• Title/Summary/Keyword: in situ physical properties

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The Performance Evaluation of In-situ Carbonation Mortar Using Gaseous CO2 (기체 CO2를 사용한 In-situ 탄산화 모르타르 성능평가)

  • Changgun Park;Deukhyun Ryu;Seongwoo Choi;Kwangwoo Wi;Seungmin Lim
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.11 no.3
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    • pp.226-233
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    • 2023
  • In this study, two phases were conducted to investigate the direct injection of gaseous CO2 into cement mortar. The aim was to advance carbon capture, utilization, and storage (CCUS) technology by harnessing industrial waste CO2 from the domestic ready-mixed concrete industry. In the first phase, the factors influencing the physical properties of cement mortar when using gaseous CO2 were identified. This included a review of materials to achieve physical properties comparable to a reference formulation. As a result of this phase, it was confirmed that traditional approaches, such as adjusting the water-to-cement ratio, had limitations in achieving the desired physical properties. Consequently, the second phase focused on the optimization of CO2-injected mortar. This involved studying the CO2 application and mixing method for cement mortar. Changes in properties were observed when gaseous CO2 was injected into the mortar. The optimal injection quantity and time to enhance the compressive strength of mortar were determinded. As a result, this study indicated that an extra mixing time exceeding 120 seconds was necessary, compared to conventional mortar. The optimal CO2 injection rate was identified as 0.1 to 0.2 % by weight of cement, taking both flowability and compressive strength performance into account. Increasing the CO2 injection time did not further enhance strength. For this approach to be employed as a CCUS technology, additional studies are required, including a microstructural analysis evaluating the amount of immobilized CO2.

In situ Electric-Field-Dependent X-Ray Diffraction Experiments for Ferroelectric Ceramics (강유전 세라믹의 전기장 인가에 따른 in situ X-선 회절 실험)

  • Choi, Jin San;Kim, Tae Heon;Ahn, Chang Won
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.35 no.5
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    • pp.431-438
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    • 2022
  • In functional materials, in situ experimental techniques as a function of external stimulus (e.g., electric field, magnetic field, light, etc.) or changes in ambient environments (e.g., temperature, humidity, pressure, etc.) are highly essential for analyzing how the physical properties of target materials are activated/evolved by the given stimulation. In particular, in situ electric-field-dependent X-ray diffraction (XRD) measurements have been extensively utilized for understanding the underlying mechanisms of the emerging electromechanical responses to external electric field in various ferroelectric, piezoelectric, and electrostrictive materials. This tutorial article briefly introduces basic principles/key concepts of in situ electric-field-dependent XRD analysis using a lab-scale XRD machine. We anticipate that the in situ XRD method provides a practical tool to systematically identify/monitor a structural modification of various electromechanical materials driven by applying an external electric field.

Synthesis and Characterization of Allyl Ester Resin-Layered Silicate Nanocomposite (알릴 에스터 수지-층상 실리케이트 나노복합재료의 합성과 특성)

  • 팽세웅;김장엽;허완수;조길원;이상원
    • Polymer(Korea)
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    • v.28 no.2
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    • pp.177-184
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    • 2004
  • Polymer-clay nanocomposite containing the low amounts of clay shows improved physical, mechanical properties. In this study, allyl ester prepolymer was synthesised by reactions of the diallyl terephthalate monomers and the 1,3-butanediol monomers. Nanocomposites of allyl ester prepolymer and the two kinds of the organically layered silicate were prepared by using the intercalation method as well as the in-situ polymerization method using. By varying the amount of clay content, curing conditions, and feeding conditions. the nanocomposite was studied using X-ray diffraction. From XRD results, allyl ester-Cloisite 30 B nanocomposite made by the in-situ polymerization method shows better exfoliation behavior compared with the intercalation method. It can be said that the transesterification reaction between functional groups (-OH) of intercalant and monomers results in the increased gallery distance. Also mechanical and thermal properties indicate that the dispersity of clay is an important factor for improving physical properties of the nanocomposite.

Correlation Analysis between Physical Properties and Compression Index for Dredged and Reclaimed Marine Clay in the Southern Coast of Korea (남해안 매립 해성점토의 물리적 특성과 압축지수의 상관성 분석)

  • Lim, Seok-Hun;Yoo, Nam-Jae
    • Journal of Industrial Technology
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    • v.34
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    • pp.53-59
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    • 2014
  • The single regression method was used to analyze the correlationship between the compression index with mechanical properties for reclaimed marine clays in the southern coast of Korea. As results of performing regression analysis for 200 samples about reclaimed marine clays in the southern coast of Korea, linear regression lines between compression index and natural water content, void ratio in situ, and liquid limit respectively wer obtained. The changed properties of soil due to disturbance during dredging and reclaiming could be investigated by comparing with the existing empirical correlation equations for the original ground where dredging was performed. These regression equations might be rationally used in the preliminary evaluation of settlement of dredged and reclaimed marine clayey ground in the southern coast of Korea.

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Study of Incipient Soot Particles with Measuring Methodologies (입자 측정방법을 통한 초기 수트입자 연구)

  • Lee Eui Ju
    • Journal of the Korean Society of Visualization
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    • v.2 no.1
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    • pp.12-17
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    • 2004
  • The physical characteristics of soot near the soot inception point were investigated with various measurements. In-situ measurements of particle size and volume fraction were introduced based on time resolved laser-induced incandescence (TIRE-LII) and laser-induced ion mobility (LIIM). The one has more convenience and accuracy than conventional LII technique and the other works best for particle sizes of a few nanometers at high concentrations in a uniform concentration field. A complementary ex-situ measurement of particle size is nano differential mobility analyzer (Nano-DMA), which recently developed for measuring particle sizes between 2nm and 100nm and provides high-resolution size information for early soot. Particles will be also collected on transmission electron microscope (TEM) grids using rapid thermophoretic sampling and analyzed for morphology. These measurements will allow fresh and original insight into the characterizing soot inception process. The measured physical properties of incipient soot will clarify the controlling growth mechanism combined with chemical ones, and the dominant mechanism for soot modeling can be deduced from the information.

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In-situ Application of Glossy Architectural Concrete (광택노출콘크리트의 현장 기술)

  • 정태웅;이현희;하재담;강창운
    • Proceedings of the Korea Concrete Institute Conference
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    • 1999.04a
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    • pp.836-839
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    • 1999
  • Glossy architectural concrete means high qulity concrete which develops marble-like gloss on the surface of concrete. In spite of many benefits of architectural concrete to R.C. structure such as appearance of natural stone, saving of envelope materials and reduction of building weight, the failure of in-situ application of architectural concrete by the absence of knowledge on the physical properties and form work for it can often be found in Korea. This study is to offer the basic materials on the mix proportion, vibrating, curing and treatment of concrete result from the mock up test and in-situ application of architectural concrete to embody high quality architectural concrete in Korea.

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In-Situ Formation of Porous HAp Using Polymer Foam Process (폴리머 발포법을 이용한 다공성 HAp 지지체의 제조 및 특성 평가)

  • Kim, Zin-Kook;Ji, Sang-Yong;Ji, Hyung-Bin;Park, Hong-Chae;Yoon, Seog-Young
    • Korean Journal of Materials Research
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    • v.18 no.6
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    • pp.289-293
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    • 2008
  • Porous HAp with three-dimensional network channels was prepared in a polymer foam process using a in-situ formation. HAp/polyol with various HAp solid contents was formed with an addition of isocyanate. Under all conditions, the obtained porous HAp had pore sizes ranging $50\;{\mu}m$ to $250\;{\mu}m$. The influence of the HAp content on the physical and mechanical properties of porous HAp scaffolds was investigated. As the solid content increased, the porosity of the porous HAp decreased from 79.3% to 77.9%. On the other hand, the compressive strength of the porous HAp increased from 0.7 MPa to 3.7 MPa. With a HAp solid content of 15 g, the obtained porous HAp had physical properties that were more suitable for scaffolds compared to other conditions.

Parametric study of ICME properties affecting space weather disturbances at 1 AU

  • An, Junmo;Magara, Tetsuya;Hayashi, Keiji;Moon, Yong-Jae
    • The Bulletin of The Korean Astronomical Society
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    • v.44 no.2
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    • pp.40.4-40.4
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    • 2019
  • Interplanetary coronal mass ejections (ICMEs) are regarded as one of the most powerful sources of space weather disturbances observed near the Earth orbit (1 AU). In this study, we aim at investigating the relation between these disturbances and the physical properties of an ICME. Toward this end, we used an spheromak-type ICME and performed a series of three-dimensional magnetohydrodynamic (MHD) simulations with different sets of ICME parameters. The ICME is injected into the background solar wind generated from near-Sun data and interplanetary scintillation (IPS) data via an MHD-IPS tomography method. We will compare simulation results to in situ observations near the Earth and discuss how the physical properties of an ICME affect the space weather disturbances at 1 AU.

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Estimation of saturated hydraulic conductivity of Korean weathered granite soils using a regression analysis

  • Yoon, Seok;Lee, Seung-Rae;Kim, Yun-Tae;Go, Gyu-Hyun
    • Geomechanics and Engineering
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    • v.9 no.1
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    • pp.101-113
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    • 2015
  • Saturated soil hydraulic conductivity is a very important soil parameter in numerous practical engineering applications, especially rainfall infiltration and slope stability problems. This parameter is difficult to measure since it is very highly sensitive to various soil conditions. There have been many analytical and empirical formulas to predict saturated soil hydraulic conductivity based on experimental data. However, there have been few studies to investigate in-situ hydraulic conductivity of weathered granite soils, which constitute the majority of soil slopes in Korea. This paper introduces an estimation method to derive saturated hydraulic conductivity of Korean weathered granite soils using in-situ experimental data which were obtained from a variety of slope areas of South Korea. A robust regression analysis was performed using different physical soil properties and an empirical solution with an $R^2$ value of 0.9193 was suggested. Besides that this research validated the proposed model by conducting in-situ saturated soil hydraulic conductivity tests in two slope areas.

The Mechanical Properties of Rocks Distributed at a Metal Mine in Jeongseon (정선지역 철광산에 분포하는 암석의 역학적 특성)

  • Kim, Jong-Woo;Park, Chan;Kim, Ju-Hwan;Heo, Seok;Kim, Dong-Kyu;Lee, Dong-Kil;Jo, Young-Do;Park, Sam-Gyu
    • Tunnel and Underground Space
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    • v.25 no.3
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    • pp.231-243
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    • 2015
  • In this study, both in-situ stress measurements and a lot of laboratory rock tests were conducted at a metal mine in Jeongseon, Korea. The stress ratio obtained from in-situ stress measurements showed a tendency to decrease according to depth below surface and its average value was 1.10. The mechanical properties such as unit weight, absorption ratio, porosity, elastic wave velocity, uniaxial compressive strength, Young's modulus, Poisson's ratio, tensile strength, shore hardness, friction angle and cohesion were investigated for the four different rocks mainly distributed at a studied mine, which were dolomite, felsite, granite and magnetite. The mechanical properties of the four different rocks were compared by means of statistical analyses, whereupon the felsite and the granite turned out to have more strength characteristics than the magnetite. The correlation of mechanical properties was also investigated, whereupon a few results against the general correlation were found out. The failure criteria of the four different rocks were finally discussed by means of both Mohr-Coulomb criterion and Hoek-Brown criterion.