• Title/Summary/Keyword: hot-pressing temperature

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Effects of Vacuum Hot Pressing Conditions on Mechanical Properties and Microstructures of $SiC_w$/2124Al Metal Matrix Composites (Vacuum Hot Pressing 조건이 $SiC_w$/2124AI 금속복합재료의 기계적 성질 및 미세구조에 미치는 영향)

  • 홍순형
    • Journal of Powder Materials
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    • v.1 no.2
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    • pp.159-166
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    • 1994
  • The variation of the microstructures and the mechanical properties with varying vacuum hot pressing temperature and pressure was investigated in PyM processed 20 vol%) SiCw/ 2124Al composites. As increasing the vacuum hot pressing temperature, the aspect ratio of whiskers and density of composites increased due to the softening of 2124Al matrix with the increased amount of liquid phase. The tensile strength of composite increased with increasing vacuum hot pressing temperature up to $570^{\circ}C$ and became saturated above $570^{\circ}C$, To attain the high densification of composites above 99%, the vacuum hot pressing pressure was needed to be above 70 MPa. However, the higher vacuum hot pressing pressure above 70 MPa was not effective to increase the tensile strength due to the reduced aspect ratio of SiC whiskers from damage of whiskers during vacuum hot pressing. A phenomenological equation to predict the tensile strength of $SiC_w$/2124AI composite was proposed as a function including two microstructural parameters, i.e. density of composites and aspect ratio of whiskers. The tensile strength of $SiC_w$/2124AI were found more sensitive to the porosity than other P/M materials due to the higher stress concentration and reduced load transfer efficiency by the pores locating at whisker/matrix interfaces.

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Near-net-shape forming of ceramic powder under hot pressing and hot isostatic pressing (가압소결과 열간 등가압소결에 의한 세라믹 분말의 정형 성형)

  • Kwon, Yeong-Sam;Kim, Ki-Tae
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.21 no.1
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    • pp.73-82
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    • 1997
  • High temperature densification behaviors of alumina powder compacts were investigated under hot pressing and hot isostatic pressing. An alumina part of valve-head shape was fabricated under hot pressing and its forming process was simulated by finite element calculation. an alumina powder compact encapsulated by a stainless steel container was also densified under hot isostatic pressing. Inhomogeneous deformations during hot isostatic pressing due to the canning effect were observed experimentally and predicted by finite element analysis.

Densification Behavior of Mixed Metal Powders under High Temperature (혼합 금속 분말의 고온 치밀화 거동)

  • Jo, Jin-Ho;Kim, Gi-Tae
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.3 s.174
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    • pp.735-742
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    • 2000
  • Densification behaviors of mixed metal powder under high temperature were investigated. Experimental data of mixed copper and tool steel powder with various volume fractions of Cu powder were obtained under hot isostatic pressing and hot pressing. By mixing the creep potentials of McMeeking and co-workers and of Abouaf and co-workers originally for pure powder, the mixed creep potentials with various volume fractions of Cu powder were employed in the constitutive models. The constitutive equations were implemented into a finite element program (ABAQUS) to compare with experimental data for densification of mixed powder under hot isostatic pressing and hot pressing. Finite element calculations by using the creep potentials of Abouaf and co-workers agreed reasonably well with experimental data, however, those by McMeeking and co-workers underestimate experimental data as observed in the case of pure metal powders.

Direct Solid State Synthesis of Zn4Sb3 by Hot Pressing and Thermoelectric Properties (열간 압축 공정에 의한 Zn4Sb3의 직접 고상 반응 합성 및 열전특성)

  • Ur Soon-Chul
    • Journal of Powder Materials
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    • v.12 no.4 s.51
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    • pp.255-260
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    • 2005
  • Direct solid state synthesis by hot pressing has been applied in order to produce high efficiency $Zn_4Sb_3$ bulk specimens. Single phase $Zn_4Sb_3$ with 98.5% of theoretical density was successfully produced by direct hot pressing of elemental powders containing 1.2 at.% excess Zn. Thermoelectric properties as a function of temperature were investigated from room temperature to 600 K and compared with results of other studies. Transport properties at room temperature were also evaluated. Thermoelectric properties of single phase $Zn_4Sb_3$ materials produced by direct synthesis were measured and are comparable to the published data. Direct solid state synthesis by hot pressing provides a promising processing route in this material.

Investigation on the mechanism of heat transfer in hot-pressing process of fiberboard manufacturing for laminate flooring (강화마루용 섬유판 열압공정에서의 열전달 원리에 대한 고찰)

  • Kim, Su-Min
    • Journal of the Korea Furniture Society
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    • v.20 no.5
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    • pp.490-503
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    • 2009
  • The objective of this work was to investigate the mechanism of heat transfer in hot-pressing process for MDF manufacturing by reference study. Firstly, general heat transfer theory was studied. The numerical analysis of heat transfer in hot-pressing process was studied on temperature profile, moisture profile, physical properties between moisture and board. The mechanism of heat and moisture transfer inside of board was analyzed by conduction, convection, radiation and diffusion of bound water in wood cell walls. Especially, the change of core temperature as hot press time was important factor to setup hot-pressing schedule in MDF manufacturing.

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Sintering of Magnesia During Hot Pressing (Hot Press에 의한 마그네시아의 소결)

  • 오기동
    • Journal of the Korean Ceramic Society
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    • v.19 no.2
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    • pp.152-156
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    • 1982
  • The behavior of magnesite during hot pressing is studied from 80$0^{\circ}C$ to 110$0^{\circ}C$ by Knoop hardness test, X-ray diffraction and electron microscopy. The growth of magnesia crystallite in magnesite is observed at 110$0^{\circ}C$ and crystallite size is about 2 microns. It is also observed that hot pressing showes enhanced sinterability comparing to ordinary pressure-less sintering. The magnesia body with 95 per cent of theoretical density is obtained by hot pressing at relatively low temperature such as 110$0^{\circ}C$.

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Microstructures and Tensile Properties of $A_2O_3$ Short Fiber/Al-Si-Mg Alloy Composites Fabricated by Rheo-compocasting and Hot Pressing (Rheo-compocasting 및 Hot Pressing에 의하여 제조한 $Al-Si-Mg/Al_2O_3$ 단섬유강화 복합재료의 조직 및 인장특성)

  • Kwak, Hyun-Man;Lee, Hag-Ju
    • Journal of Korea Foundry Society
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    • v.13 no.6
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    • pp.547-554
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    • 1993
  • Aluminum alloy matrix composites reinforced with various amounts of $Al_2O_3$ short fibers have been produced by rheo-compocasting accompanied by hot pressing. When composites reinforced with fibers are produced by rheo-compocasting, S-L process is the most effective method for homogeneous dispersion of fibers. A sound composites with the improved orientation(3 dimension${\rightarrow}$2 dimension) of the fibers and increased volume fraction of them have been fabricated through the hot pressing of the casted composites. Fibers are broken down when rheo-compocasting, hot pressing, and $T_6$ treating. Among them fibers are broken down most heavily in the hot pressing. And even in the case of the composite reinforced with 30 vol% fibers, which showed the hardest fiber break down, aspect ratio(11.6) is higher than critical aspect ratio(10.7). The fiber strengthening effect in the composites has showed upto 573K. As the test temperature increases to the range of 573K, the effect has been higher. The fracture of composites is controlled by fiber from room temperature to 473K, but the fracture of composites is controlled by interface between fiber and matrix alloy above 473K.

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Synthesis of Zn4Sb3 by Solid State Reaction and Hot Pressing, and Their Thermoeletric Properties (고상 합성과 진공 압축성형에 의한 Zn4Sb3의 제조 및 열전특성)

  • Ur Soon-Chul
    • Korean Journal of Materials Research
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    • v.15 no.7
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    • pp.473-479
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    • 2005
  • Thermoelectric $Zn_4Sb_3$ alloys were synthesized by a conventional powder metallurgy process consisting of solid state reaction and hot pressing. Single phase $Zn_4Sb_3$ was successfully produced by the annealing of cold compact starting with the mixed elemental powders, and subsequent hot pressing yielded single phase bulk specimens without microcracks. Phase transformations in this alloy system during synthesis were investigated using XRD, SEM and EDS. Thermoelectric properties as a function of temperature were investigated from room temperature to 600 K and compared with results of analogue studies. Transport properties at room temperature were also evaluated. Thermoelectric properties of single phase $Zn_4Sb_3$ materials produced by this process are comparable to the published data. Synthesis by solid state reaction and hot pressing offers a potential processing route to produce a bulk $Zn_4Sb_3$

Effect of Hot-Pressing Time and Temperature on Properties of Bamboo Zephyr Boards (대나무 Zephyr 보드의 제조에 있어서 열압시간과 열압온도가 보드성능에 미치는 영향)

  • Jung, Ki-Ho;Kim, Yu-Jung;Roh, Jeang-Kwan;Park, Sang-Jin
    • Journal of the Korean Wood Science and Technology
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    • v.31 no.2
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    • pp.77-83
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    • 2003
  • In this research, in order to investigate the effect of hot-pressing condition, properties of bamboo zephyr boards (target density 0.7 g/cm3, 400×400×12 mm) produced by different hot-pressing time and temperature were compared through Korean Standard(KS) F 3104 and F 3113, and the results were summarized as follows: All of the boards had comparatively high values in bending properties (MOR, MOE) irrespective of hot-pressing condition, and the boards hot-pressed by 160℃ and 12 min showed the highest strength in parallel direction of board-surface to span. Internal bond (IB) strength of the boards generally increased with the increase of hot pressing temperature. Boards produced by hot pressing temperature and time of 160℃ and 12 min and 180℃ and 10 min exhibited relatively higher wet-bending strength. Thickness swelling (TS) of all the boards showed good dimensional stability of 6% or less.

Thermoelectric Property and p-n Transition Mechanism of Hot Pressed Bi4/3Sb2/3Te3 ($Bi_{4/3}Sb_{2/3}Te_3$ 가압소결체의 열전특성과 p-n 전이기구)

  • 박태호;유한일;심재동
    • Journal of the Korean Ceramic Society
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    • v.29 no.11
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    • pp.855-862
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    • 1992
  • Thermoelectric power, electrical conductivity and Hall effect were measured, as functions of temperature in the range of 100 to 600 K, on polycrystalline Bi4/3Sb2/3Te3 which had been prepared via uniaxial hot-pressing at different temperatures in the range of 373 K to 773 K, aiming at searching a profitable processing route to a polycrystalline thermoelectric material, a promising, viable alternative to a single crystalline one. It was found that, with increasing temperature of pressing under a fixed pressure, the material, normally a p-type prior to being hot-pressed, underwent a transition to n-type. This transition was confirmed to be due to plastic deformation during hot-pressing and interpreted as being attributed to the change of the major ionic defect BiTe' into TeBi˙at temperature high enough for structure elements mobility. Thermoelectric figure-of-merit of the hot-pressed material was discussed in connection with the p-n transition in addition to microstructure.

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