• Title/Summary/Keyword: interfacial evaluation

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Interfacial Evaluation of Modified Jute and Hemp Fibers/Polypropylene (PP)-Maleic Anhydride Polypropylene Copolymers (PP-MAPP) Composites Using Micromechanical Test and Nondestructive Acoustic Emission (Micromechanical 시험법과 음향방출을 이용한 Flax 와 Hemp 섬유 강화 에폭시 복합재료의 계명 물성 평가)

  • Son, Tran Quang;Hwang, Byung-Sun;Park, Joung-Man
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2005.11a
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    • pp.157-160
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    • 2005
  • The surface energies and acid-base interaction between the untreated and treated Jute or Hemp fibers and different matrix compositions of polypropylene-maleic anhydride polypropylene copolymers (PP-MAPP) were investigated using dynamic contact angle measurement. The contribution of the acid-base property into the interfacial adhesion of the natural fibers/matrix systems were characterized by calculating the work adhesion coming from the acid-base interaction. On the other hand, microfailure mechanism of both single Jute and Hemp fiber bundles were investigated using the combination of single fiber tensile test and acoustic emission. Distinctly different micro failure modes of the different natural fiber/polypropylene systems wet ε observed using optical microscope and determined indirectly by AE and their FFT analysis.

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Evaluation of interfacial tension for poly(methyl methacrylate) and polystyrene by rheological measurements and interaction parameter of the two polymers

  • Sung, Y.T.;Seo, W.J.;Kim, Y.H.;Lee, H.S.;Kim, W.N.
    • Korea-Australia Rheology Journal
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    • v.16 no.3
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    • pp.135-140
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    • 2004
  • Morphological and rheological properties of the poly(methyl methacrylate) (PMMA) and polystyrene (PS) blends were studied by scanning electron microscopy (SEM) and advanced rheometric expansion system (ARES). From the SEM results, the PMMA-PS blends showed dispersed morphology and the particle size of the dispersed phase was quite small (0.1~0.6 $\mu\textrm{m}$ compared with other immiscible polymer blends. Values of the interfacial tension of the PMMA-PS blend were obtained from the Choi-Schowalter and the Palierne emulsion models using the storage modulus of the PMMA and PS, and found to be 1.0 and 2.0 mN/m, respectively. The interfacial tension between the PMMA and PS was also calculated from the Flory-Huggins polymer-polymer interaction parameter ($\chi$) and found to be from 0.98 to 1.86 mN/m depending on the molecular weight and composition. Comparing the values of the interfacial tension from the Flory-Huggins polymer-polymer interaction parameter and the values measured by oscillatory rheometer, it is suggested that the interfacial tension of the PMMA-PS blend obtained from the polymer-polymer interaction parameter are in good agreement with the values obtained by rheological measurements.

A Study on the Near-Field Stresses and Displacement of a Stationary Interfacial Crack in Two Dissimilar Isotropic Bimaterials (두 상이한 등방성 이종재료 정지계면균열의 선단 응력장과 변위장에 관한 연구)

  • Shin, Dong-Chul;Hawong, Jai-Sug;Nam, Jeong-Hwan
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.28 no.12
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    • pp.1897-1905
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    • 2004
  • In many part of machines or structures that made of bimaterial bonded with two dissimilar materials, most failures occur at their interface. Therefore, the accurate analysis of fracture characteristics and the evaluation of mechanical strength for interfacial crack are essential when we design those structures. In this research, stress and displacement components in the vicinity of stationary interfacial crack tip in the two dissimilar isotropic bimaterials are established. Hereafter, the stress components established in this research can be applied to the photoelastic hybrid method which can be used to analyze the fracture behavior of the two dissimilar isotropic bimaterials.

Study on the Evaluation for the Property of Mo-Si Multilayers (Mo/Si 다층박막의 특성 평가에 관한 연구)

  • 허성민;김형준;이동현;이승윤;이영태
    • Journal of the Microelectronics and Packaging Society
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    • v.8 no.2
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    • pp.15-18
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    • 2001
  • The Mo/si multilayer for EUV lithography was deposited using magnetron sputtering system. The multilayers were characterized using the cross-sectional transmission electron microscope (TEM) and low/high angle X-ray diffraction (XRD). The microstructure of Mo and Si was highly textured structure and amorphous, respectively. The well-defined low angle XRD peaks implies a well-defined multilayer structure. The interfacial layer of Mo-on-Si was thicker than Si-on-Mo interfacial layer.

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VOID FRACTION PREDICTION FOR SEPARATED FLOWS IN THE NEARLY HORIZONTAL TUBES

  • AHN, TAE-HWAN;YUN, BYONG-JO;JEONG, JAE-JUN
    • Nuclear Engineering and Technology
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    • v.47 no.6
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    • pp.669-677
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    • 2015
  • A mechanistic model for void fraction prediction with improved interfacial friction factor in nearly horizontal tubes has been proposed in connection with the development of a condensation model package for the passive auxiliary feedwater system of the Korean Advanced Power Reactor Plus. The model is based on two-phase momentum balance equations to cover various types of fluids, flow conditions, and inclination angles of the flow channel in a separated flow. The void fraction is calculated without any discontinuity at flow regime transitions by considering continuous changes of the interfacial geometric characteristics and interfacial friction factors across three typical separated flows, namely stratified-smooth, stratified-wavy, and annular flows. An evaluation of the proposed model against available experimental data covering various types of fluids and flow regimes showed a satisfactory agreement.

Historical Trends of Micromechanical Testing Methods for Structural Fiber Reinforced Composites to Evaluate the Interfacial Adhesion (구조용 섬유강화복합재료의 계면접착 특성 평가를 위한 미세역학시험법의 연구동향 고찰)

  • Park, Joung-Man;Kim, Jong-Hyun;Kim, Dong-Uk;Kwon, Dong-Jun
    • Journal of Adhesion and Interface
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    • v.23 no.3
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    • pp.59-69
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    • 2022
  • In composite materials, the adhesion and interfacial properties were the most important factors to obtain high performance of mechanical properties. This review paper had been focused on the micromechanical evaluation methods for the interfacial property historically. The interfacial property of fiber-reinforced composites (FRC) could be evaluated using only a single fiber and matrix via various micromechanical testing methods. Self-sensing due to the fracture behavior of FRC could be determined and discussed more critically and clearly using electro-micromechanical evaluation. In this paper, the research trends for micro-mechanical evaluation of composites was summarized, and their practical applications would be suggested in the future.

Interfacial Damage Sensing and Evaluation of Carbon and SiC Fibers/Epoxy Composites with Fiber-Embedded Angle using Electro-Micromechanical Technique (Electro-Micromechanical시험법을 이용한 섬유 함침 각에 따른 탄소와 SiC 섬유강화 에폭시 복합재료의 계면 손상 감지능 및 평가)

  • Joung-Man Park;Sang-Il Lee;Jin-Woo Kong;Tae-Wook Kim
    • Composites Research
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    • v.16 no.2
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    • pp.68-73
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    • 2003
  • Interfacial properties and electrical sensing fer fiber fracture in carbon and SiC fibers/epoxy composites were investigated by the electrical resistance measurement and fragmentation test. As fiber-embedded angle increased, the interfacial shear strength (IFSS) of two-type fiber composites decreased, and the elapsed time takes long until the infinity in electrical resistivity. The initial slope of electrical resistivity increased rapidly to the infinity at higher angle, whereas electrical resistivity increased gradually at small angle. Furthermore, both fiber composites with small embedded angle showed a fully-developed stress whitening pattern, whereas both composites with higher embedded angle exhibited a less developed stress whitening pattern. As embedded angle decreased, the gap between the fragments increased and the debonded length was wider for both fiber composites. Electro-micromechanical technique could be a feasible nondestructive evaluation to measure interfacial sensing properties depending on the fiber-embedded angle in conductive fiber reinforced composites.

Interfacial and Nondestructive Evaluation of Single Carbon Fiber/Epoxy Composites by Fiber Fracture Source Location using Acoustic Emission (Acoustic Emission 의 섬유파단 Source Location을 이용한 Carbon Fiber/Epoxy Composites의 계면특성 및 비파괴적 평가)

  • Kong, Jin-Woo;Kim, Jin-Won;Park, Joung-Man;Yoon, Dong-Jin
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2001.10a
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    • pp.116-120
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    • 2001
  • Fiber fracture is one of the dominant failure phenomena to determine total mechanical properties in composites. Fiber fracture locations were measured by optical microscopic method and acoustic emission (AE) as functions of matrix toughness and surface treatment by the electrodeposition (ED), and then two methods were compared. Two AE sensors were attached on the epoxy specimen and fiber fracture signals were detected with elapsed time. The interfacial shear stress (IFSS) was measured using tensile fragmentation test and AE system. In ED-treated case, the number of the fiber fracture measured by an optical method and AE was more than that of the untreated case. The signal number measured by AE were rather smaller than the number of fragments measured by optical method, since some fiber fracture signals were lost while AE detection. However, one-to-one correspondence between the x-position location by AE and real break positions by optical method was generally established well. The fiber break source location using AE can be a valuable method to measure IFSS for semi- or nontransparent matrix composites nondestructively (NDT).

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Interfacial Evaluation and Microfailure Mechanisms of Carbon Fiber/Bismaleimide (BMI) Composites using Tensile/compressive Fragmentation Tests and Acoustic Emission (인장/압축 Fragmentation 시험법과 음향방출을 이용한 Carbon Fiber/Bismaleimide (BMI) Composites 의 계면 평가와 미세파괴 메커니즘 연구)

  • 김진원;박종만;윤동진
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2000.11a
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    • pp.79-83
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    • 2000
  • Interfacial and microfailure properties of carbon liber/bismaleimide (BMI) composites were evaluated using both tensile fragmentation and compressive Broutman tests with acoustic emission (AE). Since BMI is rather difficult matrix to apply for the conventional fragmentation test because of its too low elongation and too brittle and high modulus properties, dual matrix composite system was applied. After carbon fiber/BMI composite was prepared for rod shape by controlling differing curing stage, composites rod was embedded in toughened epoxy as outer matrix. The typical microfailure modes including fiber break, matrix cracking, and interlayer failure were observed during tensile testing, whereas the diagonal slippage in fiber ends was observed during compressive test. On the other hand, AE amplitudes of BMI matrix fracture were higher than carbon fiber tincture under tensile test because BMI matrix has very brittle and high modulus. The waveform of signals coming from BMI matrix fractures was consistent with AE amplitude result under tensile tests.

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Micremechanics-based Evaluation of Elastic Modulus of Concrete considering Interfacial Transition Zone (천이영역을 고려한 콘크리트 탄성계수의 미시역학적 추정)

  • 송하원;조호진;변근주
    • Magazine of the Korea Concrete Institute
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    • v.10 no.2
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    • pp.99-107
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    • 1998
  • 콘크리트는 일반적으로 수회시멘트풀과 골재로 이루어진 이상의 복합체이지만 미시적으로는 수화시멘트풀과 골재, 그리고 천이영역으로 이루어진 삼상의 복합체이다. 수화시멘트풀과 골재 사이에서 형성되는 천이영역은 국부적으로 공극률이 높으므로 콘크리트의 강성과 강도에 많은 영향을 끼친다. 본 논문에서는 이러한 천이영역의 특성을 고려하여 콘크리트의 탄성계수를 추정하기 위해 이원 삼중 내포물 모델을 제안하였다. 제안된 모델에 의한 탄성계수의 추정결과는 실험결과와 비교하여 잘 일치하였으며 제안된 모델은 실험적으로 구하기 힘든 천이영역의 특성을 구하는데 사용될 수 있다.