• Title/Summary/Keyword: hot-pressing time

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Sintering Characterization of Alumina Powders by Hot Pressing after Cold Cyclic Compaction -Densification, Grain-Growth and Fracture Toughness- (상온 반복압축 후 가압소결에 의한 알루미나 분말의 소결특성 -치밀화와 결정립 성장 및 파괴인성-)

  • Son, G.S.;Suh, J.;Baik, S.K.;Kim, K.T.
    • Journal of the Korean Ceramic Society
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    • v.30 no.1
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    • pp.62-68
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    • 1993
  • Densification of alumina powder, grain size and fracture toughness of sintered body by hot pressing after cold compaction were investigated and compared to traditional hot pressing process (without cold cyclic compaction). To achieve a higher densification and to reduce the hot pressing time, hot pressing after cold cyclic compaction was more efficient compared to traditional hot pressing. This phenomenon resulted from the increment of packing densityby the acceleration fo rearrangement of powders under cold cyclic compaction. The grain size of sintered body was only dependent on relative density, and densification during hot pressing was governed by thelattice diffusion. Comprisons of grain size, densification mechanism and fracture toughness resulted from hot pressing after/without cold cyclic compaction showed that a low cyclic pressure may not effect on the fragmentation of alumina powders.

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Investigation on the mechanism of heat transfer in hot-pressing process of fiberboard manufacturing for laminate flooring (강화마루용 섬유판 열압공정에서의 열전달 원리에 대한 고찰)

  • Kim, Su-Min
    • Journal of the Korea Furniture Society
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    • v.20 no.5
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    • pp.490-503
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    • 2009
  • The objective of this work was to investigate the mechanism of heat transfer in hot-pressing process for MDF manufacturing by reference study. Firstly, general heat transfer theory was studied. The numerical analysis of heat transfer in hot-pressing process was studied on temperature profile, moisture profile, physical properties between moisture and board. The mechanism of heat and moisture transfer inside of board was analyzed by conduction, convection, radiation and diffusion of bound water in wood cell walls. Especially, the change of core temperature as hot press time was important factor to setup hot-pressing schedule in MDF manufacturing.

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Effect of Hot-Pressing Time and Temperature on Properties of Bamboo Zephyr Boards (대나무 Zephyr 보드의 제조에 있어서 열압시간과 열압온도가 보드성능에 미치는 영향)

  • Jung, Ki-Ho;Kim, Yu-Jung;Roh, Jeang-Kwan;Park, Sang-Jin
    • Journal of the Korean Wood Science and Technology
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    • v.31 no.2
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    • pp.77-83
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    • 2003
  • In this research, in order to investigate the effect of hot-pressing condition, properties of bamboo zephyr boards (target density 0.7 g/cm3, 400×400×12 mm) produced by different hot-pressing time and temperature were compared through Korean Standard(KS) F 3104 and F 3113, and the results were summarized as follows: All of the boards had comparatively high values in bending properties (MOR, MOE) irrespective of hot-pressing condition, and the boards hot-pressed by 160℃ and 12 min showed the highest strength in parallel direction of board-surface to span. Internal bond (IB) strength of the boards generally increased with the increase of hot pressing temperature. Boards produced by hot pressing temperature and time of 160℃ and 12 min and 180℃ and 10 min exhibited relatively higher wet-bending strength. Thickness swelling (TS) of all the boards showed good dimensional stability of 6% or less.

Hot-Pressing of Silicon Nitride Containing Low Amounts of $Y_2O_3$ and AlN (Y2O3-AlN 미량첨가 질화규소의 열간가압소결)

  • 조덕호;이형복
    • Journal of the Korean Ceramic Society
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    • v.29 no.2
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    • pp.143-151
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    • 1992
  • Partially stabilized alpha-sialon composition (X=0.1) powder was hot-pressed at 1800~200$0^{\circ}C$ for 0~90 min with 30 MPa. Sintering behavior, phase changes and mechanical properties for the specimens were studied. As sintering temperature was raised from 1800 to 190$0^{\circ}C$, the relative density tended to increase and reached 99% of theoretical at 190$0^{\circ}C$. However the amount of alpha-sialon decreased because alpha-sialon transformed to beta-Si3N4 and yttrium rich silicate glass. In the case of hot-pressing at 190$0^{\circ}C$ for various times, densification increased with sintering time and full densification above 99% of theoretical was attained by 30 min. The amount of alpha-sialon decreased with sintering time. The maximum strength of 825 MPa was obtained by hot-pressing at 190$0^{\circ}C$ for 60 min.

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Hot-Pressing Effects on Polymer Electrolyte Membrane Investigated by 2H NMR Spectroscopy

  • Lee, Sang Man;Han, Oc Hee
    • Bulletin of the Korean Chemical Society
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    • v.34 no.2
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    • pp.510-514
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    • 2013
  • The structural change of Nafion polymer electrolyte membrane (PEM) induced by hot-pressing, which is one of the representative procedures for preparing membrane-electrode-assembly for low temperature fuel cells, was investigated by $^2H$ nuclear magnetic resonance (NMR) spectroscopy. The hydrophilic channels were asymmetrically flattened and more aligned in the membrane plane than along the hot-pressing direction. The average O-$^2H$ director of $^2H_2O$ in polymer electrolyte membrane was employed to extract the structural information from the $^2H$ NMR peak splitting data. The dependence of $^2H$ NMR data on water contents was systematically analyzed for the first time. The approach presented here can be used to understand the chemicals' behavior in nano-spaces, especially those reshaping and functioning interactively with the chemicals in the wet and/or mixed state.

A Study on Texture Development in Liquid-Phase Sintered Silicon Carbide (액상소결한 탄화규소의 집합조직 발달에 관한 연구)

  • 성한규;조경식;박노진;최헌진;이준근
    • Journal of the Korean Ceramic Society
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    • v.37 no.4
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    • pp.320-326
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    • 2000
  • Development of texture in SiC materials by hot-pressing and subsequent annealing was studied. Crystallographic texture type was characterized by measuring X-ray pole figures on the perpendicular plane to the hot-pressing direction. Observed all pole figures were nearly axially symmetric (fiber texture). In case of ${\beta}$-SiC materials, the pole density of basal plane (0004) increased as annealing time increased, in contrast, other planes (hkil) of ${\beta}$-SiC materials and all planes of ${\alpha}$-SiC materials nearly remained unchanged. In the case of ${\beta}$-SiC materials, therefore, a weak texture of (0001) plane at the normal direction took place in the 8h annealed samples, resulting from grian growth. The fracture toughness values of ${\alpha}$-SiC materials measured in both planes parallel and perpendicular to the hot-pressing direction were very similar. However, the fracture toughness of ${\beta}$-SiC materials measured parallel to the hot-pressing direction were higher than that measured perpendicular to the hot-pressing derection, relatively, because of the texture and the microstructure anisotropy.

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Studies on Wood-based Composite Panel with Waste Tire - Properties of Composite Boards in Relation to Hot Pressing Conditions - (폐타이어를 이용한 목질계 복합판넬의 연구 - 열압조건에 의한 재질특성 -)

  • Lee, Weon-Hee;Park, Sang-Jin
    • Journal of the Korean Wood Science and Technology
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    • v.25 no.4
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    • pp.29-38
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    • 1997
  • The effect and control of wood property of reconstituted composite panels for improved board properties by wood-waste materials and development of combination method for heterogeneous materials have been of interest to the wood science researchers. The purpose of this study is to consider the properties in relation to hot pressing conditions and to develope the optimum hot pressing condition with waste wood and waste tire for the manufacturing of composite boards. The study of composite boards for recycling of wood and waste tire is nothing up to the present. Physical and mechanical properties such as specific gravity, moisture content, swelling coefficient, modulus of rupture and modulus of elasticity in bending test were studied. The condition of 3-stage press time for the lowest moisture content of composite board was $4{\rightarrow}3{\rightarrow}3$ minutes. Specific gravity of composite panels was affected mainly by the amount of rubber chip. Because of the low rigidity and high elasticity in rubber chip, it is considered the composite panel was adequate material in the place of compression load, but not bending load. Therefore, it was concluded that a use of rubber-based wood composite panel is proper to the interior materials such as floor a room than exterior materials. From the test results, the most optimum hot pressing conditions were $4{\rightarrow}3{\rightarrow}3$ minutes for 3-stage press time and $45{\rightarrow}20{\rightarrow}5kg/cm^2$ for 3-stage press pressure. The rubber-based wood composite panel was very excellent in elasticity by combination of rubber chip in comparison with existing other wood-based materials. Therefore, it was considered that rubber-based wood composites can be applicable to every interior materials such as floor a room and will be expected to effective reuse and recycle of waste tires and wood-waste materials, and will be contribute to protection of environment pollution in earth.

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Examination of Formaldehyde Emissions from the Hot-Pressing of Particleboard (파티클보드의 열압으로부터 포름알데히드 배출량 조사)

  • Oh, Yong-Sung;Kwak, Jun-Hyuk
    • Journal of the Korean Wood Science and Technology
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    • v.29 no.4
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    • pp.33-39
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    • 2001
  • Laboratory particleboards (PBs) were made with urea-formaldehyde (UF) resins at four press times and two resin application rates. Enclosed caul system was used for collecting the exhaust gases materials generated during the hot-pressing of PB. Exhaust gases materials generated inside the enclosed caul during the hot-pressing of PB were collected in a controlled air stream. Formaldehyde from the exhaust gases collected was determined per a chromotropic method of the National Institute of Occupational Safety and Health Method 3500. The test results showed that formaldehyde emissions during the hot-pressing of PB increased with increasing press time, UF resin mole ratio, and resin application rate.

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The Effect of La-silicon Oxynitride on the Densification of ${Si_3}{N_4}$ Ceramics by Spark Plasma Sintering

  • Cho, Kyeong-Sik;Kim, Sungjin;Beak, Sung-Ho;Park, Heon-Jin;Lee, June-Gunn
    • Journal of the Korean Ceramic Society
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    • v.38 no.8
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    • pp.687-692
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    • 2001
  • Silicon nitride-La-silicon oxynitride ceramics were fabricated by Spark Plasma Sintering (SPS). The density, crystalline phase and microstructure were compared with those obtained by Hot Pressing (HP). The full density was achieved within 40 min by spark plasma sintering at 1$650^{\circ}C$, whereas the same result was required by hot pressing with a dwell time of 500 min at higher temperature. There were some differences in the microstructure and second phases in the sintered ceramics, which are attributed to the rapid densification in the spark plasma sintering. The fine and acicular grain microstructure appeared in spark plasma sintering.

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Adhesion Characteristics and Anatomic Scanning of Plywood Bonded by High Density Polyethylene (고밀도 폴리에틸렌으로 접착한 합판의 접착성질과 해부학적 관찰)

  • Han, Kie-Sun;Lee, Hwa-Hyoung
    • Journal of the Korean Wood Science and Technology
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    • v.25 no.3
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    • pp.16-23
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    • 1997
  • This study was carried out to discuss feasibility of high density polyethylene(HDPE) as a new substitute for the conventional adhesives in plywood manufacture. Plywood was composed of radiata pine(Pinus radiata) and Malas(Homallium feotidium) veneers and bonded by HDPE. Adhesion characteristics and anatomical scanning has been examined through tensile-shear strength test and scanning electron microscopy(SEM). The results are as follows; 1. Optimum loading quantity was 15g/$(30.3{\times}30.3)cm^2$, and tensile-shear strength increased with the increase of loading quantity. 2. Even at the hot pressing time of 1 minute, tensile-shear strength met the value of KS(over the 7.5kgf/$cm^2$), and tensile-shear strength increased with the increase of hot pressing time. 3. Plywood composed of veneer at moisture content of 19.6% showed similar tensile-shear strength to that at air conditioned moisture content of 11.4%. 4. Under the same condition of hot pressing time, tensile-shear strength of plywood bonded by HDPE met the KS value of boil and wet test and proved the same group as phenol formaldehyde adhesive. 5. HDPE films showed mechanical adhesion through penetration into the lathe check and ray of veneer.

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