• Journal of Powder Materials
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• v.28 no.4
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• pp.317-324
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• 2021

High-strength low-alloy (HSLA) steels show excellent toughness when trace amounts of transition elements are added. In steels, prior austenite grain size (PAGS), which is often determined by the number of added elements, is a critical factor in determining the mechanical properties of the material. In this study, we used two etching methods to measure and compare the PAGS of specimens with bainitic HSLA steels having different Nb contents These two methods were nital etching and picric acid etching. Both methods confirmed that the sample with high Nb content exhibited smaller PAGS than its low Nb counterpart because of Nb's ability to hinder austenite recrystallization at high temperatures. Although both etching approaches are beneficial to PAGS estimation, the picric acid etching method has the advantage of enabling observation of the interface containing Nb precipitate. By contrast, the nital etching method has the advantage of a very short etching time (5 s) in determining the PAGS, with the picric acid etching method being considerably longer (5 h).

• Composites Research
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• v.29 no.2
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• pp.45-52
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• 2016

An understanding of the failure mechanisms of the adhesive layer is decisive in interpreting the performance of a particular adhesive joint because the delamination is one of the most common failure modes of the laminated composites such as the fiber metal laminates. The interface between different materials, which is the case between the metal and the composite layers in this study, can be loaded through a combination of fracture modes. All loads can be decomposed into peel stresses, perpendicular to the interface, and two in-plane shear stresses, leading to three basic fracture mode I, II and III. To determine the load causing the delamination growth, the energy release rate should be identified in corresponding criterion involving the critical energy release rate ($G_C$) of the material. The critical energy release rate based on these three modes will be $G_{IC}$, $G_{IIC}$ and $G_{IIIC}$. In this study, to evaluate the fracture behaviors in the fracture mode I and II of the adhesive layer in fiber metal laminates, the double cantilever beam and the end-notched flexure tests were performed using the reference adhesive joints. Furthermore, it is confirmed that the experimental results of the adhesive fracture toughness can be applied by the comparison with the finite element analysis using cohesive zone model.

• Journal of Adhesion and Interface
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• v.21 no.3
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• pp.93-100
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• 2020

3D printing technology enables proper objects to be made through an additive manufacturing method, but resulting in dimension deviation of the product due to contraction phenomenon as cooling melted filament resin injected from high-temperature use environment. In this research, we studied on acrylic adhesives for 3D printer build sheet in order to fabricate high-quality products with a precise shape and to well-mount without distortion. The solvent-free UV-curable acrylic adhesive formulation was designed by adding 4-acryloylmorpholine (ACMO) with high adhesion, toughness, glass transition temperature so that adhesion properties are stable at high temperature and products are easily mounted/detached from the adhesives. The designed formulation was polymerized through two-steps using post-addition of monomers. Using this, the acrylic adhesive was coated to make a film and then analyzed using various experimental techniques. As a result, the fabricated adhesive exhibited high glass transition temperature and there was little gap in peel strength before and after thermal treatment. Moreover, it was confirmed by rheological analysis that this adhesive can provide great bonding/debonding ability without distortion. We demonstrated the fabrication of a rectangular product using a 3D printing method using our acrylic adhesive as a build sheet. Mounting ability and workability were satisfactory and dimension deviation of the product was tiny. Because the product is easily detachable from the acrylic adhesive developed here than conventional build sheets, it is expected that this will provide work convenience to users who use the 3D printer.

• Journal of Adhesion and Interface
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• v.4 no.1
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• pp.1-8
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• 2003

In this work, the effect of PMR-15 content on the variation of surface free energy of the DGEBA/PMR-15 blend system was investigated in terms of contact angles and mechanical interfacial tests. Based on FT-IR result of the blend system. C=O (1,772, $1,778cm^{-1}$) and C-N ($1,372cm^{-1}$) peaks appeared with imidization of PMR-15 and -OH ($3,500cm^{-1}$) peak showed broadly at 10 phr of PMR-15 by ring-opening of epoxy. Contact angle measurements were performed by using deionized water and diiodomethane as testing liquids. As a result, the surface free energy of the blends gave a maximum value at 10 phr of PMR-15, due to the significant increasing of specific component. The mechanical interfacial properties measured from the critical stress intensity factor ($K_{IC}$) and the critical strain energy release rate ($G_{IC}$) showed a similar behavior with the results of surface energetics. This behavior was probably attributed to The improving of the interfacial adhesion between intermolecules, resulting from increasing the hydrogen bondings of the blends.

• Journal of Welding and Joining
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• v.29 no.6
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• pp.56-64
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• 2011

Friction stir spot welding between 5454 aluminum alloy sheets with the different thicknesses of 1.4 and 1.0 mm was performed. In the welding process, the tool for welding was rotated ranging from 500 to 2500, and plunged to the depth of 1.8 mm under a constant tool plunge speed of 100 mm/min. And then, the rotating tool was maintained at the plunge depth during the dwell time ranging from 0 to 7 sec. The pull-out speed of the rotating tool was 100 mm/min. The increase of tool rotation speed resulted in the change of the macrostructure of friction-stir-spot-welded zone, especially the geometry of welding interface. The results of the tensile shear test showed that the total displacement and toughness of the welds were increased with the increase of the tool rotation speed, although the maximum tensile shear load was decreased. However, the change in the dwell time at the plunge depth of the tool did not produce the remarkable variation in the macrostructure and mechanical properties of the welds. In all cases, the average hardness in friction-stir-spot-welded zone was higher than that of the base metal zone. By the friction stir spot welding technique, the welds with the excellent mechanical properties than the mechanically-clinched joints could be obtained.

• Journal of the Korea Institute of Building Construction
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• v.19 no.3
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• pp.201-207
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• 2019

In this study, the direct tensile properties of amorphous metallic fiber-reinforced cement based composites according to the strain was evaluated. A thin plate-shape amorphous metallic fiber with 15mm and 30mm in length was used. And fiber-reinforced cement based composites were prepared with contents of 1.0, 1.5, 2.0%. The direct tensile test was conducted under the conditions of $10^{-6}/s(static)$ and $10^1/s(dynamic)$ strain rate. As a results, amorphous metallic fiber with a length of 15mm was observed in pull-out behavior from the cement matrix because of the short fiber length and large portion of mixed fiber. On the other hand, amorphous metallic fiber with a length of 30mm were not pulled out from matrix because the bonding force between the fiber and matrix was large due to rough surface and large specific surface area. However, fracture occurred because thin plate shape fibers were vulnerable to shear force. Tensile strength, strain capacity and toughness were improved due to the increase in the fiber length. The dynamic increase factor of L15 was larger that of L30 because the bonding performance of the fiber-matrix interface is significantly affected by the strain rate.