• Title/Summary/Keyword: ion-exchange resin

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Determination of Impurities in Aluminum by Neutron Activation Analysis

  • Kim, Nak-Bae;Bak, Hae-ill;Lee, Chul
    • Nuclear Engineering and Technology
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    • v.12 no.1
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    • pp.29-38
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    • 1980
  • A radiochemical separation scheme for the neutron activation analysis is developed for the determination of 28 elements in aluminum. The scheme is based on a group separation using ion-exchange resin and mineral exchanger. Present work has employed mineral acids and their partly organic mixture excluding HF as the media as well as common glass wares. For the determination, gamma-ray spectroscopy using $3"\times3"\;Nal(TI)$ detector and a single comparator method are used.

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Ambient Pressure Dried Silica Aerogel Thin Film from Water Glass

  • Cha, Young-Chul;Yoon, Jong-Seol;Lee, Jun;Hwang, Hae-Jin;Moon, Ji-Woong
    • Journal of the Korean Ceramic Society
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    • v.45 no.2
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    • pp.87-89
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    • 2008
  • A nano structured silica aerogel thin film was manufactured from inexpensive sodium silicate (water glass) using an ambient pressure drying method. High purity silicic sol was prepared by passing a water glass solution through an ion exchange resin, and the gel films were prepared on a modified glass substrate via dip coating. The dip coating conditions, such as coating time and solvent, were optimized. The optical and physical properties of the obtained silica aerogel thin film were characterized using a UV-visable spectrometer and a scanning electron microscope.

Feasibility Study with Several Sorption Materials to Treat Road Runoff Pollutions (흡착 소재별 도로 노면 유출 오염원의 저감성 비교 연구)

  • Park, Sangwoo;Oh, Jeill;Choi, Younghwa
    • Journal of Korean Society of Water and Wastewater
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    • v.20 no.5
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    • pp.709-717
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    • 2006
  • This research was conducted to figure out the feasibility of several sorption materials to treat various pollutants in road runoff. In advance of the major feasibility test with various sorption materials, the separation process with $1.2{\mu}m$ filter was conducted and showed that slight portion of pollutants was removed(Orgamic pollutant - 20%, Nutrient salt - 50%, Heavy metals - 0~30%). To remove dissolved pollutants in runoff, various materials were tested through an isotherm sorption experiment. As a result, GAC showed most effective material among them to lessen most contaminants such as organic compounds and nutrients. On the other hand, ion-exchange resin and Zeolite showed limited usefulness on the some heavy metals. Freundlich model was most suitable for the current experiment data, and the amount of adsorbent (GAC) could calculated based on this model.

The Variation of the Contents of Free Amino Acids and the Carbohydrates in the Whole Plant of Fagopyrum escullentum Moench during the Stages of Growing (모밀(Fagopyrum esculentum Moench)생장과정중의 유리 Amino 산과 당질의 성장에 관하여)

  • 황희자
    • YAKHAK HOEJI
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    • v.8 no.2
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    • pp.48-53
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    • 1964
  • At the different growing stages of Fagopyrum esculentum Moench planted at the green house and out doors, the contents of free amino acids in the whole plants,were determined quantitatively by spot-extract colorimetric method (J. Awapara method) using the chromatograms obtained by the ion-exchange resin and paper chromatographic method. And the contents of carbohydrate in the whole plant were determined by Bertrand method. The results were summarized as follows. 1. Almost same kinds of free amino acids were detected in the both plants. 2. Concentrations of most amino acids was increased progressively during growth; further growth was accompanied by decreased concentrations. 3. Rate of growth and increasing of total amino acid content of green house plant is greater than that of out dorrs plant. 4. At the same stages of gwoth, total free amino acid content of green house plant is higher than that of out doors plant but sugar content is lower. 5. There was rapidly increasing of sugar content and decreasing of total free amino acid content except asparagine during mature of seeds.

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The Influence of Butyl Alcohol on the Distribution Coefficients of Metal Ions (금속이온의 분포계수에 미치는 부틸알코올의 영향)

  • Dong Won Kim
    • Journal of the Korean Chemical Society
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    • v.25 no.1
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    • pp.21-25
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    • 1981
  • A study was made of the influence of butyl alcohol on the distribution coefficients of barium and mercury ions between the ion exchange resin, Dowex 50w-x8, 200~400 mesh and solutions containing hydrochloric acid, butyl alcohol and water. The determination of the distribution coefficients of barium and mercury are made by using the batch method. The distribution coefficients of metal ions decrease generally as the number of branches of carbon in the molecule of butyl alcohol increase. It shows that solubility in water and stereo-isomerism of the butyl alcohol have influence upon the distribution coefficient of barium and mercury.

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On the Microbial Contamination in Softdrink Manufacturing Process (청량음료의 미생물 오염에 대하여)

  • 김용배;이병국;유건희;조남선
    • Korean Journal of Microbiology
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    • v.11 no.3
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    • pp.129-133
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    • 1973
  • The authors have investigated about the microbial contamination of goods which is a criterion of hygienic control. Conducting on investigation, a special attention has been paid on the rate of microbial contamination in the goods, especially in manufacturing process of the softdrink. The authors also made an experiment on total microbes which is the criterion of contamination in each step of the process and in raw materials together with materials to be used for subdividing. Results obtained were as follows : 1) The orgin of microbial contamination was found in bottle cap and in tap water, that is, there appeared 9 colony per ml in bottle cap and 31-74 colony per ml in tap water, respectively. 2) It was found that microbial contamination are 4 colony per ml in average through year. However, it appeared 1 colony per ml in winter and 8 colony per ml in summer. 3) Coliform groups are not detected in goods through a year. 4) There was no variation in number of total microbes after ion exchange resin passage in purification process of tap water. 5) The number of microbes in goods are decreased when the raw materials are treated in high temperature short time (HTST) sterilization.

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Studies on the Chemical composition of Zostera marina ("거머리 말"의 화학성분에 관한 연구)

  • 박명삼
    • Journal of Plant Biology
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    • v.12 no.1
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    • pp.1-6
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    • 1969
  • General components, free sugars, and free amino acids about Zostera marina which is much distributing and producing along the coastlines of Korea have been separated and identified through Ion exchange resin and Paper chromatography method. So distrigushed are sugars contained that this was quantitated by Bertrand method. 1) The result of the general component analysis of Zostera marina shows that there are much free sugars. 2) According to Bertrand method sugar containment quantitated from terrestrial stem and subterranean stem on Po-hang and Ko-hung areas is much more in terrestrial stem than subterranean stem. 3) Seven kinds of sugars are used in experiments(Table 2) among there glucose, fructose and sucrose which keep the sweetness are very much contained. 4) Shown in Fig. 3 ten kinds of free amino acids inspected from experimental liquid by Paper chromatography are separated, which are known, and one spot which in unknown is additionally separated, and in which four kinds of essential amino acid to nutrient are contained.

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Studies on the Utilization of Deodorized Condensates from Vegetable Oils (植物油 脫臭溜出物의 利用에 關한 硏究)

  • Kim, Jeom Sik
    • Journal of the Korean Chemical Society
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    • v.18 no.4
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    • pp.297-303
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    • 1974
  • An investigation has been performed to find an effective separation method of steriols and tocopherols from the deodorized condensates of vegetable oils. Simple heating of the starting mixture isolated the oil layer from water, and the former was collected. It was then methyl esterified followed by a distillation for the removal of fatty acid. The ensuing step was to saponify the residue. The unsaponifiable matter was extracted by both methanol and concentrated. The sterol was crystallized by cooling such concentrated solution. To obtain tocopherol, the mother liquor was first dissolved in methanol. Cooling this solution to $-20^{\circ}C$ trapped fatty acid which was filtered out. The filtrate was then treated with ion exchange resin.

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A Dtudy on the Effect of Polyamines of Korean Red Ginseng on the Growth of Cultured Chichen Embryonic Muscle Cells (홍삼 Polyamine 계 성분이 배양한 계배의 근육세포 성장에 미치는 영향)

  • 구향자;김영중
    • YAKHAK HOEJI
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    • v.31 no.5
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    • pp.296-301
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    • 1987
  • Polyamines of Korean red ginseng were extracted with 5% trichloroacetic acid and purified by ion exchange chromatography using Dowex-50Wx8 resin. Four spots having R$_f$ values of 0.19, 0.28, 0.35, and 0.45 were detected. It was observed under microscopy that those polyamines stimulated the growth and differentiation of chicken embryonic muscle cell. The development of muscle cells from the stage of myoblast to that of myotube was found to be enhanced by those polyamines. It was also observed that those polyamines most likely lengthened, the life-span of the cultured chicken embryonic skeletal muscle cells.

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