• Title/Summary/Keyword: lime material

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Identification of Greyish White Material Adhered to Shrouds from Tombs Covered with Lime of the Chosun Dynasty (조선시대 회곽 묘 출토 염습의에 부착된 회백색 물질의 동정)

  • OH, Joon-Suk;Yu, Hei-Sun;Yun, Eun-Young
    • Journal of Conservation Science
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    • v.16 s.16
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    • pp.21-26
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    • 2004
  • A lot of waterlogged shrouds and mummies have been found in tombs revered with lime of the Chosun Dynasty(1392-1910) of Korea. Shrouds were heavily polluted with greyish white material. Greyish white material, which adhered to shrouds excavated from tombs(16C and 17C), was submitted to FT-IR qualitative analysis and fatty acid analysis for cleaning. The results of the FT-IR qualitative analysis identified the main ingredient of the greyish white material as calcium salt of fatty acid, including a little of the fatty acids, lipids and proteins. Therefore the greyish white material fumed out adipocere which was formed from the degradation of the lipids in a dead body. From the fatty acid analysis, hydroxy fatty acids(10-Hydroxyhexadecanoic acid and 10-Hydroxyoctadecanoic acid), which were found in adipocere, were detected. The distribution of contents of fatty acids was also rimilar to that of adipocere which have a high proportion of palmitic acid of saturated fatty acid and a low proportion of oleic arid of unsaturated fatty acid. In view of the results of analyses, it was revealed that greyish white material adhered to shrouds was adipocere moved from a mummy.

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Study on the Reduction of Molten EAF Slag (용융 전기로 슬래그의 환원반응에 관한 연구)

  • Joo, Seong-Woong;Shin, Jong-Dae;Shin, Dong-Kyung;Hong, Seong-Hun;Ki, Jun-Sung;Hwang, Jin-Il;You, Byung-Don
    • Korean Journal of Metals and Materials
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    • v.50 no.10
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    • pp.753-761
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    • 2012
  • The reduction behavior of low level oxides such as (T.Fe), (MnO) and ($P_2O_5$) in molten EAF slag was investigated using commercial reductants. In an air atmosphere, the slag volume increased and the reduction rate of the slag was very low due to the oxidation loss of reductants by oxygen in the air. The reduction rate of the slag was also low when a commercial reductant was used alone in an Ar gas atmosphere. The reason is probably because the material transfer through the interface between the slag and reductant is difficult due to the formation of high melting point oxide. When reductants were mixed with burnt lime in order to form low melting point reaction products, the reduction rate of the slag increased up to the range of 45-70%. By using the mixtures of reductants and burnt lime so as to form a low melting point slag at the reaction end, the reduction rate of the slag was improved up to 60-85%.

Effects of Dolomite and Oyster Shell on Nitrogen Processes in an Acidic Mine Soil Applied with Livestock Manure Compost

  • Yun, Seok-In;Seo, Dong-Hyuk;Kang, Ho Sang;Cheng, Hyocheng;Lee, Gunteak;Choi, Woo-Jung;Lee, Chang-Kyu;Jung, Mun Ho
    • Korean Journal of Soil Science and Fertilizer
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    • v.49 no.5
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    • pp.614-620
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    • 2016
  • Mine soils are usually unfavorable for plant growth due to their acidic condition and low contents of organic matter and nutrients. To investigate the effect of organic material and lime on nitrogen processes in an acidic metal mine soil, we conducted an incubation experiment with treating livestock manure compost, dolomite, and oyster shell and measured soil pH, dehydrogenase activity, and concentration of soil inorganic N ($NH_4{^+}$ and $NO_3{^-}$). Compost increased not only soil inorganic N concentration, but also soil pH from 4.4 to 4.8 and dehydrogenase activity from 2.4 to $3.9{\mu}g\;TPF\;g^{-1}day^{-1}$. Applying lime with compost significantly (P<0.05) increased soil pH (5.9-6.4) and dehydrogenase activity ($4.3-7.0{\mu}g\;TPF\;g^{-1}day^{-1}$) compared with applying only compost. Here, the variation in dehydrogenase activity was significantly (P<0.05) correlated with that in soil pH. Soil inorganic N decreased with time by 14 days after treatment (DAT) due to N immobilization, but increased with time after 14 DAT. At 28 DAT, soil inorganic N was significantly (P<0.05) higher in the lime treatments than the only compost treatment. Especially the enhanced dehydrogenase activity in the lime treatments would increase soil inorganic N due to the favored mineralization of organic matter. Although compost and lime increased soil microbial biomass and enzyme activity, ammonia oxidation still proceeded slowly. We concluded that compost and lime in acidic mine soils could increase soil microbial activity and inorganic N concentration, but considerable ammonium could remain for a relatively long time.

Mortar Characteristics for Reinforcement of Ancient Tomb Murals Using Oyster Shells

  • Lee, Hwa Soo;Yu, Yeong Gyeong;Han, Kyeong Soon
    • Journal of Conservation Science
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    • v.34 no.4
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    • pp.295-303
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    • 2018
  • The application of reinforcing agents with hydraulic property and strength development characteristics was studied under conditions similar to those of mural-painting mortar made with oyster shell powder. Reinforcement mortar made with oyster shell powder showed hydraulic properties and strength to supplement the weaknesses of natural hydraulic lime(NHL); this confirmed its possibility as a wall-reinforcing material with enough strength for preserving mural paintings. Reinforcement mortar 1 showed hydraulic property and general characteristics of lime mortar, such as consistency and viscosity, as well as lower strength and higher whiteness compared to an NHL product. For Reinforcement mortar 2, the original wall sample characteristics were reflected by mixing more shell produced through calcination; and it showed similar strength to that of Reinforcement mortar 1 as well as high whiteness. In measuring the contraction ratio of reinforcement mortar samples, Reinforcement mortar 1 and 2 showed more stability in property change compared to the NHL Group.

Studies on Establishment of Over sown Pasture Seed II. Effect of coating materials on germination and yield of pasture species (겉뿌린 목초종자의 정착에 관한 연구 II. 각종 증량재 피복이 파종목초의 발아 , 정착 및 수량에 미치는 영향)

  • 이효원;김훈기;김창호
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.10 no.1
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    • pp.10-14
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    • 1990
  • The effects of coating materials on germination, establishment and herbage production were investigated in a laboratory and field over 1988-1989. For this purpose, four treatments of lime 50 % + briquet ash 50 %, briquet ash, dairy excreta and fowldung as coating material were applied to orchardgrass and red clover with meth ylcellulose. The germination rate of lime 50 % + briquet ash 50 % (70.6 %), briquet ash (84.0 %), dairy excreta (66.0 %) and fowldung (61.3 %) in orchardgrass were, showing lower than that of the control (86.6 %), respectively and the rate of red clover ranged from 59.0 to 18.6 %. Establishment in orchardgrass were from 2.0 to 0.9 %, showing lower than the control, whole a little higher except dairy excreta and fowldung treatments in red clover than the control. The DM yield of lime 50 % + briquet ash 50 % treatment was almost same to the control and other treatment showed lower yield compared with the yield of the control. The benefical effect of seed coating on field performance was minimal especially in terms of establishment and yield increase.

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A Comparison in Characteristics of Chemical Composition of Glass Vessels Excavated from Neungsalli Temple in Buyeo, Korea, from Baekje Period

  • Koh, Min Jeong;Kang, Hyung Tae;Kim, Na Young;Kim, Gyu Ho
    • Bulletin of the Korean Chemical Society
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    • v.33 no.12
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    • pp.4173-4179
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    • 2012
  • From Neungsalli Temple located in Buyeo, ancient glass vessel fragments were discovered along with hundreds of glass beads. In this research, we used SEM-EDS to analyze glass vessel fragments and beads excavated from Neungsalli Temple. Then, we analyzed their chemical composition and examined their characteristics. In particular, we investigated a relationship between glass vessels from Neungsalli temple and Hwangnamdaechong (South tomb). The result of our experiment showed that the glass artifacts from Neungsalli temple were all soda glass. To be specific, the vessel fragments were soda-lime glass and spherical beads were high-alumina soda glass. Then, we compared glass vessel fragments from Neungsalli temple to glass vessels excavated from Hwangnamdaechong. Glass vessels from both sites turned out to be soda lime glass. We classified them further based on raw material used for soda - natron and marine plant ash.

Hydration-Setting Property of Slaked Lime and Artificial Zeolite Synthesized with Top Water Sludge (정수슬러지로 합성한 인공제올라이트와 소석회의 수화응결특성)

  • La, Jung-Min;Choi, Duk-Jin;Kim, Min-Gil;Kim, Jin-Man
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.5 no.4
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    • pp.122-128
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    • 2010
  • On the international provision on prohibition of ocean dumping of waste, tap water sludge has been buried or recycled on th low value added product as landfill. Due to the tap water sludge having high inorganic content, differing from the sewage sludge, it is possible to use as a usable resource by suitable process. We have studied on hydro thermal processing of tap water sludge with phosphoric acid and finally synthesize a artificial zeolite having a deodorization property. To use it as a building material, it has to be solidification. This study is on the properties of artificial zeolite synthsized and solidification properties by various types of solidifier. It is showed that the slaked lime is the best on setting property and its optimum content is 30-60 weight proportion. Solid by solidified by slaked lime has low strength and excellent deodorization performance, so it is possible to use as a functional pannel as gypsum board.

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Synthesis and Characterization of V2O - Doped Karrooite Brown Pigments (V2O5가 고용된 Karrooite계의 Brown색 안료합성과 특성)

  • Kim, Gum-Sun;Lee, Byung-Ha
    • Journal of the Korean Ceramic Society
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    • v.48 no.4
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    • pp.303-306
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    • 2011
  • [ $V_2O_5$ ]doped Karrooite pigments were synthesized by the solid state method to get stabilized brown pigment in oxidation and reduction atmosphere. Optimum substitution condition and limited dopant with $V_2O_5$ for Karrooite pigment was investigated. With calcination at $1250^{\circ}C{\sim}1400^{\circ}C$, compositions were designed varying $V_2O_5$ molar ratio by increasing 0.02mole to the formula $Mg_1-xTi_2-xM_{2x}O_5$(x = 0.01~0.09 mole). Synthesized pigments were analyzed by XRD, Raman spectroscopy and UV-vis. When $V_2O_5$ was doped from 0.01 to 0.05 mole, single phase of Karrooite was observed at temperature $1300^{\circ}C$ and soaking time 4h by Raman spectroscopy. However, it was found that excess $VO_2$ peak appeared with 0.07 and 0.09 mole of $V_2O_5$ doped to $MgTi_2O_5$. This result indicated that the maximum limit of solid solution is 0.05 mole $V_2O_5$. Karrooite pigments were applied as a ceramic pigment to achieve brown colors in lime magnesia glaze and lime barium graze at both of oxidation and reduction atmosphere. CIE color coordinates are $L^*$ = 40.34, $a^*$ = 9.94, $b^*$ = 21.40 in lime magnesia glaze.

A Study on the Existence of Lime Plaster Wall in the Joseon Dynasty, Based on the Analysis of Construction Reports of 'Sanleong-Uigwe' & 'Yeonggeon-Uigwe' - Emphasized on the Government Building Constructions - (산릉.영건의궤 분석을 통한 조선시대 건축에서 회벽의 존재 여부 고찰 -조선 후기 관영건축을 중심으로-)

  • Lee, Kweon-Yeong
    • Journal of architectural history
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    • v.19 no.3
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    • pp.89-106
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    • 2010
  • Since the 1970's, UNESCO and ICOMOS have adopted or emphasized on the principles of historic preservation. One of them is what to require a repair should not be repaired beyond the limits of the features and techniques which had been adopted in those days of establishment. On the premise, this paper is to examine the materials and technique of wall plaster work in the government building constructions in the Joseon dynasty. The result of this examination shall come up with a basic conformity in the case of repairing the building established in the late of Joseon dynasty. This paper is carried out for the proper repair and restoration of architectural cultural properties. Construction reports and other documents in those days are examined for the study. Following conclusions have been reached through the study. The materials and technique which applied to wall plaster work in those days were quite different from the present. The technique that was used to wall plaster of government buildings in those days was not a lime wall plaster, but sand coat one. The kinds of material for setting of the sand coat wall plaster had been revised with the change of the times or constructions. The main kinds of material were composed of sand, white clay, paper fiber, and cereal starch. However, the present materials were composed of sand, white clay. Therefore, the present materials and technique which applied to wall plaster work for the repair and restoration of architectural cultural properties have to be revised and corrected.

Seed Coating Material and Seed Size Effects on Agronomic Characteristics of Over Sown Pasture Species (피복재료 및 종자의 크기가 겉뿌림 목초의 생육특성에 미치는 영향)

  • 김종관;권찬호;김동암
    • Journal of The Korean Society of Grassland and Forage Science
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    • v.20 no.1
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    • pp.67-76
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    • 2000
  • An experiment was conducted to evaluate the effects of lime, zeolite, and rock phosphate as coating materials and coated seed size on germination, establishment, and early growth of pasture species at the experimental livestock farm, Yonam College of Agriculture in 1997. Germinating energy and germination of coated tall fescue and orchardgrass seeds were lower than those of non-coated seeds. Coated seed of tall fescue with 70% lime and 15% rock phosphate was the best in germination. The germination of small size seed (< ${\varnothing}2$ mm) was better than those of medium (> ${\varnothing}2$ mm and < ${\varnothing}2$ mm) and large size seeds (> ${\varnothing}2$ mm). Germination of coated orchardgrass seed with 55% lime and 30% rock phosphate treatment was higher than that of other coated seeds, and germination of small size seed was higher than those of medium and large size seeds (p<0.05). Germination energy and germination of coated alfalfa and birdsfoot trefoil seeds were lower than those of non-coated seeds. Germination of coated alfalfa seed with 70% lime and 15% rock phosphate, and 45% lime and 55% rock phosphate was higher compared with other coated seeds. Germination of medium size seed was higher than those of small and large size seeds (p<0.05). Among coated birdsfoot trefoil seed, 45% lime and 40% rock phosphate treatment resulted in higher germinating energy and germination than other treatments. There was no significant difference in establishment and early growth of coated tall fescue and orchardgrass seeds. However, tall fescue and orchardgrass coated with 45 % lime and 40% phosphate rock showed higher establishment and early growth. There was also no significant difference in establishment and early growth of coated alfalfa among the treatments. Among coated treatments, establishment and early growth of alfalfa coated with 75% lime and 10% rock phosphate were the highest and showed 46.4% and $72.6\;g/\textrm{m}^2$, respectively. Establishment and early growth of coated birdsfoot trefoil with 55% lime and 30% rock phosphate were the highest among coated birdsfoot trefoil seed (p<0.05) and recorded 46.4% and $44.6\;g/\textrm{m}^2$, respectively. Results of this study indicate that the germination of coated grass and legume seed may be improved by increasing the percentage of rock phosphate and decreasing that of lime. With regard to seed size, the germination of pasture species with small seed size (< ${\varnothing}2$ mm) may be better than medium and large size seeds except alfalfa. Establishment and early growth of grasses can be also improved by increasing the percentage of rock phosphate and decreasing that of lime.

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