• Title/Summary/Keyword: interfacial analysis

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Effect of Natural Jute Fiber on Bond between Polyolefin Based Macro Fiber and Cement Matrix (폴리올레핀계 매크로 섬유와 시멘트 경화체의 부착특성에 미치는 천연마섬유의 효과)

  • Lee, Jin-Hyung;Park, Chan-Gi
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.31 no.3A
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    • pp.251-260
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    • 2011
  • In this study, the effect of natural jute fiber volume fraction on the bond characteristics of polyolefin based macro fiber in natural jute fiber reinforced cement composites, including bond strength, interface toughness, and microstructure analysis are presented. The experimental results on polyolefin based macro fiber pullout test of different conditions are reported. Natural jute fiber volume fractions ranging from 0.1% to 0.2% are used in the mix proportions. Pullout tests are conducted to measure the bond characteristics of polyolefin based macro fiber from natural jute fiber reinforced cement composites. Test results are found that the incorporation of natural jute fiber can effectively enhance the polyolefin based macro fiber-cement matrix interfacial properties. The bond strength and interface toughness between polyolefin based macro fiber and natural jute fiber reinforced cement composites increases with the volume fraction of natural jute fiber. The microstructural observation confirms the findings on the interface bond mechanism drawn from the fiber pullout test results.

A Numerical Analysis of the Binary Droplet Collision by Using a Level Set Method (레벨셋 방법을 이용한 액적 충돌에 대한 수치해석)

  • Lee, Sang-Hyuk;Hur, Nahm-Keon
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.35 no.4
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    • pp.353-360
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    • 2011
  • The prediction of binary droplet collisions is important in the formation of falling drops and the evolution of sprays. The droplet velocity, impact parameter, and drop-size ratio influence the interaction between the droplets. The effect of these parameters results in complicated collision phenomena. Droplet collisions can be classified into four types of interactions: bouncing, coalescence, reflexive separation, and stretching separation. In the present study, the interfacial flow problem of the droplet collision was numerically simulated by using the level set method. 2D axisymmetric simulations on the head-on collisions and 3D simulation on the off-center collisions were performed. The numerical results of droplet behavior after the collision agreed well with the experimental and analytical results. The mixing of the mass of the initial droplets after the collision was also predicted by using different species index of colliding droplets.

A Study on the Detection of Interfacial Defect to Boundary Surface in Semiconductor Package by Ultrasonic Signal Processing (초음파 신호처리에 의한 반도체 패키지의 접합경계면 결함 검출에 관한 연구)

  • Kim, Jae-Yeol;Hong, Won;Han, Jae-Ho
    • Journal of the Korean Society for Nondestructive Testing
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    • v.19 no.5
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    • pp.369-377
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    • 1999
  • Recently, it is gradually raised necessity that thickness of thin film is measured accuracy and managed in industrial circles and medical world. Ultrasonic signal processing method is likely to become a very powerful method for NDE method of detection of microdefects and thickness measurement of thin film below the limit of ultrasonic distance resolution in the opaque materials, provides useful information that cannot be obtained by a conventional measuring system. In the present research. considering a thin film below the limit of ultrasonic distance resolution sandwiched between three substances as acoustical analysis model, demonstrated the usefulness of ultrasonic signal processing technique using information of ultrasonic frequency for NDE of measurements of thin film thickness. Accordingly, for the detection of delamination between the junction condition of boundary microdefect of thin film sandwiched between three substances the results from digital image processing.

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Influence of the Chemical Treatment of Bamboo Fiber (BF) on Physical Properties of BF and PP/BF Composites (대나무 섬유(BF) 및 PP/BF 복합체의 물성에 미치는 BF의 화학적 처리의 영향)

  • Lee, Beom Hee;Jeong, Da Sol;Kim, Cheol Woo;Park, Seong Ho;Kim, Youn Cheol
    • Applied Chemistry for Engineering
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    • v.29 no.2
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    • pp.168-175
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    • 2018
  • In order to investigate the effect of the chemical treatment of bamboo fiber on physical properties of polypropylene (PP)/bamboo fiber (BF) composites, silane coupling agents such as ${\gamma}$-aminopropyltriethoxysilane (APS), ${\gamma}$-glycidoxypropyl-trimethoxysilane (GPS) and ${\gamma}$-mercaptopropyltrimethoxysilane (MRPS) were applied to BF and alkaline treated BF. Morphological properties of the chemically treated BF were confirmed by optical microscope and SEM measurements, and chemical structure changes were confirmed by FT-IR and EDS. TGA results showed that the thermal stability of silane treated BF increased. Based on the analysis of a universal testing machine and an Izod impact test, the flexural and impact properties of PP/silane treated BF composites showed higher values than those of PP/BF composites. The enhancement of interfacial adhesion properties of the PP/BF composite was checked from SEM images of the fracture of specimens after the tensile test.

Analysis of Reflectivity for Interfacial Roughness of Depth-Graded W/Si Multilayer Mirror (두께 변화 W/Si 다층박막거울의 계면 거칠기에 대한 반사율 분석)

  • Chon, Kwon Su
    • Journal of the Korean Society of Radiology
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    • v.12 no.1
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    • pp.101-106
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    • 2018
  • Multilayer mirrors have widely been used for monochromatization of X-ray with high reflection efficiency. The reflected X-ray energy or wavelength is determined by the d-spacing of a multilayer mirror and the incidence angle. The reflectivity critically depends on the number of bilayers and surface roughness on each interface. The multilayer mirror has a structure of alternative deposition of high and low Z-elements on the substrate. Each interface should be considered in the calculation of reflectivity. In this paper, we examine the degradation of reflectivity by the inter-diffusion combined with surface roughness on each interface for a W/Si multilayer mirror. In the depth-graded W/Si multilayer mirror, the FWHMs for angle and energy were larger than them of the uniform multilayer mirror. Inter-diffusion considerable gave rise to the degradation of reflectivity. To obtain measured reflectivity closed to the expected reflectivity, the inter-diffusion on W-Si and Si-W interfaces should be considered.

A Study on the Interlaminar Fracture Toughness of Hybrid Composites (하이브리드 복합재료의 층간파괴인성치에 관한 연구)

  • Kim, Hyung-Jin;Gwark, Dae-Won;Lee, Hern-Sik;Kim, Jae-Dong;Koh, Sung-Wi
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.40 no.4
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    • pp.328-336
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    • 2004
  • This paper describes the effect of loading rate, specimen geometries and material properties for ModeⅠ and Mode Ⅱ interlaminar fracture toughness of hybrid composite by using double cantilever beam (DCB) and end notched flexure (ENF) specimen. In the range of loading rate 0.2~20mm/min, there is found to be no significant effect of loading rate with the value of critical energy release rate (Gc).The value of Gc for variation of initial crack length are nearly similar values when material properties are CF/CF and GF/GF, however, the value of Gc are highest with the increasing intial crack length at CF/GF. The SEM photographs show good fiber distribution and interfacial bonding of hybrid composites when the moulding is the CF/GF.

Electrochemical Performance of the Solid Oxide Fuel Cell with Different Thicknesses of BSCF-based Cathode (BSCF계 혼합전도성 공기극의 두께에 따른 고체산화물 연료전지의 전기화학적 특성)

  • Jeong, Jaewon;Yoo, Chung-Yul;Joo, Jong Hoon;Yu, Ji Haeng
    • Transactions of the Korean hydrogen and new energy society
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    • v.24 no.2
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    • pp.186-192
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    • 2013
  • In order to reduce the costs and to improve the durability of solid oxide fuel cell (SOFC), the operating temperature should be decreased while the power density is maintained as much as possible. However, lowering the operating temperature increases the cathode interfacial polarization resistances dramatically, limiting the performance of low-temperature SOFC at especially purely electronic conducting cathode. To improve cathode performance at low temperature, the number of reaction sites for the oxygen reduction should be increased by using a mixed ionic and electronic conducting (MIEC) material. In this study, anode-supported fuel cells with two different thicknesses of the MIEC cathode were fabricated and tested at various operating temperatures. The anode supported cell with $32.5{\mu}m$-thick BSCFZn-LSCF cathode layer showed much lower polarization resistance than that with $3.2{\mu}m$ thick cahtode and higher power density especially at low temperature. The effects of cathode layer thickness on the electrochemical performance are discussed with analysis of impedance spectra.

Development of Hybrid Fiber-reinforced High Strength Lightweight Cementitious Composite (하이브리드 섬유로 보강한 고강도 경량 시멘트 복합체의 개발)

  • Bang, Jin-Wook;Kim, Jung-Su;Lee, Bang-Yeon;Jang, Young-Il;Kim, Yun-Yong
    • Composites Research
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    • v.23 no.4
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    • pp.35-43
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    • 2010
  • The purpose of this paper is to develop a Hybrid Fiber-reinforced High Strength Lightweight Cementitious Composite (HFSLCC) incorporated with lightweight filler and hybrid fibers for lightness and high ductility. Optimal ingredients and mixture proportion were determined on the basis of the micromechanical analysis and the steady-state cracking theory considering the fracture characteristics of matrix and the interfacial properties between fibers and matrix. Then 4 mixture proportions were determined according to the type and amount of fibers and the experiment was performed to evaluate the mechanical performance of those. The HFSLCC showed 3% of tensile strain, 4.2MPa of ultimate tensile stress, 57MPa of compressive strength and $1,660kg/m^3$ of bulk density. The mechanical performance of HFSLCC incorporated with PVA fibers of 1.0 Vol.% and PE fibers of 0.5 Vol.% is similar to those of the HFSLCC incorporated with fibers of 2.0 Vol.%.

Thixoforming Characteristics of Metal Matrix Composites (Phase identification of $SiC_p/AZ91HP$ Mg composite) (금속기 복합재료의 틱소포밍 특성 ($SiC_p/AZ91HP$ Mg 복합재료의 상분석을 중심으로))

  • Lee, Jung-Il;Kim, Young-Jig
    • Applied Microscopy
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    • v.29 no.3
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    • pp.281-289
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    • 1999
  • The stirred and thixoformed $SiC_p/AZ91HP$ Mg composites are studied on the basis of microstructural analysis using transmission electron microscopy (TEM). The products of interfacial reaction are identified as $Mg_2Si$, MgO and $Mg_{17}Al_{12}$ phases and the crystallized phases are found to be orthorhmbic $Al_6Mn$ and decagonal T phases. It is shown that $Mg_2Si$ and $Mg_{17}Al_{12}$ phases are found at the surface of $SiC_p$ and $Al_6Mn$ is found near interface and crystallized on the matrix. Phase identification is carried out by crystallographic work based on primitive cell volume, zero order Laue zone (ZOLZ) patterns and single convergent beam electron diffraction (CBED) patterns containing higher order Laue zone ring from a nanosized region.

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Tensile strength of bilayered ceramics and corresponding glass veneers

  • Anunmana, Chuchai;Champirat, Tharee;Jirajariyavej, Bundhit
    • The Journal of Advanced Prosthodontics
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    • v.6 no.3
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    • pp.151-156
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    • 2014
  • PURPOSE. To investigate the microtensile bond strength between two all-ceramic systems; lithium disilicate glass ceramic and zirconia core ceramics bonded with their corresponding glass veneers. MATERIALS AND METHODS. Blocks of core ceramics (IPS e.max$^{(R)}$ Press and Lava$^{TM}$ Frame) were fabricated and veneered with their corresponding glass veneers. The bilayered blocks were cut into microbars; 8 mm in length and $1mm^2$ in cross-sectional area (n = 30/group). Additionally, monolithic microbars of these two veneers (IPS e.max$^{(R)}$ Ceram and LavaTM Ceram; n = 30/group) were also prepared. The obtained microbars were tested in tension until fracture, and the fracture surfaces of the microbars were examined with fluorescent black light and scanning electron microscope (SEM) to identify the mode of failure. One-way ANOVA and the Dunnett's T3 test were performed to determine significant differences of the mean microtensile bond strength at a significance level of 0.05. RESULTS. The mean microtensile bond strength of IPS e.max$^{(R)}$ Press/IPS e.max$^{(R)}$ Ceram ($43.40{\pm}5.51$ MPa) was significantly greater than that of Lava$^{TM}$ Frame/Lava$^{TM}$ Ceram ($31.71{\pm}7.03$ MPa)(P<.001). Fluorescent black light and SEM analysis showed that most of the tested microbars failed cohesively in the veneer layer. Furthermore, the bond strength of Lava$^{TM}$ Frame/Lava$^{TM}$ Ceram was comparable to the tensile strength of monolithic glass veneer of Lava$^{TM}$ Ceram, while the bond strength of bilayered IPS e.max$^{(R)}$ Press/IPS e.max$^{(R)}$ Ceram was significantly greater than tensile strength of monolithic IPS e.max$^{(R)}$ Ceram. CONCLUSION. Because fracture site occurred mostly in the glass veneer and most failures were away from the interfacial zone, microtensile bond test may not be a suitable test for bonding integrity. Fracture mechanics approach such as fracture toughness of the interface may be more appropriate to represent the bonding quality between two materials.