• 제목/요약/키워드: intergranular fracture

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複合組織鋼의 부식피로파괴에 미치는 3.5% NaCl水溶液의 pH와 母相粒徑의 效果 (Effect of pH in 3.5% NaCl aqueous solution and ferrite grain size on corrosion fatigue fracture of dual phase steel)

  • 오세욱;강호민
    • 대한기계학회논문집
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    • 제11권6호
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    • pp.867-876
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    • 1987
  • 본 연구에서는 보통강재인 SS 41 강을 열처리하여 얻은 M.E.F.복합조직강의 모상입경변화와 3.5% NaCl수용액의 pH변화 조건하에서 반복굽힘피로실험을 하여 부식 피로파괴에 미치는 영향에 대해 고찰하였다.

SPS법에 의한 SiC-$ZrB_2$ 복합체의 특성에 미치는 몰드의 영향 (Effects of Mold on Properties of SiC-$ZrB_2$ Composites through SPS)

  • 신용덕;이정훈;박진형;주진영;이희승
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2011년도 제42회 하계학술대회
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    • pp.1515-1516
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    • 2011
  • Conductive SiC-$ZrB_2$ composites were produced by subjection a 40:60(vol%) mixture of zirconium diborided ($ZrB_2$) powder and ${\beta}$-silicon carbide (SiC) matrix to spark plasma sintering (SPS) under argon atmosphere. Inner diameters of graphite mold were $15mm{\varphi}$ and $20mm{\varphi}$, respectively. The relative densities of $15mm{\varphi}$ and $20mm{\varphi}$ sample were 99.4% and 97.88%, respectively. Reactions between ${\beta}$-SiC and $ZrB_2$ were not observed via x-ray diffraction (hereafter, XRD) analysis. The result of FE-SEM of fracture face of $15mm{\varphi}$ sample was intergranular fracture and that of $20mm{\varphi}$ sample was transgranular fracture. Because the fracture strength of $15mm{\varphi}$ sample was much higher than that of $20mm{\varphi}$ sample. The electrical resistivity, $9.37{\times}10^{-4}{\Omega}{\cdot}cm$ of $15mm{\varphi}$ sample was higher than that, $6.17{\times}10^{-4}{\Omega}{\cdot}cm$ of $20mm{\varphi}$ sample because of densification. Although sintering condition of SPS is same. the properties of sintered SiC-$ZrB_2$ compacts were changed according to inner diameter of graphite mold.

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316LN 및 Cr-Mo 스테인리스강의 Monkman-Grant 파라메타 평가 (Estimation of Monkman-Grant Parameter for Type 316LN and Cr-Mo Stainless Steels)

  • 김우곤;김성호;이경용;류우석
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2001년도 춘계학술대회논문집A
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    • pp.223-230
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    • 2001
  • The Monkman-Grant (M-G) and its modified parameters were estimated for modified type 316LN and $9{\sim}12Cr-1Mo$ steels with chemical variations. Several sets of creep data were obtained by constant-load creep tests in $550-650^{\circ}C$ ranges. The relation parameters, m, $m^*$, C and $C^*$ were proposed and discussed for two alloy systems. In creep fracture mode, type 316LN steel showed domination of the intergranular fracture caused by growth and coalescence of cavities. On the other hand, the Cr-Mo steel showed transgranular fracture of the ductile type caused from softening at high temperature. In spite of the basic differences in creep fracture modes as well as creep properties, the M-G and its modified relations demonstrated linearity within the $2{\sigma}$ standard deviation. The value of the m parameter of the M-G relation was 0.90 in the 316LN steel and 0.84 in the Cr-Mo steel. The value of the $m^*$ parameter of the modified relation was 0.94 in the 316LN steel and 0.89 in Cr-Mo steel. The modified relation was superior to the M-G relation because the $m^*$ slopes almost overlapped regardless of creep testing conditions and chemical variations to the two alloy systems.

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고온부재의 재질열화에 따른 응력부식균열 평가에 관한 연구 (A Study on Stress Corrosion Cracking Evaluation with Material Degradation of High Temperature Components)

  • 박종진;유호선;정세희
    • 대한기계학회논문집A
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    • 제20권4호
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    • pp.1123-1132
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    • 1996
  • It has been reported that high temperature structural components represent the phenomenon of material degradation according to a long term service under high temperature and pressure. Especially, fossile power plant components using the fossil fuel and heavy oil are affected by dewpoint corrosion of $H_2SO_4$produced during a combustion. Therefore, the service materials subjected to high temperature and pressure may occur the stress corrosion cracking. The object of this paper is to investigate SCC susceptibility according to the material degradation of the high temperature structural materials in dewpoint corrosive environment-$H_2SO_4$.The obtained results are summarized as follows : 1) In case of secondary superheater tube, the fractograph of dimple is observed at the concentration of $H_2SO_4$-5%. When the concentration of $H_2SO_4$ is above 10%, the fracture mode is shifted from a transgranular fracture to an quasi-intergranular fracture according to the increment of concentration. 2) In the relationship between [$\Delta$DBTT]$_sp$ and SCC susceptibility, it is confirmed that the greater material degradation degree is, the higher SCC susceptibility is. In addition, it can be known that SP test is useful test method to evaluate SCC susceptibility for high temperature structural components. 3) When [$\Delta$DBTT]$_sp$ is above 17$17^{\circ}C$ the SCC fracture behavior is definitely observed with SCC susceptibility of above 0.4.

알루미늄 합금의 피로강도향상과 피로특성에 미치는 쇼트피닝 영향 (The Effect of Shot Peening on the Improvement of Fatigue Strength and Characteristics Fatigue Crack of the Aluminum Alloys)

  • 전현배;임만배;박원조
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2007년도 춘계학술대회A
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    • pp.256-261
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    • 2007
  • The purpose of this study is to investigate the effect of shot peening on the fatigue strength and fatigue life of two kinds of aluminum alloys. The fatigue strength behavior of aluminum alloys were estimated by the stress ratio and shot velocities. The fatigue life and strength increased with increasing the test shot velocity. However, at the shot velocity range between 50m/s and 70m/s, the compressive residual stress phenomena were observed in test conditions of different shot velocity. The optimal shot velocity is acquired by considering the peak values of the compressive residual stress, dislocations, brittle striation, slip, and fisheye on the fracture surface of test specimen. It was observed from the SEM observation on the deformed specimen that the brittle striation, fisheye were showed in the intergranular fracture structure boundaries at the this velocities. Therefore, fatigue strength and fatigue life would be considered that shot velocity has close relationship with the compressive residual stress.

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질화규소 세라믹의 레이저 예열선삭에 관한 연구 (IV) - 질화규소 세라믹의 레이저예열선삭 메커니즘 및 적용 - (A Study on Laser Assisted Machining for Silicon Nitride Ceramics (IV) - Mechanism and Application of LAM for Silicon Nitride Ceramics -)

  • 김종도;이수진;박서정;이제훈
    • Journal of Welding and Joining
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    • 제28권6호
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    • pp.40-44
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    • 2010
  • Laser assisted machining (LAM) has been researched in order to machine the silicon nitride ceramics economically and effectively. LAM is an effective machining method by local heating of the cutting part to the softening temperature of the silicon nitride using laser beam. When silicon nitride ceramics is heated using a laser beam, the surface of silicon nitride ceramic is softened, oxidized and decomposed. And then surface hardness is decreased. Through machining in low viscosity and hardness conditions, silicon nitride was machined effectively and the life span of tool was increased. The plastic deformation was occurred due to softening of amorphous YSiAlON above $ 1,000^{\circ}C$. Transgranular fracture of ${\beta}-Si_3N_4$ was occurred when YSiAlON was not softened, but mostly intergranular fracture was occurred by the plastic deformation of softened YSiAlON.

자동차 에어 브레이크 스프링 고정용 SCM435 볼트의 파손 해석 (Failure Analysis of SCM435 Bolt for Fixing Automotive Air Brake Spring)

  • 윤서현;김민헌;남기우
    • 한국산업융합학회 논문집
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    • 제23권1호
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    • pp.73-81
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    • 2020
  • This study analyzed the causes of failure of SCM435 bolts that fix the springs of automobile air brakes that have been fractured during use. The cause of failure was analyzed using SEM, EDS, metallogical microscope and Vickers hardness tester. In the fracture, the ratchet mark began at the outer boundary of crack origin, and the grains at crack origin were found to have clear intergranular corrosion. One SCM435 bolt was subjected to a stress of 398 MPa, it's a stress of about 80% of the fatigue limit. As a result of such a large applied stress, cracks occurred at the corrosion origin and were fractured. In order to prevent the SCM435 bolt from fracture, it is necessary to use the correct composition, the accuracy of heat treatment, preventing damage by external impact, preventing corrosion of the damage part by moisture, and introduction a compressive residual stress by peening.

Cr - Mo鋼 熔接 後熱處理材 의 勞破壞 에 關한 硏究

  • 박재규;김석원;김연식
    • Journal of Welding and Joining
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    • 제3권2호
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    • pp.16-26
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    • 1985
  • Post weld heat treatment(PWHT), at more than 600.deg. C, is essential to remove residual stress and hydrogen in weld HAZ and improve fatigue characteristics. However, residual stress during PWHT is responsible for PWHT embitterment and it promotes precipitation of impurities to grain boundary. In this paper, the effect of stress simulated residual stress on fatigue failure was evaluated by fatigue test, microhardness test and fractograph. The obtained results are summarized as follows; (1) The fatigue crack growth rate(da/dN) of parent and heat treated parent was affected by microstructure due to heat treatment and it depended on stress intensity factor (.DELTA.k). (2) The fatigue strength of weld HAZ was dependent on applied stress during PWHT and da/dN after PWHT was slower than as-weld. (3) Softening amount of weld HAZ was bigger than any other due to PWHT. Hardness value of weld HAZ was affected by heat treatment under the applied stress of 10 $kgf/mm^2$, but beyond 20 $kgf/mm^2$ it was increased by the applied stress rather than heat treatment. (4) Beyond the applied stress of 20 $kgf/mm^2$ during PWHT, intergranular fracture surface was observed and its amount was increased with applied stress during PWHT. (5) Effect of applied stress during PWHT on aspect of fracture surface was larger rather than that on fatigue crack growth behavior.

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Zirconium계 합금의 Creep특성 (The Creep Characteristics of Zirconium-base Alloy)

  • 임성혁;임종국;김경환;최재하
    • 열처리공학회지
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    • 제10권3호
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    • pp.198-208
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    • 1997
  • The-steady-state creep mechanism and behavior of Zircaloy-4 used as cladding materials in PWR have been investigated in air environment over the temp, ranges from 600 to $645^{\circ}C$ and stress ranges from 4 to $7kg/mm^2$. The stress exponents for the creep deformation of this alloy, n were decreased 4.81, 4.71, 4.64, and 4.56 at 600, 615, 630 and $645^{\circ}C$, respectively; the stress exponents decreased with increasing the temperature and got closer to about 5. The apparent activation energies, Q, were 62.1, 60.0, 57.9 and 55.4 kcal/mole at stresses of 4, 5, 6, $7kg/mm^2$, respectively; the activation energies decreased with increasing the stress and were close to those of volume self diffusion of Zr in Zr-Sn-Fe-Cr system. In results, it can be considered that the creep deformation for Zircaloy-4 was controlled by the dislocation climb over the ranges of this experimental conditions. Larson-Miller parameter, P, for the crept specimens was obtained as P=(T+460)(logt,+23). The failure plane observed by SEM slightly showed up intergranular fracture at this experiment ranges. However, it was essentially dominated by the dimple phenomenon, which was a characteristics of the transgranular fracture.

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마찰교반용접된 7075-T651 알루미늄 판재의 피로균열전파의 거시적 및 미시적 관찰 (Marco and Microscopic Observations of Fatigue Crack Growth in Friction Stir Welded 7075-T651 Aluminum Alloy Plates)

  • 공유식;김선진
    • 동력기계공학회지
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    • 제18권2호
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    • pp.62-69
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    • 2014
  • In this paper, in order to investigate the effects of marco and microscopic observations of fatigue crack growth in friction stir welded (FSWed) 7075-T651 aluminum alloy plates, fatigue crack growth tests were performed under constant amplitude loading condition at room temperature with three different pre-cack locations, namely base metal (BM-CL) and two kinds of pre-crack locations in welded joints, weld metal (WM-CL) and heat affected zone (HAZ-CL) specimens. The fatigue crack growth behavior of FSWed 7075-T651 aluminum alloy plates were discussed based on the marco and microscopic fractographic observations. The marcoscopic aspects of surface crack growth path for BM-CL and HAZ-CL specimens indicate relatively straight lines, however, the crack growth paths of WM-CL specimens grow first straight and by followed toward the TMAZ and HAZ. The microscopic aspects of fatigue fracture for BM-CL and HAZ-CL specimens indicate typical fatigue striation, but WM-CL showed intergranular fracture pattern by micro structural changes of FSW process.