• Title/Summary/Keyword: lead limit test

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Comparison of Standard and Lend Limit Test of Various Institutes on Lead Limit of Synthetic and Natural Food Additives (합성 및 천연 식품첨가물의 납함량에 대한 여러 기관의 규격기준 및 납시험법 비교)

  • Shin Dong-Hwa;Kim Yong-Suk;Jeong Do-Yeong;Lee Young-Hwan;Bang Jeong-Ho;Om Ae-Son;Shin Jae-Wook;Lee Tal-Soo;Jang Young-Mi;Hong Ki-Hyoung;Park Sung-Kwan;Park Sung-Kug;Kwon Yong-Kwan
    • Journal of Food Hygiene and Safety
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    • v.21 no.2
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    • pp.82-91
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    • 2006
  • Standard and lead limit test in general test method of Korea, Japan, Joint FAO/WHO Expert Committee of Food Additives (JECFA), USA, and EU on synthetic and natural food additives were compared. There were found that the general test methods in 'Korea Food Additives Code' were different from standards of various institutes on lead limit test. For the lead limit test of food additives, Korea used dithizone method, Japan used atomic absorption spectrophotometry, and USA used dithizone method, flame atomic absorption spectrophotometric method, atomic absorption spectrophotometric graphite furnace method, and APDC extraction method. In addition, JECFA and EU used dithizone method and atomic absorption spectrophotometric method. The dithizone methods of Korea, USA, and JECFA were nearly identical. In the case of USA, JECFA, and EU, the analytical methods for lead limit test were shown in individual monograph. Lead limit test against 13 synthetic, such as magnesium stearate and L-cystine, and 12 natural, such as gua gum and diatomaceous earth, food additives distributed in Korea were performed by the analytical method of each institute. Although all institutes use various methods for analysis of lead, contents of lead in food additives tested fell into the standard of each institute.

Microstructural Analysis of the Solidified Arsenic-containing Heavy Metal Sludge (비소를 함유한 중금속슬러지 고화체의 미세구조적 분석)

  • Kim, Yeong-Kwan;Jeong, Myoung-Sun
    • Journal of Industrial Technology
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    • v.16
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    • pp.169-174
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    • 1996
  • Microstructural analyses of synthetic arsenic-containing heavy metal sludges solidified with Portland cement were performed. Heavy metal sludges containing 0.04M of cadmium, chromium, copper, lead, and arsenic were prepared by sodium hydroxide precipitation and successive vacuum filtration. The sludges mixed with cement were cured for 14 days. The solidified sample was characterized by 1) leaching test, 2) scanning electron microscopy and 3) X-ray diffractometry. Of the metals tested, only Pb concentration in the leachate exceeded the Korean regulatory limit. The level of lead in the leachate was as high as 10 times the regulatory limit. X-ray analysis suggested that the metal hydroxides might be present in complex or impure crystalline phases.

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Research of Determining the Compressed Gauge Limit Compensating for Guage Error (계측기오차 보상을 위한 압축한계 설정에 관한 연구)

  • Lee, Jong-Seong;Ko, Sung-Ho
    • Journal of Industrial Technology
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    • v.22 no.B
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    • pp.89-93
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    • 2002
  • When testing products before shipment to the customer, quality characteristics are measured to decide whether or not their values are between the specification limits. Unfortunately, this testing procedure can lead to incorrect decisions because of gauge error. That is, good products can erroneously be qualified as bad, and bad products as good, and this has consequences for producer's and consumer's risk. In cases of such as this, the compressed gauge limit can be used to achieve the desired product quality level dictated by the manufacturer or the customer. A compressed gauge limit is a limit set by the manufacturer on a test gauge that is tighter than the specification limit established by the customer. The compressed gauge limits should be set at levels to achieve the defect levels desired by the customer and simultaneously minimize the loss of good product that is rejected due to errors in the gauges. In this article, the models for determining the defect levels and the losses obtained by adding compressed gauge limits will be developed. A response surface model approach is utilized which allows an optimal operating condition to be generated relatively easily.

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동전기 기법과 Zeolite를 이용한 중금속 오염토의 고정화에 관한 연구

  • 김종윤;김기년;김병일;김수삼
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2004.09a
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    • pp.195-198
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    • 2004
  • This study applied EK method to remediate contaminated soil by heavy metal(Pb), tried to increase the efficiency of remediation using zeolite as enhanced EK remediation method to overcome the limit of traditional EK remediation method. Adsorption tests on Pb were conducted to apply the EK extraction and test conditions which contained the electrode reversal, operating time were established. After tests, lead-ions were transported into the specific position of zeolite by EK phenomena, then the immobilization of lead-ions at zeolite was developed. Based on these tests, the efficiency of remediation is different with its test conditions. In addition, the efficiency of remediation was improved dramatically by adding zeolite without electrode reversal and satisfied TCLP regulation of EPA in USA through the whole sample range. Finally, absorption and immobilization capacity of zeolite were proved its excellence and confirmed the possibility of application as enhanced EK remediation method.

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Static Test and Analysis of Wing Support Structure for External Stores (외부장착물지지 주익구조 정적 시험 및 해석)

  • Uhm, Wonseop;Yoon, Jongmin
    • Journal of Aerospace System Engineering
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    • v.9 no.1
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    • pp.28-34
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    • 2015
  • Armed aircraft of a basic trainer class installs external stores under wing box by using pylon and performs an operation such as weapon delivery and jettison, and should be designed to withstand all kinds of loads applied to external stores. The static strength test of pylons and wing box was performed to assess the static strength of pylon and their support structures for substantiation. Based on the test, the structures were verified to fully satisfy a given design requirement. In this paper, methods of test load generation of wing box and pylon, evaluation of test result data and design result of test set-up were presented. Comparing the FEM analysis with the same test data can lead to good match and reasonable deviation between both. Finally, based on the test and the analysis, the static strength of test article was substantiated and the reliability and effectiveness of analysis math model were obtained.

Correlation Development on Critical Power in a Spherical Narrow Gap (구형 간극에서의 임계 출력에 대한 상관식 개발)

  • Park, Rae-Joon;Ha, Kwang-Soon;Kim, Sang-Baik;Kim, Hee-Dong;Jeong, Ji-Hwan
    • Proceedings of the KSME Conference
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    • 2001.06e
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    • pp.235-240
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    • 2001
  • The CHFG (Critical Heat Flux in Gap) test results have been evaluated to quantify the critical power in hemispherical narrow gaps and a new correlation has been developed. The CHFG test results have shown that increases in the gap thickness and pressure lead to an increase in critical power. The pressure effect on the critical power was found to be much milder than predictions by CHF correlations of other researches. From the CHFG test results, a new correlation on critical power in the hemispherical gap has been developed using the non-dimensional parameters as follows: $$\frac{qCHF}{{\rho}g^hfg}{\cdot}4\sqrt{\frac{{\rho}_g^2}{g{\sigma}{\Delta}{\rho}}=\frac{0.1042}{1+0.1375({\rho}g/{\rho}l)^{0.21}(D/s)}$$ The developed correlation has been expanded to apply the spherical geometry using the Siemens/KWU's correlation.

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Investigation on the Material and Migration Tests of Gas Impermeable Plastic Vacuum Packaging Materials for Food-Contact Use (식품용 합성수지제 공기차단성 포장재에서의 재질 및 용출시험량 조사)

  • Lee, Jung-Pyo;Lee, Youn-Kyu;Lee, Keun-Taik
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.14 no.1
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    • pp.35-42
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    • 2008
  • Twenty eight gas impermeable plastic films for food-contact application were collected in the domestic market and material and/or migration tests for overall migration, antioxidants, potassium permanganate consumption, heavy metal, and plasticizers were carried out. The average overall migration values for NY/PE or NY/LLDPE, PETP/PE, and PVDC packaging films obtained by using n-heptane as fatty food simulant were 7.6, 6.9 and 14.1 mg/L, respectively. These values were much lower than the limit values of 150 and 30 mg/L for polyethylene and polyvinylidene chloride prescribed in the Korea Food Code. In almost of the packaging materials tested, the antioxidants such as Irganox 1010, Irganox 1076 and Irgafos 168 were found. The migration test result showed that almost of all samples except PVDC film contained Irganox 1076 and Irgafos 168, while the maximum migration value of Irganox 1076 into n-heptane was found in the Ny/PE/LLDPE(15/25/50 ${\mu}m$) sample at the concentration of 216.9 ${\mu}g/g$. From the plastic packaging samples tested, plasticizers such as DEP, DPRP, DBP, DPP, BBP, DCHP, DEHP, DEHA and observed above the detection limit. Consumption amount of potassium permanganate was much lower than the limit value of 10 mg/L. In the material test for heavy metals, cadmium and lead were determined at the concentrations far below the limit value of 100 mg/kg. The migration test for cadmium and lead showed a lower value than the detection limit. Therefore, it can be concluded that the safety status of the plastic films tested met the requirement of limit values as prescribed for the material and migration tests of food packaging utensils, containers and packages of the Korea Food Code.

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Quantitative Analysis of Heavy Metals in Packaging Papers

  • Jo, Byoung-Muk;Jeong, Myung-Joon
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.39 no.5
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    • pp.45-51
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    • 2007
  • This study was carried out to investigate various heavy metal contents in packaging papers by pre-treatments for ICP-ES (Inductively Coupled Plasma Emission Spectrometry) analysis. Pre-treatment methods of heavy metals in this study include extraction, migration and decomposition methods (dry ashing, $HNO_3-HClO_4-HF,\;HNO_3,\;and\;H_2SO_4-HNO_3$). Test results were compared with conventional extraction (water) and migration (3% acetic acid) methods. The five representative heavy metals (Cd, As, Pb, Cr and Hg) were analyzed. For Cd, Hg, and As, the results were below detection limit of the instrumental technique. It was considered that the migration test was a better method compared to extraction test, but all the decomposition methods showed much higher detection values than the extraction or migration test. In case of recycled corrugated containers, 3% acetic acid solution extracted about 25% of chromium and 30% of lead compared to the content by decomposition methods. Among all decomposition methods, the nitric acid - perchloric acid - hydrofluoric acid treatment brought a slightly higher detection value than others, but there was no significant difference among them except sulfuric acid - nitric acid method.

Development of MR Mount for Vibration Control of Marine Diesel-Generator Set (박용 발전기세트 진동 제어용 MR 마운트 개발)

  • Kang, Ok-Hyun;Kim, Won-Hyun;Joo, Won Ho;Park, Jun-Hee
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2014.04a
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    • pp.381-385
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    • 2014
  • This paper investigates the magneto-rheological(MR) mount for the marine diesel-generator(D/G) sets. Sometimes, significant vibrations over the allowable limit are observed on the D/G sets due to their huge excitation forces. Because the severe vibration can lead to structural damages to the D/G sets, it should be reduced below the limit. Although passive mounts with rubber isolators are usually used, the vibration reduction performance is not always sufficient. In addition, expecting that the vibration levels required by customers will get more severe, vibration reduction devices need to be developed. To the aim, the flow mode type of MR mount has been designed. Especially, the annular-radial configuration was adopted to enhance the damping force within the restricted space. The geometry of the mount has been optimized to obtain the required damping force and the magnetic field analysis has been carried out using ANSYS APDL. To verify the performance of the developed MR mount, an excitation test was conducted. In addition, they were applied to a medium-speed diesel generator and it was verified that about 40% of vibration reduction was yielded.

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A Study on the Guarantee of Learning Rights of Radiology Students in Nuclear Safety Act (원자력안전법에 대한 방사선학과 학생들의 학습권 보장에 관한 연구)

  • Lee, Bo-Woo
    • Journal of radiological science and technology
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    • v.45 no.2
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    • pp.159-164
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    • 2022
  • The study developed a radiation dose measurement program in the radiology laboratory to measure how much exposure the students are exposed to during the radiology class, to request for the improvement and the revision of the current Nuclear Safety Act. The experimental program is shown in the following figure, and experiments were conducted to determine the degree of radiation exposure in the control room with a lead gown at a distance of 1 m, 2 m, and 1 m, and in a control room with a radiographic lead glass wall. The duration of the experiment was 3 months from April to June, when radiation imaging practice classes were conducted, and 128 hours of imaging practice per month were conducted. In order to find out the dose of radiation dose during radiology imaging practice class, the experiment was carried out from April to June for 3 months, and according to the program, the results of exposure dose were 0.34 mSv at 1 m distance, 0.01 mSv at shielding of lead gown at 1 m distance, 0.16 mSv at 2 m distance, and 0.01 mSv at control room with radiation lead glass wall. The exposure dose from the test results was much below the annual general public limit dose of 1 mSv. The restriction on the operation of the radiation equipment in the practice of the students is a regulation that infringes the right of students to learn, and amendments or exemptions of Nuclear Safety Act should be enacted to ensure that it does not violate the fundamental right to learn for students in radiology.