoveries of 97.71${\sim}$103.65% for the five compounds analyzed. The verified method was successfully applied to quantitative determination of the three types (phenolic compounds, iridoids and flavonoids) of bioactive compounds in 21 commercial L. japonica flower buds samples from different markets in Korea and China. The analytical results demonstrated that the contents of the five analytes vary significantly with sources.

• Aerospace Engineering and Technology
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• v.1 no.1
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• pp.163-172
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• 2002

The turbine system composed of a nozzle and a rotor is used to drive turbopumps while gas passes through the nozzle, potential energy is converted to kinematic energy, which forces the rotor blades to spin. In this study, an aerodynamic design of a turbine system is investigated using compressible fluid dynamic theories with some pre-determined design requirements (i.e.,pressure ratio, rotational speed, required power etc.) obtained from a liquid rocket engine (L.R.E.) system design. For simplicity of a turbine system, impulse-type rotor blades for open type L.R.E. have been chosen. Usually, the open-type turbine system requires low mass flow rate compared to the close-type system. In this study, a partial admission nozzle is adopted to maximize the efficiency of the close-type turbine system. A design methodology of the a turbine system has been introduced. Especially, a partial admission nozzle has been designed by means of simple empirical correlations between efficiency and configuration of the nozzle. Finally, a turbine system design for a 10 ton thrust level of L.R.E is presented.

• Journal of the Korean Society of Propulsion Engineers
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• v.24 no.1
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• pp.64-77
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• 2020

An electric-pump cycle, which is a propellant supply system for driving pumps of a liquid rocket engine using an electric motor, has the advantages of simple system configuration and easy control of supply flow rate and pressure. This paper investigates and analyzes the overseas research trends of the electric-pump cycle. In addition, the research and development country, performing organization, application, engine thrust, pump pressure increase, motor power, and rotation speed are summarized. Among them, the design variables of the overseas research that applied the upper-stage propulsion system with the thrust range of 0.445~2.2 kN could be used in the study of a similar electric-pump cycle in Korea.

• Nuclear Engineering and Technology
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• v.45 no.2
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• pp.203-210
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• 2013

The objective of this conducted research is to study the iodine removal efficiency in a self-priming venturi scrubber for submerged and non-submerged operating conditions experimentally and theoretically. The alkaline solution is used as an absorbent, which is prepared by dissolving sodium hydroxide (NaOH) and sodium thiosulphate ($Na2S_2O_3$) in water to remove the gaseous iodine ($I_2$) from the gas. Iodine removal efficiency is examined at various gas flow rates and inlet concentrations of iodine for submerged and non-submerged operating conditions. In the non-submerged venturi scrubber, only the droplets take part in iodine removal efficiency. However, in a submerged venturi scrubber condition, the iodine gas is absorbed from gas to droplets inside the venturi scrubber and from bubbles to surrounding liquid at the outlet of a venturi scrubber. Experimentally, it is observed that the iodine removal efficiency is greater in the submerged venturi scrubber as compare to a non-submerged venturi scrubber condition. The highest iodine removal efficiency of $0.99{\pm}0.001$ has been achieved in a submerged self-priming venturi scrubber condition. A mathematical correlation is used to predict the theoretical iodine removal efficiency in submerged and non-submerged conditions, and it is compared against the experimental results. The Wilkinson et al. correlation is used to predict the bubble diameter theoretically whereas the Nukiyama and Tanasawa correlation is used for droplet diameter. The mass transfer coefficient for the gas phase is calculated from the Steinberger and Treybal correlation. The calculated results for a submerged venturi scrubber agree well with experimental results but underpredicts in the case of the non-submerged venturi scrubber.

• International Journal of Naval Architecture and Ocean Engineering
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• v.10 no.1
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• pp.1-8
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• 2018

As the key equipment in deep ocean mining, the slurry pump suffers from wear and blocking problems. In this paper, high-speed photography technique is applied to track the movement rule of single particle of the coarse particle solid-liquid two-phase flow in a double blade slurry pump. The influences of particle diameter and particle density on the pass-through and collision characteristics of particles are analyzed as well. The results show that the average of the passing pump time first decreases and then increases when the particle diameter increases. The average of the passing pump time decreases by 22.7%, when the particle density increases from $1.09g/cm^3$ to $1.75g/cm^3$. Besides, the particle density has great influence on the location where the particle hits the tongue. Most particles of $1.09g/cm^3$ hit the tongue on the left side, while collision location of particles of $1.75g/cm^3$ is mainly on the top and at the right side of the tongue. The research can provide a basis for the optimization design of slurry pump in deep ocean mining system.

• Journal of Mechanical Science and Technology
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• v.20 no.10
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• pp.1765-1772
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• 2006

High-pressure die casting such as thixocasting and rheocasting is an effective process in the manufacturing automotive parts. Following the recent trend in the automotive manufacturing technologies, the product design subject to the die casting becomes more and more complex. Simultaneously the injection speed is also designed to be very high to establish a short cycletime. Thus, the requirement of the die design becomes more demanding than ever before. In some cases the product's shape can have multiple slender manifolds. In such cases, design of the inlet and outlet parts of the die is very important in the whole manufacturing process. The main issues required for the qualified products are to attain gentle and uniform flow of the molten liquid within the passages of the die. To satisfy such issues, the inlet cylinder ('bed cylinder' in this paper) must be as large as possible and simultaneously the outlet opening at the end of each passage must be as small as possible. However these in turn obviously bring additional manufacturing costs caused by re-melting of the bed cylinder and increased power due to the small outlet-openings. The purpose of this paper is to develop effective simulation methods of calculation for fluid flows in multiple columns, which mimic the actual complex design, and to get some useful information which can give some contributions to the die-casting industry. We have used a commercial code CFX in the numerical simulation. The primary parameter involved is the size of the bed cylinder. We will show how the very small opening of the outlet can be treated with the aid of the porous model provided in the code. To check the validity of the numerical results we have also conducted a simple experiment by using water.

• Korean Journal of Oriental Medicine
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• v.16 no.1
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• pp.173-178
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• 2010

The purpose of this study was investigation of quantitative analysis of marker substances in solid fermented Angelicae Gigantis Radix by High performance liquid chromatography(HPLC). HPLC was performed for determination of nodakenin and decursin in solid fermented Angelicae Gigantis Radix extract, the separation method was performed on C18 column ($250\;mm\;{\times}\;4.6\;mm$, $5\;{\mu}m$, RS tech) using gradient solvent mixtures of water-acetonitrile with photodiode array detector (330 nm). The flow rate was 1.0 ml/min. Retention time of nodakenin and decursin was about 11.47, 46.79 min and linearity of calibration was showed good result(r2=0.9999, 0.9999), respectively. Content of nodakenin was $0.76\;{\pm}\;0.02%$ in control, $0.31\;{\pm}\;0.00%$ in Angelicae Gigantis Radix extract fermented with Paecilomyces japonica(SDT)(p<0.01), $0.51\;{\pm}\;0.02%$ in Angelicae Gigantis Radix extract fermented with Ganoderma lucidum(SYT)(p<0.01), $0.82\;{\pm}\;0.03%$ in Angelicae Gigantis Radix extract fermented with honey(SST)(p<0.05) and $0.88\;{\pm}\;0.01%$ in Angelicae Gigantis Radix extract fermented with Nuruk(SNT)(p<0.01). Content of decursin was $4.50\;{\pm}\;0.08%$ in control, $2.90\;{\pm}\;0.05%$ in Angelicae Gigantis Radix extract fermented with Paecilomyces japonica(SDT)(p<0.01), $2.65\;{\pm}\;0.08%$ in Angelicae Gigantis Radix extract fermented with Ganoderma lucidum(SYT)(p<0.01), $4.46\;{\pm}\;0.11%$ in Angelicae Gigantis Radix extract fermented with honey(SST) and $4.73\;{\pm}\;0.04%$ in Angelicae Gigantis Radix extract fermented with Nuruk(SNT)(p<0.05), respectively.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.37 no.11
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• pp.1096-1103
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• 2009

The predictions of the material behavior for the structural stability of thrust chamber mixing head at very-low temperatures are very important since the head is highly pressurized by the liquid oxygen with very-low temperatures and experiences impact load by the thrust of combustion chamber. The constitutive equation to express tensile deformation behavior of the material at very-low temperature to predict deformation behavior of the mixing head is formulated by composition of thermal component and athermal component based on dislocation energy barrier model suggested by Kocks. Also, increase of thermal stress components by the increase of obstacles at low temperatures is formulated to the equation similar with Ramberg-Osgood equation. The suggested model predicted well the material's behavior at the wide temperature ranges from very-low temperature to ambient temperature.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.14 no.3
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• pp.1040-1044
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• 2013

The present paper has been accomplished to elucidate the characteristics of temperature change in a car washer heater system for removal of frost formed at the surface of a car. The previous studies had used a simplified mathematical modeling to analyse the temperature change characteristics for a car washer heater system. In the present study, an unsteady computational fluid flow and heat transfer analysis for a washer heater system has been done by using computational fluid dynamic analysis method. From the present CFD analysis, the time dependent temperature change in a car washer heater system has been analysed and derived the heating time and ejection temperature of the washer liquid to establish the optimal design basis for a washer heater system.

• Resources Recycling
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• v.19 no.6
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• pp.77-85
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• 2010

This study was carried out to develop a process flow sheet for recovering valuables (gold and high purity silica) from the gold mine tailings containing 1.7 g/ton of gold and 79.48 wt.% $SiO_2$. Float-sink tests using heavy liquids was conducted to explore the possibility of recovering gold by gravity separation. Hydrocyclone, froth flotation, and triboelectrostatic separatoin tests were conducted to recover high purity silica from the gold mine tailings. The results of float-sink tests showed that particles containing 5.58 g/ton of gold could be obtained at 2.72 specific gravity, but with very low yields around 3%. Meanwhile, all tests with hydrocyclone, froth flotation, and triboelectrostatic separation showed that high purity silica with $SiO_2$ content over 90% could be obtained. The purity could be improved further up to about 94% by employing several recleaning steps in the froth flotation and triboelectrostatic process.