• Title/Summary/Keyword: interfacial analysis

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Comparison of the shear bond strength of self-etching dentin bonding agents to dentin (자가부식형 상아질 접착제와 상아질과의 전단결합강도 비교)

  • Noh, Su-Jeong;Kim, Bu-Sub;Chung, In-Sung
    • Journal of Technologic Dentistry
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    • v.29 no.2
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    • pp.141-150
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    • 2007
  • The purpose of this study was to ascertain the bonding durability of self-etching dentin bonding agents to dentin by means of shear bonding strength. Several acid-etching dentin bonding system (ESPE Z100) and self-etching dentin bonding systems (DEN-FIL, GRADIA DIRET) were used. The occlusion surface of human molars were ground flat to expose dentin and treated with the etch bonding system according to manufactures instruction and followed by composite resin application. After 24hours of storage at 37$^{\circ}C$, the shear bonding strength of the specimens was measured in a universal testing machine with a 1mm/min crosshead speed. An one-way analysis of variance and the scheffe test were performed to identify significant differences (p<0.05). The bonded interfacial surfaces and treated dentin surfaces were examined using a SEM. Through the analysis of shear bond strength data and micro-structures of dentin-resin interfaces, following results are obtained. In dentin group, the shear bond strength of DEN-FIL showed statistical superiority in comparison to the other groups and followed by ESPE Z100 and GRADIA DIRECT (p<0.05).

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A Study on Data Classification of Raman OIM Hyperspectral Bone Data

  • Jung, Sung-Hwan
    • Journal of Korea Multimedia Society
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    • v.14 no.8
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    • pp.1010-1019
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    • 2011
  • This was a preliminary research for the goal of understanding between internal structure of Osteogenesis Imperfecta Murine (OIM) bone and its fragility. 54 hyperspectral bone data sets were captured by using JASCO 2000 Raman spectrometer at UMKC-CRISP (University of Missouri-Kansas City Center for Research on Interfacial Structure and Properties). Each data set consists of 1,091 data points from 9 OIM bones. The original captured hyperspectral data sets were noisy and base-lined ones. We removed the noise and corrected the base-lined data for the final efficient classification. High dimensional Raman hyperspectral data on OIM bones was reduced by Principal Components Analysis (PCA) and Linear Discriminant Analysis (LDA) and efficiently classified for the first time. We confirmed OIM bones could be classified such as strong, middle and weak one by using the coefficients of their PCA or LDA. Through experiment, we investigated the efficiency of classification on the reduced OIM bone data by the Bayesian classifier and K -Nearest Neighbor (K-NN) classifier. As the experimental result, the case of LDA reduction showed higher classification performance than that of PCA reduction in the two classifiers. K-NN classifier represented better classification rate, compared with Bayesian classifier. The classification performance of K-NN was about 92.6% in case of LDA.

DEVELOPMENT OF GENERAL PURPOSE THERMO/FLUID FLOW ANALYSIS PROGRAM NUFLEX (범용 열/유체 유동해석 프로그램 NUFLEX의 개발)

  • Hur, Nahm-Keon;Won, Chan-Shik;Ryou, Hong-Sun;Son, Gi-Hun;Kim, Sa-Ryang
    • 한국전산유체공학회:학술대회논문집
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    • 2007.04a
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    • pp.87-90
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    • 2007
  • A general purpose program NUFLEX for the analysis 3-D thermo/fluid flow and pre/post processor in complex geometry has been developed, which consists of a flow solver based on FVM and GUI based pre/post processor. The solver employs a general non-orthogonal grid system with structured grid and solves laminar and turbulent flows with standard/RNG ${\kappa}-{\varepsilon}\;SST$ turbulence model. In addition, NUFLEX is incorporated with various physical models, such as interfacial tracking, cavitation, MHD, melting/solidification and spray model. For the purpose of verification of the program and testing the applicability, many actual problems are solved and compared with the available data. Comparison of the results with that by STAR-CD or FLUENT program has been also made for the same flow configuration and grid structure to test the validity of NUFLEX.

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Evaluation of Thin Film Residual Stress through the Analysis of Stress Relaxation Path and the Modeling of Contact Morphology (응력완화 경로분석과 압입자/시편간 접촉형상 모델링에 바탕한 박막재료의 국소 잔류응력 평가)

  • Lee, Yun-Hee;Kim, Sung-Hoon;Jang, Jae-Il;Kwon, Dong-Il
    • Proceedings of the KSME Conference
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    • 2001.06a
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    • pp.237-242
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    • 2001
  • Residual stress is a dominant obstacle to efficient production and safe usage of products by reducing the mechanical strength and failure properties. Especially, it causes interfacial failure and substrate deflection in the case of thin film. So, the exact evaluation and optimum control of thin film residual stress is indispensable. However, hole drilling or X-ray diffraction techniques have some limits in application to thin film. And, curvature technique for thin film materials cannot give the information about local stress variation. Therefore, we applied the nanoindentation technique in evaluating the thin film residual stress. In this study, we modeled the change of indentation loading curve for residually stressed and stress-free thin films during stress relaxation. The value of residual stress was directly related to the indentation depth change by relaxation. The residual stress from nanoindentation analysis was consistent with the result from curvature technique.

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Identification of Dynamic Joint Characteristics Using a Multi-domain FRF-based Substructuring Method (다중 전달함수합성법을 이용한 진동시스템의 결합부 특성 값 동정)

  • 이두호;황우석
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2003.05a
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    • pp.501-509
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    • 2003
  • A method of identifying structural parameters such as stiffness and damping coefficients at interfacial points of vibro-acoustic systems is suggested using an optimization technique. To identify the parameters using a numerical optimization algorithm, cost functions are defined. The cost function should be zero at the correct parameter values. To minimize the cost functions using an optimization technique, a design sensitivity analysis procedure is developed in the framework of the multi-domain FRF-based substructuring method. As a numerical example, a ladder-like structure problem is introduced. With known parameter values and different initial guesses of the parameters, convergence characteristics to the exact value are compared for the three cost functions. Investigating the contours of the cost functions, we find the first cost function has the largest convergent region to the correct value. As another practical problem, stiffnesses of engine mounts and bushings in a passenger car are identified. The numerical examples show that the proposed method is efficient and accurate even when applied to realistic problems.

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Film Boiling Heat Transfer from Relatively Large Diameter Downward-facing Hemispheres

  • Kim Chan Soo;Suh Kune Y.;Park Goon Cherl;Lee Un Chul;Yoon Ho Jun
    • Nuclear Engineering and Technology
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    • v.35 no.4
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    • pp.274-285
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    • 2003
  • Film boiling heat transfer coefficients for a downward-facing hemispherical surface are measured from the quenching tests in DELTA (Downward-boiling Experimental Loop for Transient Analysis). Two test sections are made of copper to maintain Bi below 0.1. The outer diameters of the hemispheres are 120 mm and 294 mm, respectively. The thickness of both the test sections is 30 mm. The effect of diameter on film boiling heat transfer is quantified utilizing results obtained from the two test sections. The measured heat transfer coefficients for the test section with diameter 120 mm lie within the bounding values from the laminar film boiling analysis, while those for diameter 294 mm are found to be greater than the numerical results on account of the Helmholtz instability. There is little difference observed between the film boiling heat transfer coefficients measured from the two test sections. In addition, the higher thermal conductivity of copper results in the higher minimum heat flux in the tests. For the test section of diameter 120 mm, the Leidenfrost point is lower than that for the test section of diameter 294 mm. Destabilization of film boiling propagates radially inward for the 294 mm test section versus radially outward for the 120 mm Test Section.

Parametric study on the structural response of a high burnup spent nuclear fuel rod under drop impact considering post-irradiated fuel conditions

  • Almomani, Belal;Kim, Seyeon;Jang, Dongchan;Lee, Sanghoon
    • Nuclear Engineering and Technology
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    • v.52 no.5
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    • pp.1079-1092
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    • 2020
  • A parametric study of several parameters relevant to design safety on the spent nuclear fuel (SNF) rod response under a drop accident is presented. In the view of the complexity of interactions between the independent safety-related parameters, a factorial design of experiment is employed as an efficient method to investigate the main effects and the interactions between them. A detailed single full-length fuel rod is used with consideration of post-irradiated fuel conditions under horizontal and vertical free-drops onto an unyielding surface using finite-element analysis. Critical drop heights and critical g-loads that yield the threshold plastic strain in the cladding are numerically estimated to evaluate the fuel rod structural resistance to impact load. The combinatory effects of four uncertain parameters (pellet-cladding interfacial bonding, material properties, spacer grid stiffness, rod internal pressure) and the interactions between them on the fuel rod response are investigated. The principal finding of this research showed that the effects of above-mentioned parameters on the load-carrying capacity of fuel rod are significantly different. This study could help to prioritize the importance of data in managing and studying the structural integrity of the SNF.

Lubrication phenomenon in the stagnation point flow of Walters-B nanofluid

  • Muhammad Taj;Manzoor Ahmad;Mohamed A. Khadimallah;Saima Akram;Muzamal Hussain;Madeeha Tahir;Faisal Mehmood Butt;Abdelouahed Tounsi
    • Advances in concrete construction
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    • v.15 no.5
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    • pp.303-312
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    • 2023
  • The present study investigates the effects of Cattaneo-Christov thermal effects of stagnation point in Walters-B nanofluid flow through lubrication of power-law fluid by taking the slip at the interfacial condition. For the solution, the governing partial differential equation is transformed into a series of non-linear ordinary differential equations. With the help of hybrid homotopy analysis method; that consists of both the homotopy analysis and shooting method these equations can be solved. The influence of different involved constraints on quantities of interest are sketched and discussed. The viscoelastic parameter, slip parameters on velocity component and temperature are analyzed. The velocity varies by increase in viscoelastic parameter in the presence of slip parameter. The slip on the surface has major effect and mask the effect of stagnation point for whole slip condition and throughout the surface velocity remained same. Matched the present solution with previously published data and observed good agreement. It can be seen that the slip effects dominates the effects of free stream and for the large values of viscoelastic parameter the temperature as well as the concentration profile both decreases.

Removal Torque and Histomorphometric Investigation of Surface Modified Commercial Implants: An Experimental Study in the Rabbit Tibia (상용화된 치과용 임플란트의 뒤틀림 제거력 및 조직학적 분석 연구: 가토 경골에서의 연구)

  • Park, Jong-Hyun;Kim, Dae-Gon;Cho, Lee-Ra;Park, Chan-Jin
    • Journal of Dental Rehabilitation and Applied Science
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    • v.24 no.1
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    • pp.41-56
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    • 2008
  • The methods of surface modification of commercial implants were various according to the manufacturer. Surface modification of implant may produce diverse physical and chemical surface characteristics resulted from the treatment method and treatment condition. As a result, the bone response might be different. Even though surface modified implants have been used clinically, most researches are focusing on the bone response of surface modified implants comparing to machined implants rather than surface modified commercial implants. This study compare and analyze bone responses of 4 surface modified commercial implants with different shapes and surfaces. Eighty surface modified commercial implants with 4 different surface characteristics were installed in the tibia of white Newzealand rabbits. Biomechanical stability tests and histomorphometric evaluation were done. The results were as follows: 1. Surface modified commercial implants showed stable osseointegration at 6 weeks after installation. 2. Histomorphometric evaluation showed that there was no significant differences in bone to implant contact among 4 different commercial titanium implants. In comparing the implants with different shape the measurement of bone growth in subcortical area would be more reliable than entire bone to implant contact length. 3. Resonance Frequency Analysis showed that there was no significant differences among 4 types of implants, even though they were significantly different in installation. 4. There was significant differences in interfacial shear strength among 4 type of implants. 5. It is difficult to observe accurate bone to implant interface using Micro-CT. However, it is possible to measure the entire contact length of the implant to the bone.

Soluble Polyimide Binder for Silicon Electrodes in Lithium Secondary Batteries (리튬이차전지 실리콘 전극용 용해성 폴리이미드 바인더)

  • Song, Danoh;Lee, Seung Hyun;Kim, Kyuman;Ryou, Myung-Hyun;Park, Won Ho;Lee, Yong Min
    • Applied Chemistry for Engineering
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    • v.26 no.6
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    • pp.674-680
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    • 2015
  • A solvent-soluble polyimide (PI) polymeric binder was synthesized by a two-step reaction for silicon (Si) anodes for lithium-ion batteries. Polyamic acid was first prepared through ring opening between two monomers, bicyclo[2,2,2]oct-7-ene-2,3,5,6-tetracarboxylic dianhydride (BCDA) and 4,4-oxydianiline (ODA), followed by condensation reaction. Using the synthesized PI polymeric binder (molecular weight = ~10,945), the coating slurry was then prepared and Si anode was fabricated. For the control system, Si anode based on polyvinylidene fluoride (PVDF, molecular weight = ~350,000) having the same constituent ratio was prepared. During precycling, PI polymeric binder revealed much improved discharge capacity ($2,167mAh\;g^{-1}$) compared to that of using PVDF polymeric binder ($1,740mAh\;g^{-1}$), while the Coulombic efficiency of two systems were similar. PI polymeric binder improved the cycle retention ability during cycles compared to that of using PVDF, which is attributed to an improved adhesion property inside Si anode diminishing the dimensional stress during Si volume changes. The adhesion property of each polymeric binder in Si anode was confirmed by surface and interfacial cutting analysis system (SAICAS) (Si anode based on PI polymeric binder = $0.217kN\;m^{-1}$ and Si anode based on PVDF polymeric binder = $0.185kN\;m^{-1}$).