• 제목/요약/키워드: light curing

검색결과 466건 처리시간 0.031초

초기 저광도 광중합이 레진 수복물의 결합강도에 미치는 영향에 관한 연구 (A STUDY OF THE EFFECT OF LOW INTENSITY INITIAL LIGHT CURING ON THE BOND STRENGTH OF RESIN RESTORATION)

  • 한미란;권순원;김종수
    • 대한소아치과학회지
    • /
    • 제28권1호
    • /
    • pp.45-53
    • /
    • 2001
  • 레진 수복에서 초기에 저광도로 중합하여 레진의 유동성을 허용함으로써 중합시 내부응력을 상쇄하며, 다시 고광도로 중합하여 레진의 물성도 유지할 수 있는 방법이 시도되고 있어 초기 저광도 중합이 상아질과의 결합 강도와 레진의 미세경도에 미치는 영향을 알아보고자 하였다. 소의 건전한 하악 전치 20개를 3개의 절편으로 절단하여 각 군에 배분하고 상아질면에 레진을 충전한 후, I군은 $450mW/cm^2$의 광도도 40초간, II군은 $300mW/cm^2$$600mW/cm^2$의 광도로 각각 20초씩 III군은 $250mW/cm^2$$450mW/cm^2$에서 각각 20초씩 광중합하여 전단 결합 강도를 측정하였고, 직경 5.0mm깊이 2.0mm레진 시편을 제작하여 상, 하면 중앙에서 Vickers 미세 경도를 측정하였다. 전단결합 강도는 초기 저광도 중합군의 평균이 다소 높았으나 각 군간 통계학적 유의한 차이는 없었으며, 미세 경도는 상하면 모두에서 각 군간 통계학적으로 유의한 차이는 보이지 않았다.

  • PDF

UV광 측정용 아조벤젠 코팅된 FBG의 열적 효과 제거 및 파장 의존성에 대한 연구 (The Study of Thermal Effect Suppression and Wavelength Dependence of Azobenzene-coated FBG for UV Sensing Application)

  • 최동석;김현경;안태정
    • 한국광학회지
    • /
    • 제22권2호
    • /
    • pp.67-71
    • /
    • 2011
  • 본 논문에서는 ultraviolet (UV) 광의 세기를 원격으로 측정하기 위한 아조벤젠 (azobenzene) 코팅된 fiber Bragg grating (FBG)를 구현하였다. 아조벤젠 폴리머는 UV 광에 의해서 탄성이 변화하여 FBG의 코어 격자의 주기 변화를 유도하여 중심파장을 이동시킨다. 중심파장의 이동은 UV 광과 UV 이외의 파장대역의 빛에 의해서 복합적으로 발생하는데 중심파장의 이동량은 약 0.18 nm 이다. 측정의 정확성을 향상시키기 위해서 광원의 복사열에 의한 중심파장의 이동을 열차단 필터(thermal filter)를 사용하여 제거한 결과 중심파장의 이동량은 약 0.06 nm로 다소 감소하였지만 분석 결과 열에 의한 이동량이 충분히 제거된 것을 확인하였다. 또한 서로 다른 방법인 열경화법과 UV 경화법으로 각각 제작된 아조벤젠 폴리머를 이용하여 아조벤젠 코팅 FBG를 제작하였고, 각 제조법에 따른 UV센서로서의 적합성을 확인하였다. 몇 개의 밴드패스 필터(band pass filter)를 사용하여 파장에 대한 민감도를 측정한 결과, 단위 UV 세기당 중심파장의 이동량은 370nm 파장 밴드에서 가장 큰 값인 0.029로, 단파장 영역에서 반응성이 우수하다는 사실을 확인 하였다. 아조벤젠 폴리머의 흡수 스펙트럼과 아조벤젠 코팅 FBG의 파장 의존도가 서로 잘 일치하는 것을 확인하였다.

오토클레이브 양생시간에 따른 경량기포콘크리트의 강도 변화에 관한 실험적 연구 (Strength Variations of Light Weight Foamed Concrete According to the Autoclaving Time)

  • 강철;강기웅;곽은구;노재명;권기주;김진만
    • 한국건축시공학회:학술대회논문집
    • /
    • 한국건축시공학회 2005년도 춘계 학술기술논문발표대회 논문집
    • /
    • pp.57-60
    • /
    • 2005
  • This is the experimental study on the strength development of the light weight concrete block according to the autoclaving time. The calcareous source used the cement, siliceous material used the bottom ash ground to fine particle, and the PP fiber used to increase toughness. The results of this experiment are as follows. According to the increase of autoclaving time and the fiber content, compressive and flexural strengths are increased. Despite of the changes of the autoclaving time, tobermorite was produced on each of the specimens. However, the phase of tobermorite was changed in accordance with the changes of autoclaving time.

  • PDF

네가지 상아질 접착제의 전단 결합 강도 비교 (COMPARISON OF SHEAR BOND STRENGTHS OF FOUR DENTINAL ADHESIVES)

  • 조경미;허복;이희주
    • Restorative Dentistry and Endodontics
    • /
    • 제21권1호
    • /
    • pp.280-288
    • /
    • 1996
  • The purpose of this study was to assess comparatively the shear bond strength on dentin of four dentin bonding agents used in conjunction with light-curing composite resins. Clearfil New Bond, Scotchbond Multipurpose Dentin Adhesive, All-Bond 2 and X-R Bond were applicated on labial dentin surfaces just below dentin - enamel juction of bovine incisor teeth. After shear bond strength testing with the universal testing machine, the bonding interface of the specimens were observed under light stereomicroscope. Following results were obtained. 1. The shear bond strength was high in the order of B,C,D,A and group B Scotchbond Multipurpose Dentine Adhesive revealed greater bond strength than Clearfil New Bond and X-R Bond. (p<.001) 2. When using ANOVA and Duncan's multiple range test, there were statistical differences among the four groups, except between group Band C,group D and A. 3. There was no relationship between mode of failure and shear bond strength.

  • PDF

Synthesis and Characterization of Crosslinked Hole Transporting Polymers for Organic Light Emitting Diodes

  • Jang, Do-Young;Lim, Youn-Hee;Kim, Joo-Hyun;Kim, Jang-Joo;Shin, Jung-Hyu;Yoon, Do-Y.
    • 한국고분자학회:학술대회논문집
    • /
    • 한국고분자학회 2006년도 IUPAC International Symposium on Advanced Polymers for Emerging Technologies
    • /
    • pp.235-235
    • /
    • 2006
  • Triphenylamine derivatives play important roles as hole transporting materials in organic light emitting devices. However, low molecular weight triphenylamine derivatives show low glass transition temperature and aggregation behavior, and the vapor deposition step of low molecular weight materials is incompatible with large area display fabrication. Conventional polymer PEDOT-PSS HTL has serious drawbacks such as the ITO anode corrosion, poor surface energy match with aromatic EMLs. To solve these problems, we introduced crosslinkable units to triphenylamine-based polymers to make insoluble HTL by thermal curing following spin-coating. Electrochemical and optical properties of the new hole transporting materials were investigated. In addition, the device characteristics obtained with new hole transporting polymers were investigated in details.

  • PDF

UV 나노임프린트를 위한 UV 경화성 수지 개발 및 경화 특성 평가 (Development of UV curable polymer and curing characteristics estimation for UV nanoimprint)

  • 이진우;이승재;이응숙;정준호;조동우
    • 한국정밀공학회:학술대회논문집
    • /
    • 한국정밀공학회 2003년도 춘계학술대회 논문집
    • /
    • pp.1220-1223
    • /
    • 2003
  • The UV nanoimprint technology uses the UV light as the energy source. Because the imprint process is carried out in room temperature and low pressure, this technology has its own merits compared to the thermal nanoimprint. However, in UV nanoimprint technology, a resin which has low viscosity is essential for the improvement of accuracy. In this research, a resin (named as IMS01) which has relatively low viscosity was developed. And a measurement system was developed in order to measure the degree of cure of the resin. The measurement system which is composed of FT-IR, UV light source and optical guide can measure the degree of cure in real time. From the experimental results, it was found that the IMS01 is cured more rapidly than existing resin (PAK01).

  • PDF

UV-LED를 이용한 광조형 장치 개발 (Development of Stereolithography Apparatus by using UV-LED)

  • 윤해룡;고태조;김호찬
    • 한국기계가공학회지
    • /
    • 제13권2호
    • /
    • pp.15-20
    • /
    • 2014
  • The stereolithography(SL) process is a type of fabrication technology which relies on photopolymerization. It has a relatively simple fabrication process and a resolution of several tens of ${\mu}m$. Recently, SL technology has been applied to various areas, such as bioengineering and MEMS devices, due to the development of advanced materials. This technologycan be divided intothe scanning(SSL) and projection (PSL) types. In this paper, in stereolithography, parts are fabricated by curing photopolymeric resins with light. The application of stereolithography can now include fabricated parts. This process, called stereolithography, can fabricate parts by taking into account theirdegrees of geometry complexity. In particular, UV-LED stereolithography can perform quite rapid fabrication in which specific cross-sections are cured upon exposure to light.

Preparation and Characterizations of Polymethylmethacrylate (PMMA)/Acrylate Rubber (ACM) Blend for Light Diffuser Applications

  • Lee, Byung Hwan;Chang, Young-Wook;Lim, Hyung Mi
    • Elastomers and Composites
    • /
    • 제50권1호
    • /
    • pp.49-54
    • /
    • 2015
  • Dynamically vulcanized PMMA/ACM (80 wt%/20 wt%) blend using DCP as a curing agent was prepared using internal mixer. The morphology, mechanical properties, optical properties, melt viscosity and die swell were characterized by using FE-SEM, tensile test, Izod impact test, dynamic mechanical analysis, ARES and capillary rheometer, respectively. The blends show a phase-separated morphology in which ACM are dispersed in PMMA matrix. Dynamically vulcanized blend exhibits higher mechanical properties, higher melt viscosity, and die swell as compared to simple blend. And, the dynamically vulcanized blend showed total transmittance of more than 75% and haze of higher than 90%, which enable it to find potential applications to fabricate an optical diffuser by extrusion process.

고체 amine 광개시제에 따른 치과용 복합수지의 중합효율 (Photopolymerization efficiency of dental resin composites with solid amine photoinitiators)

  • 선금주
    • 대한치과기공학회지
    • /
    • 제28권1호
    • /
    • pp.43-52
    • /
    • 2006
  • Three t-amines, 4-(dimethylamino)benzoic acid (ABA), 4-(dimethylamino)benzaldehyde (MBA), 4-(dimethylamino)benzophenone (MBP), were investigated as new visible light photoinitiators for a dental resin composite of UDMA in order to improve photopolymerization effect. Three t-amines mixed with three photosensiizers, CQ, PD and DA, respectively. And the photopolymerization effect of photoinitiators were compared with that of 4-(dimethylamino)ethyl methacrylate (AEM), the most widely used photoinitiator. The photopolymerization efficiency of UDMA containing the photoinitiator increased with irradiation time. The increase was in the order: MBP

  • PDF

A newly-designed method to measure liner polymerization shrinkage

  • Ikejima, Iwao;Matsuzawa, Norihiko;Momol, Yasko;Kohno, Atsushi
    • 대한치과보존학회:학술대회논문집
    • /
    • 대한치과보존학회 2003년도 제120회 추계학술대회 제 5차 한ㆍ일 치과보존학회 공동학술대회
    • /
    • pp.604-604
    • /
    • 2003
  • I. Objectives Newly-designed method was evaluated to measure the linear polymerization shrinkage of light-cured resin composites. II. Materials and Methods A resin composite(Clearfil AP-X, Kuraray, Japan) was filled into a vinyl-polysiloxan mold(1 to 8mm-depth, and 7mm-diameter). As indicators, 4 beads(Retention Beads 2 SS, GC, Japan;particle size $200{\;}\mu\textrm{m}$) were placed diagonally on the resin surface of a mold. The coordinates (x, y, z, pasition) of each indicator were measrued by a measuring-microscope after which the resin surface was irradiated by a curing-light source(Optilux 500, Demetron/Kerr, USA) for 40 sec. After 20 sec the coordinates were again measured.(omitted)

  • PDF