• 콘크리트학회논문집
• /
• 제14권4호
• /
• pp.474-482
• /
• 2002

본 연구의 목적은 섬유의 부착시험을 통하여 섬유의 파괴없이 최대 인발저항을 가지고 시멘트 모체 내에서 완전한 정착작용을하는 구조용 합성섬유의 최적형상과 최적형상함수를 도출하는데 있다. 7가지 다른 형상의 구조용 합성섬유를 조사하였고 부착시험을 수행하였다. 부착시험의 변수는 7가지의 다른 형상이고, 2종류의 시멘트 모르타르의 배합이다. 부착시험 결과, 7가지 다른 형상중 crimped type이 계면인성(인발에너지)와 인발하중에서 가장 우수한 성능을 보였다. Crimped type을 기본으로 하여 섬유의 주기와 높이를 바꾸어 부착시험을 실시한 결과 최적형상함수, D= $b^{{\alpha}ο{\alpha}}$ $h^{λ{\beta}}$ 를 도출하였다.

• 한국재료학회지
• /
• 제14권5호
• /
• pp.322-327
• /
• 2004

Copper-based leadframe sheets were oxidized in two kinds of hot alkaline solutions to form brown-oxide or black-oxide layer on the surface. The oxide coated leadframe sheets were molded with epoxy molding compound (EMC). After post mold curing, the oxide-coated EMC-leadframe joints were machined to form sandwiched Brazil-nut (SBN) specimens. The SBN specimens were used to measure the fracture toughness of the EMC/leadframe interfaces under mixed-mode (mode I + mode II) loading conditions. Fracture surfaces were analyzed by various equipment to investigate failure path. The results revealed that the failure paths were strongly dependent on the oxide type. In case of brown oxide, hackle-type failure was observed and failure path lay near the EMC/CuO interface with a little inclining to CuO at all case. On the other hand, in case of black oxide, quite different failure path was observed with respect to the distance from the tip of pre-crack and phase angle. Different failures occurred with oxide type is presumed to be due to the difference in microstructure of the oxides.

• 공업화학
• /
• 제10권5호
• /
• pp.789-795
• /
• 1999

본 연구에서는 비원형의 단-탄소섬유를 이용하여 시멘트 복합재를 제조하고 이 복합재의 특성(건조 수축, 동결 융해저항성, 파괴 인성)을 원형 탄소섬유보강 복합재와 비교하여 연구하였다. 그 결과 섬유의 형상과 길이에 크게 의존하였다. C형 탄소섬유보강 시멘트 복합재의 건조수축저감 효과가 다른 형상의 섬유보강 복합재에 비해 우수하였다. 이 효과는 섬유의 종횡비가 클수록 증가하였다. 또한, 동결융해 저항성은 섬유형상의 영향은 두드러지지 않았으나 섬유길이와 섬유함유율에 따라 증가하였다. 특히, C형 보강 시멘트 복합재의 파괴 인성 및 균열 저항성은 다른 것에 비해 크게 개선되었다. 이는 더 큰 계면으로 파괴에너지를 더 많이 흡수하였기 때문으로 생각된다.

• 열처리공학회지
• /
• 제25권2호
• /
• pp.74-79
• /
• 2012

This study has been carried out to investigate the precipitation behavior of ${\chi}$ phase and effect of ${\chi}$ phase precipitation on the impact toughness of 25%Cr-7%Ni-4%Mo super duplex stainless steel. It was proved that the ${\chi}$ phase was a intermetallic compound, which represented the higher chromium and molybdenum concentration than the matrix phases, and also showed the higher molybdenum concentration than the ${\sigma}$ phase. The ${\chi}$ phase was precipitated at the interface between ferrite and austenite or inside the ferrite matrix in the early stage of aging. The number of ${\chi}$ phase precipitates increased with increasing aging time, however, after showing the maximum value, the number was decreased due to the gradual transformation of ${\chi}$ phase into ${\sigma}$-phase. Aging ferrite phase was decomposed by the $r^2$ phase and ${\sigma}$-phase. Impact toughness rapidly decreased with time in the initial stage of aging at ${\chi}$ phase start to precipitate. Thus, the impact toughness was greatly influence for the precipitation of ${\chi}$ phase.

• Restorative Dentistry and Endodontics
• /
• 제32권3호
• /
• pp.208-221
• /
• 2007

파괴 인성 실험은 상아질-복합레진 계면의 파절 저항성을 평가할 수 있는 임상적으로 신뢰 할 만한 방법이다. 본 연구의 목적은 상아질-레진 계면의 파괴인성과 미세인장결합강도를 측정하여 이 두 실험방법이 상아질-레진 결합을 평가하는 데 가지는 유용성을 비교, 평가하는 것이다 파괴 인성 측정에는 short-rod 시편 형태를 이용하였다. 각 시편에서는 소의 하악절치에서 절단한 치아 절편을 포함시켜 결합면을 얻었다. 미세인장 결합강도 또한 소의 하악절치 순면을 연마하여 상아질을 노출시킨 후 상아질 접착제를 도포하고 레진 블록을 축조하여 측정하였다. 각 시편들은 $37^{\circ}C$ 증류수에 24시간 보관한 후 각 실험방법에 맞게 인장력을 가하여 측정치를 구하였다. 통계분석은 95% 신뢰수준의 ANOVA와 Tukey's test를 이용하였으며, 두 실험방법의 상관관계를 보기 위해 Pearson's 상관계수를 계산하였다. 전자현미경 검사를 통해 미세구조 또한 관찰하여 다음과 같은 결론을 얻었다. 1. 파괴인성은 SE군이 가장 높은 값을 나타냈으며, Adper Single Bond 2 (SB), OptiBond Solo (OB) ONE-STEP PLUS (OS), ScotchBond Multi-purpose (SM)군 순으로 나타났고, Clearfil SE Bond (SE)군은 다른 실험군에 비해 유의하게 높은 값을 나타내었으나 (p <0.05), 다른 실험군 사이에는 유의차가 없었다 (p > 0.05). 2. 미세인장결합강도는 SE군이 가장 높은 값을 나타냈으며, SB, OB, SM, 그리고 OS 순으로 나타났다. SB, OB, SM, SE군 사이에는 통계학적인 유의차가 없었으나 (p > 0.05), OS군의 미세인장결합강도는 다른 4개의 실험군에 비해 낮은 값을 나타내었다 (p < 0.05). 3. FE-SEM관찰에서 피막도가 두껍게 나타난 SM군, SE군과 피막도가 얇은 OS군, OB군, SB군 간에 파괴양상이 다르게 나타났다 즉 전자는 접착층 내 파괴가 일어난 반면, 후자는 resin tag나 레진 침투층 내에서 파절되는 양상을 나타내었다. 4. 파괴 인성과 미세인장결합강도 사이에는 통계학적으로 유의 한 상관 관계가 없었다 ($r^2=0.223$, t=0.927). 이와 같은 결과를 토대로, 상아질 접착제의 임상적 효율성을 평가하고자 할 때는 결합강도 뿐만 아니라. 파괴인성도 함께 고려하여 임상적용의 예견성을 높여야 한다고 결론내릴 수 있다.

• 한국안전학회지
• /
• 제21권4호
• /
• pp.19-24
• /
• 2006

Fatigue crack propagation tests for the brake disc cast iron were conducted for investigating fatigue crack propagation rate(da/dN), crack propagation path and fracture toughness($K_c$) of the material. The threshold stress intensity factor range, ${\Delta}K_{th}$, was found to be about $6MPa{\sqrt{m}}$ at the stress ratio of R = 0.1. Also, fracture toughness value was determined to be $24.7MPa{\sqrt{m}}$. Irregular fatigue fracture surfaces were observed, indicating that fatigue crack growth occurred at the interface between randomly scattered flak graphite and ferrite, where the interfacial strength was relatively weak.

• 한국철도학회논문집
• /
• 제8권6호
• /
• pp.573-580
• /
• 2005

Model I interlaminar fracture behaviors of the carbon/epoxy composite, one of the candidate composites for a tilting train carbody, were investigate by the use of DCB(Double cantilever beam) specimens. These specimens were made of CF3327 plain woven fabric with epoxy resin, and an artificial starter delamination was fabricated by inserting Teflon film with the thickness of $12.5{\mu}m$ of $25.0{\mu}m$ at the one end of the specimen. Mode I interlaminar fracture toughness was evaluated for the specimens with the different thickness of an inserter. Also delamination propagating behaviors and interlaminar fracture surface were examined through an ooptical travelling scope and a scanning electron microscope. We found that abruptly unstable crack propagation called as stick-slip phenomena was observed. In addition, interlaminar fracture behaviors were affected on the location and the morphology of a crack tip as well as an interface region.

• 세라미스트
• /
• 제23권2호
• /
• pp.114-131
• /
• 2020

Fracture in the titanium carbonitride-metal composites occurs by crack propagation through the carbonitride grains or in the interfaces. Thus, intrinsic properties of the carbonitride need to be enhanced and the interfaces should be also modified to coherent structure to strengthen the composites. Especially, interfacial structure can be the main factor to determine the mechanical properties of titanium carbonitride-metal composites because the interfaces between carbonitride grains and metallic phase are weak parts due to heterogeneous nature of carbonitride and metallic phase. In this paper, methodologies for improving the interfacial structure of titanium carbonitride-metal composites are suggested. Total area of the interfaces can be reduced using solid solution type carbonitrides as raw materials instead of a mixture of various carbonitrides in the composites. Also, synthesis of titanium carbonitride-metal composite powders and the low-temperature sintering of the composite powders for short time can be the way for formation of coherent interfaces. The sintering of the composite powders for short time at low temperature can reduce the potential of formation of interfaces by dissolution and precipitation of carbonitride in the liquid metal. As a result of formation of coherent boundaries due to low-temperature and short-time sintering, interfaces between titanium carbonitride grains and metallic phase have the favorable structure for the enhanced fracture toughness. It is believed that the low-temperature sintering of solid solution type composite powders for short time can be the way to improve the low toughness of the titanium carbonitride-metal composites.

• 한국생산제조학회지
• /
• 제5권4호
• /
• pp.53-62
• /
• 1996

Recently, ceramic / metal bonded joints have led to inccreasing use of structural materials such as automobile, heat engine in various industries. In this paper, a method to analyze an interface crack under both residual stresses and applied loading was proposed. and some results of boundary element method(BEM) analysis Were presented, Fracture thoughness tests of ceramic/metals bonded joints with an interface crack Were carried out, and the stress intensity factors of these joints Ware analyzed by BEM. Also crack propagtion direction was simulated numerically by using BEM. Crack propagation angle was able to easily determine based on the maximum stress concept. The prediction of fracture strength by the fracture thoughness of the ceramics/metals bonded joints was proposed.

• 한국농공학회논문집
• /
• 제54권5호
• /
• pp.25-34
• /
• 2012

It has been well known that concrete structures exposed to acid and sulfate environments such as sewer etc. show significant decrease in their durability due to chemical attack. Such deleterious acid and sulfate attacks lead to expansion and cracking in concrete, and thus, eventually result in damage to cement mortar by forming expansive hydration products due to the reaction between cement hydration products and acid and sulfate ions. In this study, the effect of fly ash and blast furnace slag on the bond performances of structural synthetic fiber in latex modified cement mortar under sulfate environments. Fly ash and blast furnace slag contents ranging from 0 % to 20 % are used in the mix proportions. The latex modified cement mortar specimens were immersed in fresh water, 8 % sodium sulfate ($Na_2SO_4$) solutions for 28 and 50 days, respectively. Pullout tests are conducted to measure the bond performance of structural synthetic fiber from latex modified cement mortar after sulfate environments exposure. Test results are found that the incorporation of fly ash and blast furnace slag can effectively enhance the PVA fiber-latex modified cement mortar interfacial bond properties (bond behavior, bond strength and interface toughness) after sulfate environments exposure. The microstructural observation confirms the findings on the interface bond mechanism drawn from the fiber pullout test results under sulfate environments.