• Title/Summary/Keyword: initial curing temperature

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TEMPERATURE CHANGES IN THE PULP ACCORDING TO VARIOUS ESTHETIC RESTORATIVE MATERIALS AND BASES DURING CURING PROCEDURE (광중합 시 수종의 심미적 수복재와 이장재의 사용에 따른 치수내 온도변화)

  • 장혜란;이형일;이광원;이세준
    • Restorative Dentistry and Endodontics
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    • v.26 no.5
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    • pp.393-398
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    • 2001
  • Polymerization of light-activated restorations results in temperature increase caused by both the exothermic reaction process and the energy absorbed during irradiation. Within composite resin, temperature increases up to 2$0^{\circ}C$ or more during polymerization. But, insulation of hard tissue of tooth lowers this temperature increase in pulp. However, many clinicians are concerned about intrapulpal temperature injury. The purpose of this study was to evaluate temperature changes in the pulp according to various restorative materials and bases during curing procedure. Caries and restoration-free mandibular molars extracted within three months were prepared Class I cavity of 3$\times$6mm with high speed handpiece fissure bur. 1mm depth of dentin was evaluated with micrometer in mesial and distal pulp horns. Pulp chambers were filled with 37.0$\pm$0.1$^{\circ}C$ water to CEJ. Chromium-alumina thermocouple was placed in pulp horn below restorative materials for evaluating of temperature changes. This thermocouple was connected to temperature-recording device(Multiplication analyzer MX, 6.000, JAPAN). Temperature changes was evaluated from initial 37.$0^{\circ}C$ after temperature changes to 37.$0^{\circ}C$. Tip of curing unit was placed in the center of prepared cavity separated 1mm from restorative materials. Curing time was 40s. The restorative materials were used with Z 100, Fuji II LC, Compoglass flow and bases were used with Vitrebond, Dycal. Resrorative materials were placed in 2mm. The depth of bases were formed in 1mm and in this upper portion, resin of 2mm depth was placed. This procedure was performed 10 times. The results were as follows. 1. All the groups showed that the temperature in pulp increased as curing time increased 2. The temperature increase of glass ionomer was significantly higher than that of Resin and Compomer during curing procedure (P<0.05). 3. The temperature increase in glass ionomer base was significantly higher than that of Calcium hydroxide base during Resin curing procedure (P<0.05).

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Relationship between Compressive Strength of Geo-polymers and Pre-curing Conditions

  • Kim, Hyunjung;Kim, Yooteak
    • Applied Microscopy
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    • v.43 no.4
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    • pp.155-163
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    • 2013
  • Meta-kaolin (MK) and blast furnace slag (BS) were used as raw materials with NaOH and sodium silicate as alkali activators for making geo-polymers. The compressive strength with respect to the various pre-curing conditions was investigated. In order to improve the recycling rate of BS while still obtaining high compressive strength of the geo-polymers, it was necessary to provide additional CaO to the MK by adding BS. The specimens containing greater amounts of BS can be applied to fields that require high initial compressive strength. Alkali activator(s) are inevitably required to make geo-polymers useful. High temperature pre-curing plays an important role in improving compressive strength in geo-polymers at the early stage of curing. On the other hand, long-term curing produced little to no positive effects and may have even worsened the compressive strength of the geo-polymers because of micro-structural defects through volume expansion by high temperature pre-curing. Therefore, a pre-curing process at a medium range temperature of $50^{\circ}C$ is recommended because a continuous increase in compressive strength during the entire curing period as well as good compressive strength at the early stages can be obtained.

Temperature History of Concrete Corresponding to Various Bubble Sheets Layer and Curing Temperature (양생온도 변화 및 버블시트 두께변화에 따른 콘크리트의 온도이력특성)

  • Hong, Seak-Min;Baek, Dae-Hyun;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2008.11a
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    • pp.21-25
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    • 2008
  • In this paper, the temperature history and the strength development of concrete corresponded to various bubble sheets layer and curing temperature. Based on the results, In case of the test temperature of -5℃, concrete subject in the exposure condition, result in a frost damage at initial stage by a fall of below zero temperature. In case of the combination of PE film and non woven fabric was after 36 hour, and combination of bubble sheet over double, a tremendous insulating effect of bubble sheet over double is confirmed due to the temperature of concrete fall of below zero temperature after 60 hours. Meanwhile, regarding the -15℃ of temperature, special measure for insulation curing is necessary to secure stability against early frost damage because frost damage was not affected by the lapping thickness of bubble sheet subjected to severe cold weather condition.

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Strength Development of Mock-up Concrete Structure subjected to Extremely Low Temperature Condition Due to Curing Methods (극저온 조건에서의 양생방법 변화에 따른 실구조체 콘크리트의 강도발현 특성)

  • Jung, Eun-Bong;Jung, Sang-Hyeon;Ahn, Sang-Ku;Ko, Gyeong-Taek;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2012.11a
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    • pp.47-49
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    • 2012
  • Under this study, the characteristics of concrete intensity condition following the curing method under the extremely low temperature environment have been contemplated, and as a result, in the event of insulation + heat cable curing, the intensity and accumulated temperature accomplishment period is required for two times of requiring initial frost damage prevention than the case of heating + heat insulation curing method due to the insufficient calories supplied in general.

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Effects of Curing Conditions on the Chemical Compositions of Positive Plate for Lead Acid Battery Plates (납축전지 극판의 숙성 조건이 양극판의 화학적 조성에 미치는 영향)

  • Ku, Bon-Keun;Jeong, Soon-Wook
    • Journal of the Korean Applied Science and Technology
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    • v.23 no.4
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    • pp.347-354
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    • 2006
  • Generally, it has been known that positive plate efficiency is the most influential effect on the initial current capacity of lead acid battery. Thus, in this study, we have investigated the curing effect of the positive plate, which is one of the important lead acid battery processes. The curing process of the positive plate is performed either with the separation of each plate with 1mm gap or with no gap of plate. As a result, when there is no interval between each plate, the higher temperature current happened than expected, resulting in the changes in the initial current efficiency of the lead acid battery. The chemical composition and crystal structure of a material coated on the positive plate were identified with XRD and SEM. It was resulted that were only there not a lot of 4BS (tetrabasic-lead sulfate, $4PbO{\cdot}PbSO_4)$ on the plate in case of curing of plates without interval, but a large quantity of $Pb_3O_4$ also formed on the surface. On the other hand, it was observed that 3BS (tribasic-lead sulface, $3PbO{\cdot}PbSO_4{\cdot}H_2O)$ was the main product on the plate in case of typical curing process with some interval. From the initial current capacity test, the positive plate having 3BS was approximately 40% higher in initial current capacity than that having 4BS. It was concluded that 4BS and $Pb_3O_4$ on the plate surface were harmful to the initial current capacity of lead acid battery.

Effect of Compressive Strength and Curing Condition on the Direct Tensile Strength Properties of Ultra High Performance Concrete (압축강도 및 양생조건에 따른 초고성능 콘크리트의 직접인장강도 특성)

  • Park, Ji Woong;Lee, Gun Cheol
    • Journal of the Korea Institute of Building Construction
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    • v.17 no.2
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    • pp.175-181
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    • 2017
  • The purpose of this study is evaluating the characteristics of tensile strength of UHPC and examining tensile performance of notched specimens by direct tensile test. For test variables, 120, 150, and 180MPa of target design standard strength were aimed at. With general water curing and $90^{\circ}C$ high temperature steam as curing conditions, the properties were reviewed. Overall, it was represented that the specimens of notch-type direct tensile strength concrete was effective in inducing central cracks compared with existing direct tension specimens. Through this, it was judged that data construction with high reliability was possible. Above all, in a graph of direct tensile strength and strain, in the case of steam curing at high temperature, there was great difference of initial tensile strength compared with water curing. As passing of ages, an aspect that the difference gradually decreased was shown. Maximum tensile strength was found to increase steadily with increasing age for all target design strengths in water curing, in the case of steam curing, the tendency to increase significantly due to the initial strength development effect at 7 days of age. The initial crack strength increases with age in case of underwater curing, in the case of steam curing, it was higher than that of water curing in 7 days, while the strength of 28 days was lowered. In this part, it is considered necessary to examine the arrangement condition of the steel fiber.

Study on the Electro-Optic Characteristics Depending on UV Condition in the Normally Scattering(NS)/Normally Transparent(NT) Polymer Dispersed Liquid Crystal Mode (Normally Scattering(NS)/Normally Transparent (NT) 고분자 분산형 액정 모드에서 UV 조건에 따른 전기 광학특성 연구)

  • Kim, M.S.;Seo, Y.H.;Lee, M.H.;Rhee, J.M.;Lee, T.S.;Lee, S.H.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2003.07b
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    • pp.1050-1053
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    • 2003
  • Polymer dispersed liquid crystal mode can be classified into two cases, normally scattering mode (NS) and normally transparent (NT) mode according to an initial state. Electro-optic characteristic NS/NT PDLC mode can be improved by controlling the factors to influence the phase separation. In case of NS PDLC mode, we inspected change of a phase separation as a function of curing temperature for the mixture of E7 and NOA65 with different ratios. When the LC concentration is less than polymer such as LC : NOA65 = 40 : 60wt%, the PDLC cell is influenced strongly by the curing temperature. However, when LC concentration is much less than polymer such as LC : NOA65 : 80 : 20wt%, it is influenced slightly by the curing temperature. In case of NT PDLC mode, we observed change of a phase separation as a function of the ratio of the mixture and UV conditions such as curing temperature, UV intensity The cell made with strong UV intensity and curing temperature of $20^{\circ}C$, in case that the ratio of LC to polymer is 70:30wt%, showed good electro-optic characteristics.

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Laboratory investigation for engineering properties of sodium alginate treated clay

  • Cheng, Zhanbo;Geng, Xueyu
    • Structural Engineering and Mechanics
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    • v.84 no.4
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    • pp.465-477
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    • 2022
  • The formation of biopolymer-soil matrices mainly depends on biopolymer type and concentration, soil type, pore fluid and phase transfer to influence its strengthening efficiency. In this study, the physical and mechanical properties of sodium alginate (SA) treated kaolinite are investigated through compaction test, thread rolling teat, fall cone test and unconfined compression test with considering biopolymer concentration, curing time, initial water content, mixing method. The results show that the liquid limit slightly decreases from 69.9% to 68.3% at 0.2% SA and then gradually increases to 98.3% at 5% SA. At hydrated condition, the unconfined compressive strength (UCS) of SA treated clay at 0.5%, 1%, 2% and 3% concentrations is 2.57, 4.5, 7.1 and 5.48 times of untreated clay (15.7 kPa) at the same initial water content. In addition, the optimum biopolymer concentration, curing time, mixing method and initial water content can be regarded as 2%, 28 days, room temperature water-dry mixing (RD), 50%-55% to achieve the maximum unconfined compressive strength, which corresponds to the UCS increment of 593%, compared to the maximum UCS of untreated clay (780 kPa).

An Experimental Study on Crack Control of Core-wall Using 700kg/$\textrm{cm}^2$ Ultra High Strength Concrete (초고강도 콘크리트로 타설된 내부코아 벽체의 균열발생 및 제어에 관한 실험적 연구)

  • 윤영수;이승훈;노병용;박희도
    • Proceedings of the Korea Concrete Institute Conference
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    • 1995.04a
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    • pp.201-206
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    • 1995
  • This paper presents the experimental study on crack control of core-wall placed with 700kg/$\textrm{cm}^2$ Ultra high strength concrete. The thermal sensors were installed into the core-walls prior to the concrete casting to measure the heat of hydration and atmospheric temperature whose difference might cause the initial crack. Several curing schemes were taken for each basement floor 8 thru 6 to examine the influence of curing method on the crack width, total crack length and the number of crack occurred. This paper demonstrates that the proper curing scheme have a great favorable effect on the initial crack control on the structural elements with noticiable reduction in crack width.

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Estimation of Setting Time of Cement Mortar combined with Recycled Aggregate Powder and Cement Kiln Dust based on Equivalent Age

  • Han, Min-Cheol
    • Journal of the Korea Institute of Building Construction
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    • v.12 no.1
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    • pp.87-97
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    • 2012
  • This paper presents a method of estimating the setting time of cement mortar incorporating recycled aggregate powder (RP) and cement kiln dust (CKD) at various curing temperatures by applying an equivalent age method. To estimate setting time, the equivalent age using apparent activation energy (Ea) was applied. Increasing RP and CKD leads to a shortened initial and final set. Ea at the initial set and final set obtained by Arrhenius function showed differences in response to mixture type. These were estimated to be from 10~19 KJ/mol in all mixtures, which is smaller than those of conventional mixture ranging from 30~50 KJ/mol. Based on the application of Ea to Freisleben Hansen and Pederson's equivalent age function, equivalent age is nearly constant, regardless of curing temperature and RP contents. This implies that the concept of maturity is applicable in estimating the setting time of concrete containing RP and CKD. A high correlation was observed between estimated setting time and measured setting time. A multiregression model was provided to determine setting time reflecting RP and CKD. Thus, the setting time estimation method studied herein can be applicable to concrete incorporating RP and CKD in the construction field.