• 대한소아치과학회지
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• 제34권1호
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• pp.122-129
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• 2007

본 연구는 복합 레진의 중합률에 영향을 미치는 광조사 시간을 달리하여 치면열구전색제를 중합하였을 경우 이로부터 용리되는 미반응 모노머들을 확인하고 정량화하고자 하였다. 그리고 치면열구전색제 중합 후 표면에 나타나는 미반응 모노머 층을 다양한 방법으로 제거한 후 용리되는 미반응 모노머들을 정량분석함으로써 미반응 모노머의 제거효과를 비교평가하고자 하였다. 광중합 시간에 따라 각각 20초, 40초, 60초간 중합한 후, 중합시간 별로 어떠한 처리도 시행하지 않은 군을 대조군, 증류수로 10초간 세척한 군을 I군(Group I), 75% 알콜에 젖은 면구로 10초간 문지른 군을 II군(Group II), 퍼미스와 러버컵을 이용하여 10초간 처리하고 증류수로 가볍게 세척한 군을 III군(Group III)으로 분류하였다. 표면처리 후 각 시편을 3차 증류수에 넣고 $37^{\circ}C$ 항온 수조에서 10분간 보관한 후 각각의 용리액을 고성능 액체 크로마토그래피를 이용하여 정성 및 정량 분석을 시행하였고 다음과 같은 결과를 얻었다. 1. 모든 대조군과 실험군에서 TEGDMA를 제외한 어떠한 모노머들도 검출되지 않았다. 2. 최소 중합시간, 권장 중합시간, 권장 중합시간 이상의 순으로 중합시간이 증가할수록 TEGDMA의 용리량은 감소하였다. 3. 표면처리를 한 군들은 대조군에 비하여 TEGDMA의 용리량이 유의할 만하게 감소하였다. 4. 표면처리를 한 군 가운데 퍼미스와 러버컵을 이용한 경우 잔존 모노머의 제거 효과가 다른 군에 비하여 유의성 있게 높았다. 5. 권장 중합시간 이상인 60초 중합 후, 퍼미스와 러버컵을 이용하여 표면처리한 경우 가장 적은 양의 모노머 용리량을 보였다.

• The Journal of Advanced Prosthodontics
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• 제13권2호
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• pp.89-99
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• 2021

PURPOSE. This study aimed to compare the accuracy (trueness and precision) of interim crowns fabricated using DLP (digital light processing) according to post-curing time. MATERIALS AND METHODS. A virtual stone study die of the upper right first molar was created using a dental laboratory scanner. After designing interim crowns on the virtual study die and saving them as Standard Triangulated Language files, 30 interim crowns were fabricated using a DLP-type 3D printer. Additively manufactured interim crowns were post-cured using three different time conditions-10-minute post-curing interim crown (10-MPCI), 20-minute post-curing interim crown (20-MPCI), and 30-minute post-curing interim crown (30-MPCI) (n = 10 per group). The scan data of the external and intaglio surfaces were overlapped with reference crown data, and trueness was measured using the best-fit alignment method. In the external and intaglio surface groups (n = 45 per group), precision was measured using a combination formula exclusive to scan data (10C2). Significant differences in accuracy (trueness and precision) data were analyzed using the Kruskal-Wallis H test, and post hoc analysis was performed using the Mann-Whitney U test with Bonferroni correction (α=.05). RESULTS. In the 10-MPCI, 20-MPCI, and 30-MPCI groups, there was a statistically significant difference in the accuracy of the external and intaglio surfaces (P<.05). On the external and intaglio surfaces, the root mean square (RMS) values of trueness and precision were the lowest in the 10-MPCI group. CONCLUSION. Interim crowns with 10-minute post-curing showed high accuracy.

• 대한치과보존학회:학술대회논문집
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• 대한치과보존학회 2001년도 추계학술대회(제116회) 및 13회 Workshop 제3회 한ㆍ일 치과보존학회 공동학술대회 초록집
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• pp.578.2-578
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• 2001

The purpose of this study was to evaluate the color change of composite resin polymerized with three type of light curing units. Composite resin (Z100, shade A2) were condensed inside a 2 mm thick metal mold with 7 mm diameter and devided into three groups. Twenty specimens of each light curing units were made. Group 1 : the specimens were polymerized with Apollo 95E (AP) for 3 seconds ($1370{\;}㎽/\textrm{cm}^2$). Group 2: the specimens were polymerized with Spectrum 800 (SP) for 10 seconds ($250{\;}㎽/\textrm{cm}^2$) and 30seconds ($700{\;}㎽/\textrm{cm}^2$). Group 3: the specimens were polymerized with XL 3000 (XL) for 40 seconds ($480{\;}㎽/\textrm{cm}^2$).(omitted)

• 대한치과의사협회지
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• 제57권3호
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• pp.175-184
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• 2019

Increasing the aesthetic needs of patients and decreasing the use of amalgam had led to increased demand for dental resin composite. Thereby, light curing unit (LCU) has become an essential equipment in dental clinic. To ensure long-term prognosis of photopolymerized materials, LCU should have a uniform and consistent radiant output and an emission spectrum that includes the active wavelength range of photoinitiators. In addition, when the correct use and thorough maintenance and repair of LCU are performed, the higher success rate of restoration using photopolymerization materials will be achieved.

• 대한소아치과학회지
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• 제32권4호
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• pp.604-610
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• 2005

현재 광중합 복합레진은 치아의 수복을 위하여 많이 사용되며 복합레진이 많이 사용되는 만큼 광중합을 위한 광중합기도 다양하게 사용된다. 하지만 광중합기에 따른 복합레진의 미세누출은 아직 연구대상이다. 본 연구의 목적은 광중합기에 따라 발생하는 미세누출에 대한 평가를 하는 것으로 최근에 개발된 광중합기의 중합능력을 전통적 인 할로겐 광중합기와 비교하는 것이다. 전통적으로 사용되어지던 저출력 할로겐 광중합기(Optilux 360), 일반 플라즈마 아크 광중합기(Flipo). 저발열 플라즈마 아크 광중합기 (Aurys), 고출력 LED 광중합기 (Freelight 2)를 사용하였다. 건전한 유구치에 와동을 형성한 후 복합레진(Z100)을 동일한 레진 접착제 (Scotchbond Multi-Purpose)를 사용하여 충전한 후 각 광중합기를 이용하여 복합레진을 중합시켰다. 광중합기의 광조사 시간은 제조사에서 복합레진의 광중합을 위해 권장하는 시간으로 Optilux 360은 40초, Flipo는 5초, Aurys는 9초, Freelight 2는 20초간 조사하였다. Optilux 360만 광강도의 변화가 없는 광조사 방식이며 그 외 광중합기들은 광강도가 광조사 중에 증가되는 soft-start 광조사 방식이다. 각 시편을 증류수에 24시간 보관 후 열 순환을 1000회 시행한 후 2% methylene blue용액으로 색소침투를 시켰으며 각 시편을 절단하여 색소침투 정도를 점수화시켜 다음과 같은 결론을 얻었다. 미세누출을 각 점수화하였을 때 Aurys가 평균 0.95로 가장 낮은 값을 보였고 Freelight 2(1.05), Flipo(1.25), Optilux 360(1.30)의 순이었다. 하지만 각 광중합기군 간의 값에서는 통계학적인 유의성은 관찰되지 않았다(P>0.05).

• Restorative Dentistry and Endodontics
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• 제39권3호
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• pp.155-163
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• 2014

Objectives: Light-curing of resin-based materials (RBMs) increases the pulp chamber temperature, with detrimental effects on the vital pulp. This in vitro study compared the temperature rise under demineralized human tooth dentin during light-curing and the degrees of conversion (DCs) of three different RBMs using quartz tungsten halogen (QTH) and light-emitting diode (LED) units (LCUs). Materials and Methods: Demineralized and non-demineralized dentin disks were prepared from 120 extracted human mandibular molars. The temperature rise under the dentin disks (n = 12) during the light-curing of three RBMs, i.e. an Ormocer-based composite resin (Ceram. X, Dentsply DeTrey), a low-shrinkage silorane-based composite (Filtek P90, 3M ESPE), and a giomer (Beautifil II, Shofu GmbH), was measured with a K-type thermocouple wire. The DCs of the materials were investigated using Fourier transform infrared spectroscopy. Results: The temperature rise under the demineralized dentin disks was higher than that under the non-demineralized dentin disks during the polymerization of all restorative materials (p < 0.05). Filtek P90 induced higher temperature rise during polymerization than Ceram.X and Beautifil II under demineralized dentin (p < 0.05). The temperature rise under demineralized dentin during Filtek P90 polymerization exceeded the threshold value ($5.5^{\circ}C$), with no significant differences between the DCs of the test materials (p > 0.05). Conclusions: Although there were no significant differences in the DCs, the temperature rise under demineralized dentin disks for the silorane-based composite was higher than that for dimethacrylate-based restorative materials, particularly with QTH LCU.

• Restorative Dentistry and Endodontics
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• 제45권4호
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• pp.55.1-55.12
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• 2020

Objectives: This study investigated the effects of physically damaged and resin-contaminated tips on radiant emittance, comparing them with new undamaged, non-contaminated tips using 3 pieces of spectrophotometric laboratory equipment. Materials and Methods: Nine tips with damage and/or resin contaminants from actual clinical situations were compared with a new tip without damage or contamination (control group). The radiant emittance was recorded using 3 spectrophotometric methods: a laboratory-grade thermopile, a laboratory-grade integrating sphere, and a portable light collector (checkMARC). Results: A significant difference between the laboratory-grade thermopile and the laboratory-grade integrating sphere was found when the radiant emittance values of the control or damaged/contaminated tips were investigated (p < 0.05), but both methods were comparable to checkMARC (p > 0.05). Regardless of the method used to quantify the light output, the mean radiant emittance values of the damaged/contaminated tips were significantly lower than those of the control (p < 0.05). The beam profile of the damaged/contaminated tips was less homogeneous than that of the control. Conclusions: Damaged/contaminated tips can reduce the radiant emittance output and the homogeneity of the beam, which may affect the energy delivered to composite restorations. The checkMARC spectrophotometer device can be used in dental offices, as it provided values close to those produced by a laboratory-grade integrated sphere spectrophotometer. Dentists should assess the radiant emittance of their light-curing units to ensure optimal curing in photoactivated, resin-based materials.

• 대한소아치과학회지
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• 제34권1호
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• pp.81-90
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• 2007

본 연구에서는 세 가지 서로 다른 광원(할로겐 램프 :. Elipar Trilight ; 3M ESPE, Seefeld, Germany, Light Emitting Diode (LED) ; Elipar Freelight2 ; 3M ESPE, Seefeld, Germany, 플라즈마 광 : Flipo ; LOKKI, France)을 사용하여 브라켓과 광원사이의 거리에 따른 광중합형 글라스 아이오노머 시멘트(Fuji ORTHO LC : GC, Japan)의 전단 결합 강도를 알아보고자 하였다. 1. 광중합기에 따른 전단 결합 강도는 광중합기로부터 브라켓까지의 거리가 0mm일 때 3가지 광원에 유의할 만한 차이는 보이지 않았고 광중합기로부터 브라켓까지의 거리가 3mm, 6mm일 때, 할로겐 광과 플라즈마 광 사이에는 유의할 만한 차이가 없었으나 LED 광은 유의성 있게 낮은 전단 결합 강도를 나타냈다. 2. 할로겐 광과 플라즈마 광으로 광중합시 거리에 따른 전단 결합 강도에 유의한 차 없었고 LED광을 사용하여 광중합시에는 거리가 증가할수록 전단 결합 강도가 감소하였다. 특히 0mm에서 3mm로 거리가 증가시 유의할 만한 감소를 나타내었다.

• Restorative Dentistry and Endodontics
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• 제21권1호
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• pp.360-365
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• 1996

The purpose of this study was to evaluate the changes in the degree of conversion on a composite resin surface following heat treatment and mylar strip finishing. The effects of the time interval between the light-curing and heat-curing process were also evaluated. The composite resin surface which had been covered with a coverglass showed a lower conversion rate than the surface from which a layer of $500{\mu}m$ was ground away. The composite resin surface was definitely affected by oxygen during the heat curing process when it had not been insulated. When the composite resins were heat cured after 3 days of storage following the light curing process, the increased in the degree of conversion through heatcuring was limited.

• 대한치과보존학회:학술대회논문집
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• 대한치과보존학회 2003년도 제120회 추계학술대회 제 5차 한ㆍ일 치과보존학회 공동학술대회
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• pp.613-613
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• 2003

The purpose of this study was to compare the effect of exponential curing method with conventional curing and two step soft start curing method on polymerization shrinkage of composite resins. Three brands of composite resins (Synergy Duo Shade, Z-250, Supreme) and three brands of light curing units (Spectrum 800, Elipar Highlight, Elipar Trillight) were used. In this study, the diameter of specimen was 5.5mm and height 1.6mm and the specimen was cured for 40 seconds. The shrinkage was measured by custom made linometer. The amount of linear polymerization shrinkage recorded in the computer every 0.5 second for 90 seconds. Each group was measured 10 times.(omitted)